ES2093705T3 - Metodo para fabricar membranas de fibras huecas de pvdf. - Google Patents

Metodo para fabricar membranas de fibras huecas de pvdf.

Info

Publication number
ES2093705T3
ES2093705T3 ES91909883T ES91909883T ES2093705T3 ES 2093705 T3 ES2093705 T3 ES 2093705T3 ES 91909883 T ES91909883 T ES 91909883T ES 91909883 T ES91909883 T ES 91909883T ES 2093705 T3 ES2093705 T3 ES 2093705T3
Authority
ES
Spain
Prior art keywords
solvent
polymer
phase
polyvinyldene
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES91909883T
Other languages
English (en)
Other versions
ES2093705T5 (es
Inventor
Thomas William Beck
Matthew Brian Lee
Richard David Grant
Robert John William Streeton
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Memtec Ltd
Original Assignee
Memtec Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=3774654&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2093705(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Memtec Ltd filed Critical Memtec Ltd
Application granted granted Critical
Publication of ES2093705T3 publication Critical patent/ES2093705T3/es
Publication of ES2093705T5 publication Critical patent/ES2093705T5/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/28—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof by elimination of a liquid phase from a macromolecular composition or article, e.g. drying of coagulum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0002—Organic membrane manufacture
    • B01D67/0009—Organic membrane manufacture by phase separation, sol-gel transition, evaporation or solvent quenching
    • B01D67/0011—Casting solutions therefor
    • B01D67/00111—Polymer pretreatment in the casting solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0002—Organic membrane manufacture
    • B01D67/0009—Organic membrane manufacture by phase separation, sol-gel transition, evaporation or solvent quenching
    • B01D67/0018—Thermally induced processes [TIPS]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0002—Organic membrane manufacture
    • B01D67/0023—Organic membrane manufacture by inducing porosity into non porous precursor membranes
    • B01D67/0025—Organic membrane manufacture by inducing porosity into non porous precursor membranes by mechanical treatment, e.g. pore-stretching
    • B01D67/0027—Organic membrane manufacture by inducing porosity into non porous precursor membranes by mechanical treatment, e.g. pore-stretching by stretching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
    • B01D67/0002—Organic membrane manufacture
    • B01D67/0023—Organic membrane manufacture by inducing porosity into non porous precursor membranes
    • B01D67/003—Organic membrane manufacture by inducing porosity into non porous precursor membranes by selective elimination of components, e.g. by leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/02—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor characterised by their properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D69/00—Semi-permeable membranes for separation processes or apparatus characterised by their form, structure or properties; Manufacturing processes specially adapted therefor
    • B01D69/08—Hollow fibre membranes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D71/00—Semi-permeable membranes for separation processes or apparatus characterised by the material; Manufacturing processes specially adapted therefor
    • B01D71/06—Organic material
    • B01D71/30—Polyalkenyl halides
    • B01D71/32—Polyalkenyl halides containing fluorine atoms
    • B01D71/34—Polyvinylidene fluoride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/08—Specific temperatures applied
    • B01D2323/081—Heating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2323/00—Details relating to membrane preparation
    • B01D2323/12—Specific ratios of components used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2327/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
    • C08J2327/02—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
    • C08J2327/12—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C08J2327/16—Homopolymers or copolymers of vinylidene fluoride

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Artificial Filaments (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)

Abstract

UN METODO PARA FABRICAR UN MATERIAL POLIMERICO POROSO CALENTANDO UNA MEZCLA QUE COMPRENDE FLUORURO DE POLIVINILDENO Y UN SISTEMA DISOLVENTE QUE COMPRENDE, INICIALMENTE, UN PRIMER COMPONENTE QUE ES UN DISOLVENTE LATENTE PARA EL FLUORURO DE POLIVINILDENO Y UN SEGUNDO COMPONENTE QUE NO ES UN DISOLVENTE PARA EL FLUORURO DE POLIVINILDENO EN DONDE, A TEMPERATURA ELEVADA, EL FLUORURO DE POLIVINILDENO SE DISUELVE EN EL SISTEMA DISOLVENTE PARA PROPORCIONAR UNA SOLUCION OPTICAMENTE TRANSPARENTE. A CONTINUACION, LA SOLUCION SE ENFRIA RAPIDAMENTE PARA QUE NO TENGA LUGAR UNA SEPARACION DE FASE LIQUIDO-LIQUIDO NO EQUILIBRADA CON EL FIN DE FORMAR UNA FASE CONTINUA RICA EN POLIMERO Y UNA FASE CONTINUA POBRE EN POLIMERO ENTREMEZCLANDOSE LAS DOS FASES EN FORMA DE UNA MATRIZ BICONTINUA CON UNA GRAN AREA INTERFACIAL, Y SE PROSIGUE CON EL ENFRIADO HASTA QUE LA FASE RICA EN POLIMERO SE SOLIDIFICA. SE EXTRAE LA FASE POBRE DE POLIMERO DEL MATERIAL POLIMERICO SOLIDO. UN MATERIAL POROSO PREPARADO DE ESTA FORMA SE CARACTERIZA POR UNA ESTRUCTURA FINA O FILAMENTOSA FORMADA POR UNA PLURALIDAD DE HEBRAS DE POLIMERO (1) UNIDAS EN MUCHOS LUGARES (2) ESPACIADOS A LO LARGO DE CADA HEBRA.
ES91909883T 1990-05-09 1991-05-09 Metodo para fabricar membranas de fibras huecas de pvdf. Expired - Lifetime ES2093705T5 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AUPK003690 1990-05-09
PCT/AU1991/000198 WO1991017204A1 (en) 1990-05-09 1991-05-09 Polyvinylidene fluoride membrane

Publications (2)

Publication Number Publication Date
ES2093705T3 true ES2093705T3 (es) 1997-01-01
ES2093705T5 ES2093705T5 (es) 2000-12-01

Family

ID=3774654

Family Applications (2)

Application Number Title Priority Date Filing Date
ES91909883T Expired - Lifetime ES2093705T5 (es) 1990-05-09 1991-05-09 Metodo para fabricar membranas de fibras huecas de pvdf.
ES96105245T Expired - Lifetime ES2129245T3 (es) 1990-05-09 1991-05-09 Membrana de poli(fluoruro de vinilideno).

Family Applications After (1)

Application Number Title Priority Date Filing Date
ES96105245T Expired - Lifetime ES2129245T3 (es) 1990-05-09 1991-05-09 Membrana de poli(fluoruro de vinilideno).

Country Status (6)

Country Link
EP (2) EP0734759B1 (es)
JP (1) JP3442384B2 (es)
CA (1) CA2082511C (es)
DE (2) DE69122754T3 (es)
ES (2) ES2093705T5 (es)
WO (1) WO1991017204A1 (es)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL9102151A (nl) * 1991-12-20 1993-07-16 Delair Droogtech & Lucht Het spinnen van asymmetrische holle vezelmembranen met een dichte, niet-poreuze toplaag en een poreuze onderlaag, resp. met zowel een poreuze toplaag als een poreuze onderlaag.
DE69322776T2 (de) * 1992-05-06 1999-08-05 Costar Corp., Cambridge, Mass. Verfahren zur herstellung einer mikroporösen polyvinylidenfluorid-membran
US5444097A (en) * 1992-07-07 1995-08-22 Millipore Corporation Porous polymeric structures and a method of making such structures by means of heat-induced phase separation
US5418091A (en) * 1993-03-05 1995-05-23 Bell Communications Research, Inc. Polymeric electrolytic cell separator membrane
US6235377B1 (en) * 1995-09-05 2001-05-22 Bio Med Sciences, Inc. Microporous membrane with a stratified pore structure created in situ and process
TW581709B (en) 1999-10-22 2004-04-01 Asahi Kasei Corp Heat-resistant microporous film
WO2003026779A1 (en) 2001-08-01 2003-04-03 Asahi Kasei Kabushiki Kaisha Multilayer microporous film
EP1435261B1 (en) * 2001-10-04 2009-06-17 Toray Industries, Inc. Method for production of a hollow fiber membrane
AU2003301399B2 (en) 2002-10-18 2006-07-06 Asahi Kasei Medical Co., Ltd. Microporous hydrophilic membrane
AU2003903507A0 (en) 2003-07-08 2003-07-24 U. S. Filter Wastewater Group, Inc. Membrane post-treatment
US7819956B2 (en) 2004-07-02 2010-10-26 Siemens Water Technologies Corp. Gas transfer membrane
CN101342465B (zh) * 2008-09-01 2011-11-09 天津工业大学 一种中空纤维多孔膜及其制备方法
ATE528066T1 (de) 2008-12-12 2011-10-15 Membrana Gmbh Hydrophobe ozonstabile pvdf-membran mit hoher mechanischer stabilität
US20130327711A1 (en) * 2012-06-11 2013-12-12 Great Salt Lakes Minerals Corporation Methods for sustainable membrane distillation concentration of hyper saline streams
KR20150054918A (ko) 2012-09-14 2015-05-20 에보쿠아 워터 테크놀로지스 엘엘씨 막을 위한 중합체 블렌드
US10946345B2 (en) 2013-05-29 2021-03-16 Em Innovative Properties Company Microporous polyvinylidene fluoride membrane
CN107073411B (zh) 2014-11-03 2021-05-07 3M创新有限公司 微孔聚偏二氟乙烯平膜
WO2017011068A1 (en) 2015-07-14 2017-01-19 Evoqua Water Technologies Llc Aeration device for filtration system
AU2018212812A1 (en) 2017-01-26 2019-08-15 Dassault Systemes Simulia Corp. Multi-phase flow visualizations based on fluid occupation time
US11714040B2 (en) 2018-01-10 2023-08-01 Dassault Systemes Simulia Corp. Determining fluid flow characteristics of porous mediums
US11530598B2 (en) 2018-08-21 2022-12-20 Dassault Systemes Simulia Corp. Determination of oil removed by gas via miscible displacement in reservoir rock
CN110064309B (zh) * 2019-04-15 2021-06-15 沈阳环境科学研究院 一种mabr用复合膜及制备方法
US11847391B2 (en) 2020-06-29 2023-12-19 Dassault Systemes Simulia Corp. Computer system for simulating physical processes using surface algorithm
US11907625B2 (en) 2020-12-29 2024-02-20 Dassault Systemes Americas Corp. Computer simulation of multi-phase and multi-component fluid flows including physics of under-resolved porous structures

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2222999C3 (de) * 1970-12-23 1975-08-07 Du Pont Verfahren zum Herstellen von mikroporösen, offenzelligen Polymerisaterzeugnissen
JPS5676208A (en) * 1979-11-29 1981-06-23 Mitsubishi Rayon Co Ltd Filtering method for organic liquid
CA1170010A (en) * 1980-03-28 1984-07-03 Donald N. Robinson Porous vinylidene fluoride polymer membrane and process for its preparation
US4434116A (en) * 1981-06-26 1984-02-28 Diamond Shamrock Corporation Method for making a porous fluorinated polymer structure
EP0133882B1 (de) † 1983-07-30 1990-04-04 Akzo Patente GmbH Poren aufweisende Formkörper
JP2512909B2 (ja) † 1986-09-30 1996-07-03 エヌオーケー株式会社 中空糸多孔質膜の製造方法
GB8716618D0 (en) * 1987-07-15 1987-08-19 Unilever Plc Porous material
US4867881A (en) * 1987-09-14 1989-09-19 Minnesota Minning And Manufacturing Company Orientied microporous film
IT1216467B (it) * 1988-02-26 1990-03-08 Separem Spa Membrana semipermeabile per la separazione di fluidi, procedimento per la sua preparazione e uso ditale membrana per microfiltrazione, distillazione, e tessuti speciali.
DE3829766A1 (de) * 1988-09-01 1990-03-22 Akzo Gmbh Verfahren zur herstellung von membranen
JP2541294B2 (ja) * 1988-09-14 1996-10-09 エヌオーケー株式会社 複合膜
DE68914156T2 (de) * 1988-11-10 1994-08-25 Memtec Ltd Extrusion von hohlfasermembranen.
US5022990A (en) * 1989-01-12 1991-06-11 Asahi Kasei Kogyo Kabushiki Kaisha Polyvinylidene fluoride porous membrane and a method for producing the same
DE3923128A1 (de) * 1989-07-13 1991-01-24 Akzo Gmbh Flach- oder kapillarmembran auf der basis eines homogenen gemisches aus polyvinylidenfluorid und eines zweiten, durch chemische umsetzung hydrophilierbaren polymeren
US5013339A (en) * 1989-12-05 1991-05-07 The Dow Chemical Company Compositions useful for making microporous polyvinylidene fluoride membranes, and process

Also Published As

Publication number Publication date
ES2093705T5 (es) 2000-12-01
DE69130879D1 (de) 1999-03-18
EP0527913B1 (en) 1996-10-16
EP0527913A4 (en) 1992-12-15
WO1991017204A1 (en) 1991-11-14
EP0734759A1 (en) 1996-10-02
DE69122754D1 (de) 1996-11-21
DE69130879T2 (de) 1999-07-29
DE69122754T3 (de) 2000-10-19
ES2129245T3 (es) 1999-06-01
JP3442384B2 (ja) 2003-09-02
CA2082511A1 (en) 1991-11-10
EP0527913A1 (en) 1993-02-24
CA2082511C (en) 2002-09-10
DE69122754T2 (de) 1997-02-13
EP0527913B2 (en) 2000-07-05
JPH05506883A (ja) 1993-10-07
EP0734759B1 (en) 1999-02-03

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