ES2095986T3 - Cristalizacion en etapas multiples para la purificacion de productos cristalizables. - Google Patents

Cristalizacion en etapas multiples para la purificacion de productos cristalizables.

Info

Publication number
ES2095986T3
ES2095986T3 ES92111357T ES92111357T ES2095986T3 ES 2095986 T3 ES2095986 T3 ES 2095986T3 ES 92111357 T ES92111357 T ES 92111357T ES 92111357 T ES92111357 T ES 92111357T ES 2095986 T3 ES2095986 T3 ES 2095986T3
Authority
ES
Spain
Prior art keywords
crystallization
purification
multiple stages
transfers
controlling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES92111357T
Other languages
English (en)
Inventor
Kenneth F Griffiths
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Application granted granted Critical
Publication of ES2095986T3 publication Critical patent/ES2095986T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/004—Fractional crystallisation; Fractionating or rectifying columns
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0063—Control or regulation
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/10—Inorganic compounds or compositions
    • C30B29/12—Halides
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Detergent Compositions (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

SE PRESENTAN UN METODO Y UN APARATO PARA LA SUPERPURIFICACION DE SUSTANCIAS CRISTALIZABLES A UN NIVEL DE PUREZA DEL 99,999 POR CIENTO. SE INCLUYE EL CONTROL DEL COEFICIENTE DE REFLUJO A BASE DE CONTROLAR Y/O DETERMINAR LAS TRANSFERENCIAS DE CRISTALES Y DE LICORES MADRE EN LUGARES SELECCIONADOS Y A BASE DE MANTENER UN ESTADO ESTABLE DE LAS TRANSFERENCIAS ENTRE UNA PLURALIDAD DE ETAPAS EN QUE SE LLEVAN A CABO OPERACIONES SIMILARES.
ES92111357T 1988-07-28 1992-07-03 Cristalizacion en etapas multiples para la purificacion de productos cristalizables. Expired - Lifetime ES2095986T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US22530488A 1988-07-28 1988-07-28
CA002072820A CA2072820A1 (en) 1988-07-28 1992-06-30 Multistage recrystallization for superpurifying crystallizable substances
EP92111357A EP0576718B1 (en) 1988-07-28 1992-07-03 Multistage recrystallization for superpurifying crystallizable substances

Publications (1)

Publication Number Publication Date
ES2095986T3 true ES2095986T3 (es) 1997-03-01

Family

ID=27169120

Family Applications (1)

Application Number Title Priority Date Filing Date
ES92111357T Expired - Lifetime ES2095986T3 (es) 1988-07-28 1992-07-03 Cristalizacion en etapas multiples para la purificacion de productos cristalizables.

Country Status (5)

Country Link
EP (1) EP0576718B1 (es)
AT (1) ATE143283T1 (es)
CA (1) CA2072820A1 (es)
DE (1) DE69214134T2 (es)
ES (1) ES2095986T3 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5466266A (en) * 1993-06-17 1995-11-14 Griffiths; Kenneth F. Closed system multistage superpurification recrystallization
CN111498929B (zh) * 2020-04-20 2023-08-22 内蒙古久科康瑞环保科技有限公司 分级结晶系统和分级结晶方法
CN119588001A (zh) * 2025-02-10 2025-03-11 中稀(寿光)资源科技有限公司 一种稀土氯化物清洁化生产系统

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3561225A (en) * 1968-08-26 1971-02-09 Phillips Petroleum Co Apparatus and process for 4-step separation of a crystallizable component of a mixed feedstock
US4885016A (en) * 1988-08-31 1989-12-05 Griffiths Kenneth F Multistage fractional freezing for superpurifying crystallizable substances

Also Published As

Publication number Publication date
ATE143283T1 (de) 1996-10-15
DE69214134D1 (de) 1996-10-31
CA2072820A1 (en) 1993-12-31
EP0576718B1 (en) 1996-09-25
DE69214134T2 (de) 1997-04-30
EP0576718A1 (en) 1994-01-05

Similar Documents

Publication Publication Date Title
DE69330963D1 (de) Herstellung von aluminosilikatzeolithen
FR2582149B1 (fr) Appareil pour la croissance d'un cristal semiconducteur
FI892067A0 (fi) Gabapentinmonohydrat och foerfarande foer framstaellning daerav.
FR2538415B1 (fr) Creuset pour tirer des monocristaux
IT8147789A0 (it) Procedimento per produrre monocristalli purissimi mediante tiraggio da crogiolo secondo czochralski
FR2527650B1 (fr) Procede de production par voie solide d'articles multiples a structure monocristalline
NO177040C (no) Fremgangsmåte og apparat for krystallisering av en uorganisk substans
AU3910189A (en) Process and plant for the crystallization of an inorganic substance and crystals of sodium chloride
FR2553793B1 (fr) Procede de commande d'une machine de tirage de monocristaux
PT86631A (pt) Process for the preparation of a novel crystalline form of potassium clavulanate
ATE112693T1 (de) Mehrstufiges fraktionelles gefrieren zum superreinigen von kristallisierbaren substanzen.
FI102165B (fi) Menetelmä monityydyttymättömien alifaattisten yhdisteiden puhdistamise ksi
DE69400447D1 (de) Tiegel zum Ziehen von Silizium-Einkristallen
DE69214134D1 (de) Mehrstufige Umkristallisation zum Reinigen kristallisierbare Stoffe
FI895842A0 (fi) Menetelmä fruktoosin jatkuvaksi kiteyttämiseksi
RO92794A (ro) Procedeu pentru prepararea unor esteri de acid 2-brom-4-metilimidazol-5-carboxilic
DE3477739D1 (en) High efficiency column crystallizer
FR2595692B1 (fr) Procede pour la production d'acide naphtalenedicarboxylique en meme temps que d'acide trimellitique
FR2636322B1 (fr) Procede de production de fluorure d'uranium-(iv)
MA22587A1 (fr) Procede de preparation des isomeres optiques d'un derive de l'amino-2 naphtyridine
FR2542758B1 (fr) Procede de preparation de l'acide l-glutamique
FR2629476B1 (fr) Procede de preparation d'un lingot cristallin de hgcdte
FR2616788B1 (fr) Procede pour la fabrication d'esters du 1-methyl-10a-methoxy-lu milysergol
FR2636358B1 (fr) Procede pour ameliorer la stabilite a la lumiere des materiaux ligno-cellulosiques
RO92779A2 (ro) Procedeu pentru prepararea unor esteri bisiperidinici

Legal Events

Date Code Title Description
FG2A Definitive protection

Ref document number: 576718

Country of ref document: ES