ES2105682T3 - Procedimiento de fabricacion de capas delgadas que presentan propiedades opticas y propiedades de resistencia a la abrasion. - Google Patents

Procedimiento de fabricacion de capas delgadas que presentan propiedades opticas y propiedades de resistencia a la abrasion.

Info

Publication number
ES2105682T3
ES2105682T3 ES94912579T ES94912579T ES2105682T3 ES 2105682 T3 ES2105682 T3 ES 2105682T3 ES 94912579 T ES94912579 T ES 94912579T ES 94912579 T ES94912579 T ES 94912579T ES 2105682 T3 ES2105682 T3 ES 2105682T3
Authority
ES
Spain
Prior art keywords
properties
thin layers
substrate
abrasion resistance
manufacturing procedure
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94912579T
Other languages
English (en)
Inventor
Herve Floch
Philippe Belleville
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Commissariat à l'Énergie Atomique et Aux Énergies Alternatives
Original Assignee
Commissariat a lEnergie Atomique CEA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Commissariat a lEnergie Atomique CEA filed Critical Commissariat a lEnergie Atomique CEA
Application granted granted Critical
Publication of ES2105682T3 publication Critical patent/ES2105682T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
    • C03C17/007—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character containing a dispersed phase, e.g. particles, fibres or flakes, in a continuous phase
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
    • C03C17/23—Oxides
    • C03C17/25—Oxides by deposition from the liquid phase
    • G02B1/105—
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
    • G02B1/11—Anti-reflection coatings
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
    • G02B1/14—Protective coatings, e.g. hard coatings
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00—Coatings on glass
    • C03C2217/20—Materials for coating a single layer on glass
    • C03C2217/21—Oxides
    • C03C2217/213—SiO2
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00—Coatings on glass
    • C03C2217/40—Coatings comprising at least one inhomogeneous layer
    • C03C2217/425—Coatings comprising at least one inhomogeneous layer consisting of a porous layer
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/10—Deposition methods
    • C03C2218/11—Deposition methods from solutions or suspensions
    • C03C2218/113—Deposition methods from solutions or suspensions by sol-gel processes
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/30—Aspects of methods for coating glass not covered above
    • C03C2218/32—After-treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Composite Materials (AREA)
  • Surface Treatment Of Glass (AREA)
  • Surface Treatment Of Optical Elements (AREA)
  • Coating Of Shaped Articles Made Of Macromolecular Substances (AREA)
  • Laminated Bodies (AREA)

Abstract

LA PRESENTE INVENCION SE REFIERE A UN PROCESO DE FABRICACION DE CAPAS DELGADAS QUE PRESENTAN PROPIEDADES OPTICAS Y PROPIEDADES DE RESISTENCIA A LA ABRASION. EL OBJETIVO DE LA INVENCION ES REALIZAR CAPAS DELGADAS QUE PRESENTAN BUENAS PROPIEDADES DE COMPORTAMIENTO MECANICO, ES DECIR UNA BUENA RESISTENCIA A LA ABRASION Y A UNA ADHESION SATISFACTORIA SOBRE EL SUSTRATO SOBRE EL QUE SE DEPOSITAN. ESTE OBJETIVO ES ALCANZADO MEDIANTE UN PROCESO QUE COMPRENDE AL MENOS UN CICLO COMPUESTO DE LAS ETAPAS QUE CONSISTE EN: APLICAR SOBRE UN SUSTRATO (1) AL MENOS UNA CAPA DE SUELO-GEL ANTIRREFLEJO (39 CONSTITUIDO POR UNA SUSPENSION COLOIDAL DE OXIDO DE SILICIO DISPERSA EN UN ALCOHOL ALIFATICO, DEJAR SECAR ESTA CAPA ANTIRREFLEJO (3), SOMETER AL SUSTRATO (1) RECUBIERTO POR DICHA CAPA (3) DE SILICE COLOIDAL, UN TRATAMIENTO ALCALINO EN MEDIO LIQUIDO O GASEOSO.
ES94912579T 1993-04-05 1994-03-31 Procedimiento de fabricacion de capas delgadas que presentan propiedades opticas y propiedades de resistencia a la abrasion. Expired - Lifetime ES2105682T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9303987A FR2703791B1 (fr) 1993-04-05 1993-04-05 Procédé de fabrication de couches minces présentant des propriétés optiques et des propriétés de résistance à l'abrasion .

Publications (1)

Publication Number Publication Date
ES2105682T3 true ES2105682T3 (es) 1997-10-16

Family

ID=9445750

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94912579T Expired - Lifetime ES2105682T3 (es) 1993-04-05 1994-03-31 Procedimiento de fabricacion de capas delgadas que presentan propiedades opticas y propiedades de resistencia a la abrasion.

Country Status (6)

Country Link
EP (1) EP0693186B1 (es)
JP (1) JP3604387B2 (es)
DE (1) DE69403901T2 (es)
ES (1) ES2105682T3 (es)
FR (1) FR2703791B1 (es)
WO (1) WO1994023315A1 (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3488965B2 (ja) 1996-05-21 2004-01-19 日本山村硝子株式会社 ゾル−ゲル法による独立膜の製造方法
FR2759360B1 (fr) 1997-02-10 1999-03-05 Commissariat Energie Atomique Materiau polymerique inorganique a base d'oxyde de tantale notamment a indice de refraction eleve, mecaniquement resistant a l'abrasion, son procede de fabrication et materiau optique comprenant ce materiau
WO2000010934A1 (en) * 1998-08-18 2000-03-02 Ppg Industries Ohio, Inc. Process for producing durable antireflective surfaces and antireflective articles
US6277203B1 (en) 1998-09-29 2001-08-21 Lam Research Corporation Method and apparatus for cleaning low K dielectric and metal wafer surfaces
CN1102622C (zh) * 1998-10-07 2003-03-05 中国科学院山西煤炭化学研究所 防潮增透二氧化硅涂层及其制法
DE10329806A1 (de) * 2003-04-09 2004-10-21 Silicaglas Ilmenau Gmbh Verfahren und Vorrichtungen zur Herstellung von Kieselglasgranulaten mit definierten Formen der Granalien
US8734906B2 (en) 2003-11-21 2014-05-27 Brismat Inc. Films and method of production thereof
JP5183066B2 (ja) * 2003-11-21 2013-04-17 ブリスマット インコーポレイテッド シリカ膜およびその製造方法
NZ563647A (en) * 2005-05-31 2010-01-29 Xerocoat Inc Control of morphology of silica films
FR2900351B1 (fr) 2006-04-26 2008-06-13 Commissariat Energie Atomique Procede de preparation d'une couche nanoporeuse de nanoparticules et couche ainsi obtenue
FR2967992B1 (fr) 2010-11-26 2015-05-29 Commissariat Energie Atomique Preparation de sols d'oxydes metalliques stables, utiles notamment pour la fabrication de films minces a proprietes optiques et resistants a l'abrasion
FR2968081B1 (fr) 2010-11-26 2015-06-26 Commissariat Energie Atomique Films minces de silices mesoporeuses comme materiaux sensibles dans des capteurs chimiques pour la detection ou le dosage de vapeurs de composes nitres
FR2980847B1 (fr) 2011-09-29 2014-08-29 Commissariat Energie Atomique Utilisation de nanoparticules d'oxydes de metaux de transition comme materiaux sensibles dans les capteurs chimiques pour la detection ou le dosage de vapeurs de molecules cibles.
FR3056578B1 (fr) 2016-09-23 2018-12-07 Commissariat A L'energie Atomique Et Aux Energies Alternatives Procede pour ameliorer la tenue au flux laser d'un composant optique.
CN107555811A (zh) * 2017-09-15 2018-01-09 重庆市中光电显示技术有限公司 一种用于触摸屏的抗刮增透保护玻璃及其制备方法
KR102267504B1 (ko) 2017-12-22 2021-06-21 주식회사 엘지화학 메조포러스 실리카 코팅층을 포함하는 광학 부재의 제조방법 및 이를 이용하여 제조된 광학 부재
FR3117900B1 (fr) 2020-12-23 2024-03-01 Commissariat Energie Atomique Procede de preparation de couches minces, notamment par la technique sol-gel

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4271210A (en) * 1979-10-25 1981-06-02 Westinghouse Electric Corp. Method of forming transmissive, porous metal oxide optical layer of a vitreous substrate
US4929278A (en) * 1988-01-26 1990-05-29 United States Department Of Energy Sol-gel antireflective coating on plastics
US4966812A (en) * 1988-01-26 1990-10-30 The United States Of America As Represented By The Department Of Energy Sol-gel antireflective coating on plastics
FR2680583B1 (fr) * 1991-08-22 1993-10-08 Commissariat A Energie Atomique Materiau presentant des proprietes antireflet, hydrophobes et de resistance a l'abrasion et procede de depot d'une couche antireflet, hydrophobe et resistante a l'abrasion sur un substrat.
FR2681435B1 (fr) * 1991-09-18 1993-11-19 Air Liquide Verre ophtalmique et son procede d'elaboration.

Also Published As

Publication number Publication date
EP0693186B1 (fr) 1997-06-18
FR2703791A1 (fr) 1994-10-14
DE69403901T2 (de) 1998-01-08
EP0693186A1 (fr) 1996-01-24
FR2703791B1 (fr) 1995-05-19
JP3604387B2 (ja) 2004-12-22
JPH08508582A (ja) 1996-09-10
WO1994023315A1 (fr) 1994-10-13
DE69403901D1 (de) 1997-07-24

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