ES2109223T3 - Reactivo para la determinacion coulombimetrica de agua. - Google Patents
Reactivo para la determinacion coulombimetrica de agua.Info
- Publication number
- ES2109223T3 ES2109223T3 ES90102147T ES90102147T ES2109223T3 ES 2109223 T3 ES2109223 T3 ES 2109223T3 ES 90102147 T ES90102147 T ES 90102147T ES 90102147 T ES90102147 T ES 90102147T ES 2109223 T3 ES2109223 T3 ES 2109223T3
- Authority
- ES
- Spain
- Prior art keywords
- reagent
- water
- coulombimetric
- determination
- alcoholic
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000003153 chemical reaction reagent Substances 0.000 title abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title 1
- 230000001476 alcoholic effect Effects 0.000 abstract 2
- 239000002904 solvent Substances 0.000 abstract 2
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 abstract 1
- XLYOFNOQVPJJNP-PWCQTSIFSA-N Tritiated water Chemical compound [3H]O[3H] XLYOFNOQVPJJNP-PWCQTSIFSA-N 0.000 abstract 1
- MTNDZQHUAFNZQY-UHFFFAOYSA-N imidazoline Chemical compound C1CN=CN1 MTNDZQHUAFNZQY-UHFFFAOYSA-N 0.000 abstract 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000012795 verification Methods 0.000 abstract 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N31/00—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
- G01N31/16—Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using titration
- G01N31/168—Determining water content by using Karl Fischer reagent
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Measuring Or Testing Involving Enzymes Or Micro-Organisms (AREA)
- Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
Abstract
SE TRATA DE UN REACTIVO PARA LA VERIFICACION CULOMBIMETRICA DE AGUA, SITUADO EN UNA CELULA SIN DIAFRAGMA, QUE CONSISTE EN UN DISOLVENTE ALCOHOLICO O MEZCLA DE DISOLVENTES ALCOHOLICOS QUE CONTIENE IMIDAZOL Y/O UN DERIVADO DE IMIDAZOL Y/O DIETANOLAMINA Y/O TRITANOLAMINA Y DIOXIDO DE SULFURO Y UNO O MAS YODUROS Y, EVENTUALMENTE, UNA O MAS SALES CONDUCTORAS.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3904992A DE3904992A1 (de) | 1989-02-18 | 1989-02-18 | Reagenz fuer die coulometrische wasserbestimmung |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2109223T3 true ES2109223T3 (es) | 1998-01-16 |
Family
ID=6374402
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES90102147T Expired - Lifetime ES2109223T3 (es) | 1989-02-18 | 1990-02-03 | Reactivo para la determinacion coulombimetrica de agua. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5139955A (es) |
| EP (1) | EP0384195B1 (es) |
| JP (1) | JP3105900B2 (es) |
| BR (1) | BR9000691A (es) |
| DD (1) | DD292083A5 (es) |
| DE (2) | DE3904992A1 (es) |
| ES (1) | ES2109223T3 (es) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0240554A (ja) * | 1988-07-30 | 1990-02-09 | Bridgestone Corp | 管内走行装置 |
| DE4123976A1 (de) * | 1991-07-19 | 1993-01-21 | Riedel De Haen Ag | Katholyt fuer die coulometrische wasserbestimmung nach karl fischer |
| US5300207A (en) * | 1993-01-14 | 1994-04-05 | Harald Dahms | High current coulometric KF titrator |
| KR100324309B1 (ko) * | 1993-06-16 | 2002-05-13 | 석 영 정 | 운전경보의자동제어방법및제어장치 |
| US5389545A (en) * | 1993-07-26 | 1995-02-14 | Dahms; Harald | Reagents, methods and kits for water determination |
| US5453377A (en) * | 1993-07-26 | 1995-09-26 | Dahms; Harald | Methods for making iodine-free Karl Fischer reagents |
| DE4421453A1 (de) * | 1994-06-18 | 1995-12-21 | Riedel De Haen Ag | Karl-Fischer-Reagenz |
| IL114938A (en) * | 1995-08-15 | 2000-08-13 | State Of Israel Ministry Of In | Reagent for determining water and ene-diols or thiols |
| SE507338C2 (sv) | 1996-12-23 | 1998-05-18 | Anders Cedergren | Förfarande och anordning vid coulometrisk bestämning av vatten medelst Karl Fischerreaktion i en diafragmafri cell |
| DE59813376D1 (de) * | 1998-01-29 | 2006-04-20 | Sigma Aldrich Laborchemikalien | Verwendung eines Salzes als Zusatz in Karl-Fischer Reagenzien zur Stabilisierung der Ethanol-Lösungsmittelkomponente |
| US6707571B1 (en) | 1998-08-28 | 2004-03-16 | Seiko Epson Corporation | Character printing method and device as well as image forming method and device |
| US6544842B1 (en) * | 1999-05-01 | 2003-04-08 | Micron Technology, Inc. | Method of forming hemisphere grained silicon on a template on a semiconductor work object |
| SE9901857D0 (sv) * | 1999-05-21 | 1999-05-21 | Anders Cedergren | Karl Fischer reagent |
| DE10056547A1 (de) * | 2000-11-15 | 2002-05-23 | Sigma Aldrich Laborchemikalien | Karl-Fischer-Reagenz |
| KR20030059842A (ko) * | 2001-12-28 | 2003-07-12 | 대정화금주식회사 | 칼-피셔 전기량 적정용 일액형 시약 |
| KR100648856B1 (ko) * | 2002-06-25 | 2006-11-24 | 대정화금주식회사 | 칼-피셔 전기량 적정용 일액형 시약 |
| KR20040026397A (ko) * | 2002-09-24 | 2004-03-31 | 대정화금주식회사 | 칼-피셔 전기량 적정용 일액형 시약 |
| GB0407908D0 (en) * | 2004-04-07 | 2004-05-12 | Univ York | Ionic liquids |
| WO2006066039A2 (en) * | 2004-12-17 | 2006-06-22 | Kram Brian H | High temperature tissue conditioning with low volatility solutions and applications |
| US20090170152A1 (en) * | 2007-06-01 | 2009-07-02 | Ventana Medical Systems, Inc. | Tissue Conditioning Protocols |
| US20200033307A1 (en) * | 2018-07-25 | 2020-01-30 | Honeywell International Inc. | Method of determining an amount of water in a sample using a derivative of imidazole and a hydrogen halide donor |
| CN109254110A (zh) * | 2018-09-30 | 2019-01-22 | 东莞市杉杉电池材料有限公司 | 一种锂离子电池电解液水分检测用卡尔费休试剂及其制备方法 |
| US11714072B2 (en) * | 2019-03-28 | 2023-08-01 | Honeywell International Inc. | Reagent compositions and method for Karl Fischer titration |
| US11885782B2 (en) * | 2020-10-29 | 2024-01-30 | Honeywell International Inc. | Method of determining an amount of water in a sample using a sulfonic acid |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4378972A (en) * | 1980-03-05 | 1983-04-05 | Riedel-De Haen Aktiengesellschaft | Titration agent and method for using same |
| DE3008421C2 (de) * | 1980-03-05 | 1982-08-26 | Riedel-De Haen Ag, 3016 Seelze | Titrationsmittel und seine Verwendung |
| DE3010436A1 (de) * | 1980-03-19 | 1981-09-24 | Merck Patent Gmbh, 6100 Darmstadt | Pyridinfreies karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
| DE3204962A1 (de) * | 1982-02-12 | 1983-08-25 | Merck Patent Gmbh, 6100 Darmstadt | Karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
| DE3329020A1 (de) * | 1983-08-11 | 1985-02-21 | Riedel-De Haen Ag, 3016 Seelze | Loesemittel fuer die wasserbestimmung nach karl-fischer |
| US4720464A (en) * | 1983-12-28 | 1988-01-19 | Mitsubishi Chemical Industries, Limited | Electrolytes for Karl Fischer coulometric titration |
| DE3407014A1 (de) * | 1984-02-27 | 1985-08-29 | Merck Patent Gmbh, 6100 Darmstadt | Karl-fischer-reagenz und verfahren zur bestimmung von wasser mit hilfe dieses reagenzes |
| US4725552A (en) * | 1984-05-21 | 1988-02-16 | Harald Dahms | Karl Fischer reagent and its use |
| JPH0658340B2 (ja) * | 1985-04-26 | 1994-08-03 | 三菱化成株式会社 | カ−ルフイツシヤ−電量滴定用電解液 |
| DE3723084A1 (de) * | 1987-07-13 | 1989-01-26 | Merck Patent Gmbh | Loesungsmittel fuer die wasserbestimmung nach karl-fischer |
-
1989
- 1989-02-18 DE DE3904992A patent/DE3904992A1/de not_active Ceased
-
1990
- 1990-02-03 ES ES90102147T patent/ES2109223T3/es not_active Expired - Lifetime
- 1990-02-03 EP EP90102147A patent/EP0384195B1/de not_active Expired - Lifetime
- 1990-02-03 DE DE59010754T patent/DE59010754D1/de not_active Expired - Lifetime
- 1990-02-07 US US07/476,180 patent/US5139955A/en not_active Expired - Lifetime
- 1990-02-15 BR BR909000691A patent/BR9000691A/pt not_active IP Right Cessation
- 1990-02-16 DD DD90337915A patent/DD292083A5/de not_active IP Right Cessation
- 1990-02-16 JP JP02034033A patent/JP3105900B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE59010754D1 (de) | 1997-09-25 |
| US5139955A (en) | 1992-08-18 |
| EP0384195B1 (de) | 1997-08-20 |
| EP0384195A2 (de) | 1990-08-29 |
| EP0384195A3 (de) | 1993-08-18 |
| BR9000691A (pt) | 1991-01-22 |
| DD292083A5 (de) | 1991-07-18 |
| JPH0315751A (ja) | 1991-01-24 |
| DE3904992A1 (de) | 1990-08-23 |
| JP3105900B2 (ja) | 2000-11-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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