ES2107824T3 - Procedimiento para el secado subcritico de aerogeles. - Google Patents

Procedimiento para el secado subcritico de aerogeles.

Info

Publication number
ES2107824T3
ES2107824T3 ES94916929T ES94916929T ES2107824T3 ES 2107824 T3 ES2107824 T3 ES 2107824T3 ES 94916929 T ES94916929 T ES 94916929T ES 94916929 T ES94916929 T ES 94916929T ES 2107824 T3 ES2107824 T3 ES 2107824T3
Authority
ES
Spain
Prior art keywords
airgels
procedure
subcritical drying
drying
subcritical
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94916929T
Other languages
English (en)
Inventor
Rolf-Michael Jansen
Birgit Kessler
Johann Wonner
Andreas Zimmermann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Application granted granted Critical
Publication of ES2107824T3 publication Critical patent/ES2107824T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/08—Silica
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/0091—Preparation of aerogels, e.g. xerogels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B01J37/036—Precipitation; Co-precipitation to form a gel or a cogel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/34—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation
    • B01J37/341—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation
    • B01J37/344—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation of electromagnetic wave energy
    • B01J37/346—Irradiation by, or application of, electric, magnetic or wave energy, e.g. ultrasonic waves ; Ionic sputtering; Flame or plasma spraying; Particle radiation making use of electric or magnetic fields, wave energy or particle radiation of electromagnetic wave energy of microwave energy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/157—After-treatment of gels
    • C01B33/158—Purification; Drying; Dehydrating
    • C01B33/1585—Dehydration into aerogels
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/16—Preparation of silica xerogels
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S521/00—Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S521/915—Utilizing electrical or wave energy during cell forming process

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Inorganic Chemistry (AREA)
  • Plasma & Fusion (AREA)
  • Optics & Photonics (AREA)
  • Toxicology (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • Silicon Compounds (AREA)
  • Colloid Chemistry (AREA)
  • Developing Agents For Electrophotography (AREA)
  • Drying Of Solid Materials (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Catalysts (AREA)
  • Glass Compositions (AREA)
  • Phenolic Resins Or Amino Resins (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCEDIMIENTO PARA LA ELABORACION DE AEROGELES MEDIANTE SECADO SUB-CRITICO DE HIDROGELES ORGANICOS E INORGANICOS Y LIOGELES PARA LA OBTENCION DE AEROGELES, DONDE SE UTILIZAN PROCESO DE SECADO DIELECTRICO.
ES94916929T 1993-05-18 1994-05-04 Procedimiento para el secado subcritico de aerogeles. Expired - Lifetime ES2107824T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4316540A DE4316540A1 (de) 1993-05-18 1993-05-18 Verfahren zur unterkritischen Trocknung von Aerogelen

Publications (1)

Publication Number Publication Date
ES2107824T3 true ES2107824T3 (es) 1997-12-01

Family

ID=6488333

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94916929T Expired - Lifetime ES2107824T3 (es) 1993-05-18 1994-05-04 Procedimiento para el secado subcritico de aerogeles.

Country Status (12)

Country Link
US (2) US5705535A (es)
EP (1) EP0699104B1 (es)
JP (1) JP3560062B2 (es)
AT (1) ATE156385T1 (es)
BR (1) BR9406533A (es)
CA (1) CA2163237C (es)
DE (2) DE4316540A1 (es)
DK (1) DK0699104T3 (es)
ES (1) ES2107824T3 (es)
FI (1) FI955527A0 (es)
NO (1) NO305386B1 (es)
WO (1) WO1994026406A1 (es)

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DE19502453C1 (de) * 1995-01-27 1996-09-05 Hoechst Ag Verfahren zur Herstellung von modifizierten Si0¶2¶- Aerogelen und deren Verwendung
DE19506141A1 (de) * 1995-02-22 1996-08-29 Hoechst Ag Verwendung von Aerogelen in der Pharmazie, in der Kosmetik und im Pflanzenschutz
DE19533851A1 (de) * 1995-09-13 1997-03-20 Hoechst Ag Organofunktionalisierte Aerogele
DE19534198A1 (de) * 1995-09-15 1997-03-20 Hoechst Ag Verfahren zur Herstellung organofunktionalisierter Aerogele
DE19538333A1 (de) * 1995-10-14 1997-04-17 Basf Ag Verfahren zur unterkritischen Herstellung von Aerogelen
US5680713A (en) * 1996-03-05 1997-10-28 Hoechst Aktiengesellschaft Process for the subcritical drying of aerogels
DE19612628A1 (de) * 1996-03-29 1997-10-02 Hoechst Ag Verfahren zur Herstellung von porösen hydrophilen, hochquellfähigen Hydrogelen
US5877100A (en) * 1996-09-27 1999-03-02 Cabot Corporation Compositions and insulation bodies having low thermal conductivity
DE19648797A1 (de) * 1996-11-26 1998-05-28 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten, dauerhaft hydrophoben Aerogelen
DE19648798C2 (de) * 1996-11-26 1998-11-19 Hoechst Ag Verfahren zur Herstellung von organisch modifizierten Aerogelen durch Oberflächenmodifikation des wäßrigen Gels (ohne vorherigen Lösungsmitteltausch) und anschließender Trocknung
DE19702238A1 (de) * 1997-01-24 1998-08-06 Hoechst Ag Verwendung von Aerogelen zur Körper- und/oder Trittschalldämmung
DE19718740A1 (de) 1997-05-02 1998-11-05 Hoechst Ag Verfahren zur Granulierung von Aerogelen
DE19718741A1 (de) 1997-05-02 1998-11-05 Hoechst Ag Verfahren zur Kompaktierung von Aerogelen
DE19756633A1 (de) 1997-12-19 1999-06-24 Hoechst Ag Verfahren zur unterkritischen Trocknung von Lyogelen zu Aerogelen
US6090861A (en) * 1998-12-28 2000-07-18 General Ideas, Inc. Process for high temperature production of organic aerogels
DE19801004A1 (de) 1998-01-14 1999-07-15 Cabot Corp Verfahren zur Herstellung von im wesentlichen kugelförmigen Lyogelen in wasserunlöslichen Silylierungsmitteln
US6168737B1 (en) * 1998-02-23 2001-01-02 The Regents Of The University Of California Method of casting patterned dielectric structures
DE19810564A1 (de) * 1998-03-11 1999-09-16 Basf Ag Verfahren zur Trocknung und Herstellung von mikroporösen Teilchen sowie eine Vorrichtung zur Trocknung
DE59811774D1 (de) * 1998-06-05 2004-09-09 Cabot Corp Nanoporöse interpenetrierende organisch-anorganische netzwerke
DE19834265A1 (de) * 1998-07-30 2000-02-17 Thomas Gesner Verfahren zur Herstellung von Aerogelen und Anlage zur Herstellung von Aerogelschichten auf Substraten oder aus Aerogelen bestehenden Produkten
US6586501B1 (en) 1999-01-20 2003-07-01 Cabot Corporation Aggregates having attached polymer groups and polymer foams
US6258864B1 (en) 1999-01-20 2001-07-10 Cabot Corporation Polymer foam containing chemically modified carbonaceous filler
US7005181B2 (en) * 2000-04-06 2006-02-28 American Aerogel Corporation Organic, open cell foam materials, their carbonized derivatives, and methods for producing same
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EP1401731A2 (en) * 2000-11-29 2004-03-31 American Aerogel Corporation Insulated barriers and methods for producing same
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US6800608B2 (en) 2001-06-22 2004-10-05 Beckman Coulter, Inc. Homogeneous assay of vancomycin using a stable particle-vancomycin conjugate, a novel rate enhancer, and a novel dose response modulator
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EP1356865A1 (en) * 2002-04-19 2003-10-29 OMG AG & Co. KG Article comprising a cryogel
US20050069464A1 (en) * 2003-09-25 2005-03-31 Obee Timothy N. Photocatalytic oxidation of contaminants through selective desorption of water utilizing microwaves
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EP1870649A1 (en) 2006-06-20 2007-12-26 Octapharma AG Lyophilisation targetting defined residual moisture by limited desorption energy levels
KR101079308B1 (ko) 2008-11-12 2011-11-04 한국세라믹기술원 에어로젤 블랑켓의 제조방법
ITMI20090950A1 (it) * 2009-05-29 2010-11-30 Gegussa Novara Technology Spa Processo per la preparazione di un aerogelo in pellets
FR2981341B1 (fr) 2011-10-14 2018-02-16 Enersens Procede de fabrication de xerogels
CN102765725B (zh) * 2012-08-10 2014-03-05 蓝烟（北京）科技有限公司 一种低成本制备疏水性二氧化硅气凝胶的方法
DE102012019984A1 (de) * 2012-10-11 2014-04-17 Leibniz-Institut für Oberflächenmodifizierung e.V. Verfahren zur Herstellung von porösen Gelen mit inkorporierten katalytisch oder biologisch aktiven Materialien sowie damit hergestellte Gele und deren Verwendung
PT106781A (pt) 2013-02-15 2014-08-18 Inst Superior Tecnico Aerogéis híbridos flexíveis preparados em condições subcríticas e processo de preparação dos mesmos
DE102013108805A1 (de) * 2013-08-14 2015-02-19 Elringklinger Ag Thermoelektrisches Modul sowie Verfahren zum Herstellen eines thermoelektrischen Moduls
FR3018207B1 (fr) 2014-03-07 2016-03-18 Enersens Procede de fabrication d'aerogels par chauffage dielectrique
KR101789371B1 (ko) 2015-02-13 2017-10-23 주식회사 엘지화학 실리카 에어로겔 함유 블랑켓의 제조방법 및 이에 따라 제조된 실리카 에어로겔 함유 블랑켓
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KR101931569B1 (ko) 2015-11-03 2018-12-21 주식회사 엘지화학 소수성의 산화금속-실리카 복합 에어로겔의 제조방법 및 이로부터 제조된 소수성의 산화금속-실리카 복합 에어로겔
KR101800938B1 (ko) * 2015-11-27 2017-11-23 주식회사 엘지화학 소수성의 실리카 에어로겔의 제조방법 및 이로부터 제조된 소수성의 실리카 에어로겔
KR101955307B1 (ko) * 2015-11-27 2019-05-30 주식회사 엘지화학 소수성의 실리카 에어로겔의 제조방법 및 이로부터 제조된 소수성의 실리카 에어로겔
CN108602681B (zh) 2016-09-12 2021-12-17 株式会社Lg化学 二氧化硅气凝胶的制备方法以及由其制备的二氧化硅气凝胶
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Also Published As

Publication number Publication date
CA2163237A1 (en) 1994-11-24
JP3560062B2 (ja) 2004-09-02
EP0699104B1 (de) 1997-08-06
DE4316540A1 (de) 1994-11-24
EP0699104A1 (de) 1996-03-06
FI955527A7 (fi) 1995-11-16
FI955527L (fi) 1995-11-16
NO954537L (no) 1995-11-10
DK0699104T3 (da) 1998-03-09
US5811031A (en) 1998-09-22
NO305386B1 (no) 1999-05-25
BR9406533A (pt) 1996-01-02
NO954537D0 (no) 1995-11-10
ATE156385T1 (de) 1997-08-15
DE59403670D1 (de) 1997-09-11
FI955527A0 (fi) 1995-11-16
JPH08511197A (ja) 1996-11-26
WO1994026406A1 (de) 1994-11-24
CA2163237C (en) 2003-07-08
US5705535A (en) 1998-01-06

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