ES2117395T3 - Recuperacion de catalizadores usados. - Google Patents
Recuperacion de catalizadores usados.Info
- Publication number
- ES2117395T3 ES2117395T3 ES95905375T ES95905375T ES2117395T3 ES 2117395 T3 ES2117395 T3 ES 2117395T3 ES 95905375 T ES95905375 T ES 95905375T ES 95905375 T ES95905375 T ES 95905375T ES 2117395 T3 ES2117395 T3 ES 2117395T3
- Authority
- ES
- Spain
- Prior art keywords
- sub
- tantalo
- salt
- suitable substitute
- recovery
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000003054 catalyst Substances 0.000 title abstract 3
- 238000011084 recovery Methods 0.000 title 1
- 238000000034 method Methods 0.000 abstract 3
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 abstract 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 1
- -1 K {SUB Chemical class 0.000 abstract 1
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 229960002050 hydrofluoric acid Drugs 0.000 abstract 1
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical class [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000002699 waste material Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/20—Obtaining niobium, tantalum or vanadium
- C22B34/24—Obtaining niobium or tantalum
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/28—Regeneration or reactivation
- B01J27/32—Regeneration or reactivation of catalysts comprising compounds of halogens
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J38/00—Regeneration or reactivation of catalysts, in general
- B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
- B01J38/60—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using acids
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G33/00—Compounds of niobium
- C01G33/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G33/00—Compounds of niobium
- C01G33/006—Compounds containing niobium, with or without oxygen or hydrogen, and containing two or more other elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G35/00—Compounds of tantalum
- C01G35/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G35/00—Compounds of tantalum
- C01G35/006—Compounds containing tantalum, with or without oxygen or hydrogen, and containing two or more other elements
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B4/00—Electrothermal treatment of ores or metallurgical products for obtaining metals or alloys
- C22B4/005—Electrothermal treatment of ores or metallurgical products for obtaining metals or alloys using plasma jets
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
- C01P2006/82—Compositional purity water content
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Manufacturing & Machinery (AREA)
- Plasma & Fusion (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- Physics & Mathematics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Catalysts (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
SE PRESENTA UN PROCESO PARA CONVERTIR UN CATALIZADOR AGOTADO DE PROCESOS DE FLUORACION CONVENCIONALES DE UNA SAL DE TANTALO O NIOBIO COMERCIALMENTE UTIL TAL COMO K{SUB, 2}TAF{SUB, 7} O K{SUB, 2}NBF{SUB, 7}. EL PROCESO SE REFIERE AMPLIAMENTE A LA DISOLUCION DEL CATALIZADOR AGOTADO EN AGUA O EN UNA SOLUCION ACUOSA DE ACIDO FLUORHIDRICO, A LA SEPARACION Y ELIMINACION DEL RESIDUO NO DISUELTO, A LA EXTRACCION DE LA SOLUCION ACUOSA CON UN SOLVENTE ADECUADO TAL COMO CETONA DE ISOBUTILO DE METILO (MIBK), Y A LA OBTENCION DE PRODUCTOS DE TANTALO UTILES A PARTIR DE LA SOLUCION DE CIBH TALES COMO UNA SAL DE TANTALO.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/166,495 US5620936A (en) | 1993-12-14 | 1993-12-14 | Recovery of spent catalyst |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2117395T3 true ES2117395T3 (es) | 1998-08-01 |
Family
ID=22603556
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES95905375T Expired - Lifetime ES2117395T3 (es) | 1993-12-14 | 1994-12-13 | Recuperacion de catalizadores usados. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5620936A (es) |
| EP (1) | EP0734355B1 (es) |
| JP (1) | JP3527509B2 (es) |
| AU (1) | AU1401395A (es) |
| DE (1) | DE69408869T2 (es) |
| ES (1) | ES2117395T3 (es) |
| WO (1) | WO1995016636A1 (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4118527B2 (ja) * | 2001-04-06 | 2008-07-16 | 三井金属鉱業株式会社 | 高純度フッ化タンタル酸カリウム結晶又は高純度フッ化ニオブ酸カリウム結晶の製造方法及びそれらの製造方法で用いる再結晶槽並びにそれらの製造方法で得られたフッ化タンタル酸カリウム結晶又は高純度フッ化ニオブ酸カリウム結晶 |
| WO2003072504A1 (fr) * | 2002-02-27 | 2003-09-04 | Stella Chemifa Kabushiki Kaisha | Procede de purification servant a produire un compose de niobium et/ou de tantale de grande purete |
| BR0307880A (pt) * | 2002-02-27 | 2004-12-28 | Stella Chemifa Kabuskiki Kaish | Método para purificar um composto de nióbio e/ou um composto de tântalo altamente puro |
| EP2776383B1 (en) | 2011-11-10 | 2020-03-11 | The Chemours Company FC, LLC | Catalytic fluorination process of making hydrohaloalkane |
| EP4303331A1 (en) * | 2022-07-08 | 2024-01-10 | Commissariat à l'Energie Atomique et aux Energies Alternatives | Process for extracting tantalum and niobium from an aqueous acidic solution |
| DE102023211423A1 (de) | 2023-11-16 | 2025-05-22 | Walter Bludssus | Ökonomisches, doppeltes, Aufschlussverfahren für Ta/Nb-haltige Rohstoffe unter Recyclierung der verwendeten Flusssäure |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3107976A (en) * | 1957-11-29 | 1963-10-22 | Ernest L Koerner | Niobium-tantalum separation |
| US2962372A (en) * | 1958-01-17 | 1960-11-29 | Union Carbide Corp | Columbium and tantalum separation |
| US3117833A (en) * | 1958-09-25 | 1964-01-14 | Fansteel Metallurgical Corp | Process of purifying and separating columbium and tantalum values from each other |
| US3065046A (en) * | 1959-04-06 | 1962-11-20 | Nat Distillers Chem Corp | Process for recovering tantalum and niobium values from organic solutions |
| US3112991A (en) * | 1960-03-28 | 1963-12-03 | Union Carbide Corp | Process for recovery of fluoride-free columbium and tantalum pentoxides from organic extracts |
| US3712939A (en) * | 1971-03-29 | 1973-01-23 | Union Carbide Corp | Method for recovering tantalum and/or columbium |
| US3830871A (en) * | 1973-07-02 | 1974-08-20 | Exxon Research Engineering Co | Removal of a metal pentafluoride from hydrocarbons |
| DE2435427A1 (de) * | 1974-07-23 | 1976-02-05 | Starck Hermann C Fa | Verfahren zur verarbeitung von tantalniob-haltigen schlacken und rueckstaenden |
| DK449074A (da) * | 1974-08-22 | 1976-02-23 | Atomenergikommissionen | Fremgangsmade til udvinding af tantal og/eller niob i fri eller bunden form fra tantal- og niobholdige oplosninger |
| US4065405A (en) * | 1976-12-03 | 1977-12-27 | Exxon Research And Engineering Company | Recovery of tantalum and/or niobium pentafluorides from a hydrocarbon conversion catalyst |
| US4258225A (en) * | 1977-08-15 | 1981-03-24 | E. I. Du Pont De Nemours And Company | TaF5 and NbF5 as fluorination catalysts |
| AT370153B (de) * | 1981-03-09 | 1983-03-10 | Plasser Bahnbaumasch Franz | Gleisstopfaggregat |
| US4451438A (en) * | 1982-03-26 | 1984-05-29 | Herman C. Starck Berlin | Process for recovering niobium and/or tantalum metal compounds from such ores further containing complexes of uranium, thorium, titanium and/or rare earth metals |
| US4663130A (en) * | 1983-11-14 | 1987-05-05 | Cabot Corporation | Process for dissolving tantalum/columbium materials containing alkali metal impurities |
| JPS61146717A (ja) * | 1984-12-18 | 1986-07-04 | Sumitomo Chem Co Ltd | タンタルの精製方法 |
| US4967024A (en) * | 1988-06-23 | 1990-10-30 | E. I. Du Pont De Nemours And Company | Catalyzed hydrofluorination process |
| FR2636939B1 (fr) * | 1988-09-06 | 1991-08-30 | Inst Nat Rech Chimique | Procede perfectionne d'obtention de composes de ta et (ou) nb exempts d'impuretes a partir de materiaux contenant ces metaux |
| DE4021207A1 (de) * | 1990-07-03 | 1992-01-16 | Starck Hermann C Fa | Verfahren zur gewinnung und trennung von tantal und niob |
| US5437848A (en) * | 1992-07-10 | 1995-08-01 | Cabot Corporation | Recovery of metal values from process residues |
-
1993
- 1993-12-14 US US08/166,495 patent/US5620936A/en not_active Expired - Lifetime
-
1994
- 1994-12-13 AU AU14013/95A patent/AU1401395A/en not_active Abandoned
- 1994-12-13 EP EP95905375A patent/EP0734355B1/en not_active Expired - Lifetime
- 1994-12-13 ES ES95905375T patent/ES2117395T3/es not_active Expired - Lifetime
- 1994-12-13 WO PCT/US1994/014369 patent/WO1995016636A1/en not_active Ceased
- 1994-12-13 JP JP51692395A patent/JP3527509B2/ja not_active Expired - Fee Related
- 1994-12-13 DE DE69408869T patent/DE69408869T2/de not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0734355A1 (en) | 1996-10-02 |
| DE69408869T2 (de) | 1998-10-08 |
| EP0734355B1 (en) | 1998-03-04 |
| JP3527509B2 (ja) | 2004-05-17 |
| AU1401395A (en) | 1995-07-03 |
| DE69408869D1 (de) | 1998-04-09 |
| JPH09507466A (ja) | 1997-07-29 |
| HK1015135A1 (en) | 1999-10-08 |
| US5620936A (en) | 1997-04-15 |
| WO1995016636A1 (en) | 1995-06-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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