ES2128256B1 - Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano. - Google Patents

Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano.

Info

Publication number
ES2128256B1
ES2128256B1 ES9700910A ES9700910A ES2128256B1 ES 2128256 B1 ES2128256 B1 ES 2128256B1 ES 9700910 A ES9700910 A ES 9700910A ES 9700910 A ES9700910 A ES 9700910A ES 2128256 B1 ES2128256 B1 ES 2128256B1
Authority
ES
Spain
Prior art keywords
synthesis
trifluorpropen
pentafluorpropane
fluoration
chlorine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES9700910A
Other languages
English (en)
Other versions
ES2128256A1 (es
Inventor
Andre Lantz
Laurent Wendlinger
Benoit Requieme
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Elf Atochem SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Elf Atochem SA filed Critical Elf Atochem SA
Publication of ES2128256A1 publication Critical patent/ES2128256A1/es
Application granted granted Critical
Publication of ES2128256B1 publication Critical patent/ES2128256B1/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00Acyclic saturated compounds containing halogen atoms
    • C07C19/08Acyclic saturated compounds containing halogen atoms containing fluorine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/202Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
    • C07C17/206Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/20Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
    • C07C17/21Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms with simultaneous increase of the number of halogen atoms

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Síntesis de 1-cloro-3,3,3-triflúorpropeno y su fluoración en 1,1,1,3,3-pentaflúorpropano con ácido fluorhídrico anhidro. La reacción se realiza en dos etapas: la primera en fase gaseosa que proporciona esencialmente el 1-cloro-3,3,3-triflúorpropeno y la segunda en fase líquida que permite transformar el 1-cloro-3,3,3-triflúorpropeno en 1,1,1,3,3-pentafluorpropano.
ES9700910A 1996-05-13 1997-04-28 Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano. Expired - Lifetime ES2128256B1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9605908A FR2748473B1 (fr) 1996-05-13 1996-05-13 Synthese du 1-chloro-3,3,3 trifluoropropene et sa fluoration en 1,1,1,3,3 pentafluoropropane

Publications (2)

Publication Number Publication Date
ES2128256A1 ES2128256A1 (es) 1999-05-01
ES2128256B1 true ES2128256B1 (es) 2000-01-16

Family

ID=9492063

Family Applications (1)

Application Number Title Priority Date Filing Date
ES9700910A Expired - Lifetime ES2128256B1 (es) 1996-05-13 1997-04-28 Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano.

Country Status (7)

Country Link
JP (1) JPH1087523A (es)
CN (1) CN1166479A (es)
CA (1) CA2203433A1 (es)
DE (1) DE19716337A1 (es)
ES (1) ES2128256B1 (es)
FR (1) FR2748473B1 (es)
GB (1) GB2313118A (es)

Families Citing this family (36)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5710352A (en) * 1996-09-19 1998-01-20 Alliedsignal Inc. Vapor phase process for making 1,1,1,3,3-pentafluoropropane and 1-chloro-3,3,3-trifluoropropene
US5777184A (en) * 1997-06-25 1998-07-07 Alliedsignal Inc. Preparation of fluoroalkyl compounds and their derivatives
BE1011765A3 (fr) * 1998-02-26 2000-01-11 Solvay Procede d'hydrofluoration d'hydrocarbures.
JP3154702B2 (ja) 1998-02-26 2001-04-09 セントラル硝子株式会社 1,1,1,3,3−ペンタフルオロプロパンの製造方法
DE69909860T2 (de) * 1998-02-26 2004-05-27 Central Glass Co., Ltd., Ube Verfahren zur Herstellung von fluorierten Propanen
DE69919536T2 (de) * 1998-06-02 2005-09-01 E.I. Du Pont De Nemours And Co., Wilmington Verfahren zur herstellung von hexafluorpropen und gegebenenfalls weiteren halogenierten fluor enthaltenden kohlenwasserstoffen
CN1225441C (zh) 1998-06-02 2005-11-02 纳幕尔杜邦公司 从CClF2CClFCF3和CClF2CClFCF3同HF共沸物制备六氟丙烯的方法
EP1132365B1 (en) * 1998-11-13 2007-11-07 Daikin Industries, Ltd. Azeotropic composition comprising 1,1,1,3,3-pentafluoropropane and 1,1,1-trifluoro-3-chloro-2-propene, method of separation and purification of the same, and process for producing 1,1,1,3,3-pentafluoropropane and 1,1,1-trifluoro-3-chloro-2-propene
AU6359400A (en) * 1999-07-21 2001-02-13 Halocarbon Products Corporation Production of aliphatic fluorocarbons
EP1153906B1 (en) * 2000-05-08 2003-05-21 Atofina Chemicals, Inc. Preparation of 245fa
ATE556124T1 (de) * 2002-10-25 2012-05-15 Honeywell Int Inc Fluorsubstituierte olefine enthaltendezusammensetzungen
US6844475B1 (en) * 2003-08-08 2005-01-18 Honeywell International Business Machines Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd)
US9499729B2 (en) * 2006-06-26 2016-11-22 Honeywell International Inc. Compositions and methods containing fluorine substituted olefins
CN110003859A (zh) * 2005-03-04 2019-07-12 科慕埃弗西有限公司 包含氟代烯烃的组合物
TWI482748B (zh) * 2005-06-24 2015-05-01 Honeywell Int Inc 含有經氟取代之烯烴之組合物
PL3336074T3 (pl) 2006-01-03 2025-10-20 Honeywell International Inc. Sposób produkcji fluorowanych związków organicznych
WO2007079435A2 (en) * 2006-01-03 2007-07-12 Honeywell International Inc. Method for producing fluorinated organic compounds
ES2607226T3 (es) * 2007-03-29 2017-03-29 Arkema Inc. Espuma de células cerradas y procedimiento
US8071826B2 (en) * 2008-04-04 2011-12-06 Honeywell International Inc. Process for the preparation of 2,3,3,3-tetrafluoropropene (HFO-1234yf)
US9340758B2 (en) 2008-05-12 2016-05-17 Arkema Inc. Compositions of hydrochlorofluoroolefins
TR201906881T4 (tr) * 2008-05-12 2019-05-21 Arkema Inc Hidroklorofluoroolefinlerin bileşimleri.
US8293954B2 (en) * 2010-03-10 2012-10-23 Honeywell International Inc. Catalyst life improvement for the vapor phase manufacture of 1-chloro-3,3,3-trifluoropropene
US8426656B2 (en) * 2010-04-05 2013-04-23 Honeywell International Inc. Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene and trans-1,3,3,3-tetrafluoropropene
CN101913983B (zh) * 2010-09-07 2013-04-17 西安近代化学研究所 1,1,1,3,3-五氟丙烷的制备方法
CN105367377B (zh) * 2010-10-22 2018-10-30 阿克马法国公司 通过五氯丙烷的气相氟化制造2-氯-3,3,3-三氟丙烯的方法
US8648221B2 (en) * 2011-01-19 2014-02-11 Honeywell International Inc. Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene, trans-1,3,3,3-tetrafluoropropene, and 1,1,1,3,3-pentafluoropropane
US8436217B2 (en) 2011-04-25 2013-05-07 Honeywell International Inc. Integrated process to co-produce 1,1,1,3,3-pentafluoropropane, trans-1-chloro-3,3,3-trifluoropropene and trans-1,3,3,3-tetrafluoropropene
US9000240B2 (en) * 2011-05-19 2015-04-07 Honeywell International Inc. Integrated process for the production of 1-chloro-3,3,3-trifluoropropene
US8664456B2 (en) 2012-03-28 2014-03-04 Honeywell International Inc. Integrated process for the co-production of trans-1-chloro-3,3,3-trifluoropropene, trans-1,3,3,3-tetrafluoropropene, and 1,1,1,3,3-pentafluoropropane
CN104058928B (zh) * 2014-06-19 2017-11-21 巨化集团技术中心 一种含溴氟代烷烃合成中提高装置生产能力的方法
JP6274314B2 (ja) 2014-07-15 2018-02-07 セントラル硝子株式会社 トランス−1−クロロ−3,3,3−トリフルオロプロペンの製造方法
FR3027304B1 (fr) 2014-10-16 2018-02-23 Arkema France Compositions a base de 1,1,1,3,3-pentachloropropane
US20160332935A1 (en) * 2015-05-12 2016-11-17 Honeywell International Inc. Integrated Process for Making HCFO-1233zd and HFC-245fa
CN112239704B (zh) * 2015-09-04 2022-04-01 Agc株式会社 溶剂组合物、清洗方法和涂膜的形成方法
JP6826280B2 (ja) 2016-01-15 2021-02-03 セントラル硝子株式会社 トランス−1−クロロ−3,3,3−トリフルオロプロペンの製造方法
CN115850020B (zh) * 2022-11-16 2025-06-10 江西中欣埃克盛新材料有限公司 连续联产制备HFO1234ze、HCFO1233zd(E、Z)的方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1252182B (es) * 1962-01-13 1967-10-19
JP3369604B2 (ja) * 1992-09-04 2003-01-20 ダイキン工業株式会社 1,1,1,2,3,3−ヘキサフルオロプロパンの製造方法及びテトラフルオロクロロプロペンの製造方法
ES2104521T3 (es) * 1994-07-11 1999-05-01 Allied Signal Inc Proceso para la fabricacion de 1,1,1,3,3-pentafluoropropano.
US5414165A (en) * 1994-07-29 1995-05-09 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,1,1,3,3,3,-hexafluoropropane
FR2724928B1 (fr) * 1994-09-26 1996-10-31 Atochem Elf Sa Synthese de 1,1,1,3,3-pentafluoropropane
US5616819A (en) * 1995-08-28 1997-04-01 Laroche Industries Inc. Process for preparing fluorinated aliphatic compounds
FR2740132B1 (fr) * 1995-10-23 1997-12-19 Solvay Procede pour la preparation de 1,1,1,3,3-pentafluoropropane

Also Published As

Publication number Publication date
CA2203433A1 (fr) 1997-11-13
ES2128256A1 (es) 1999-05-01
DE19716337A1 (de) 1997-11-20
CN1166479A (zh) 1997-12-03
FR2748473A1 (fr) 1997-11-14
JPH1087523A (ja) 1998-04-07
FR2748473B1 (fr) 1998-07-24
GB2313118A (en) 1997-11-19
GB9709202D0 (en) 1997-06-25

Similar Documents

Publication Publication Date Title
ES2128256A1 (es) Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano.
ES2074328T3 (es) Procedimiento para la preparacion de 1-cloro-1,1,3,3,3-pentafluoropropano y 1,1,1,3,3,3-hexafluoropropano.
DK0770048T3 (da) Fremgangsmåde til fremstilling af 1,1,1,3,3-pentafluorpropan
BRPI0010891A (pt) geração de microespuma terapêutica.
AR248158A1 (es) Composicion casi-azeotropica para uso como refrigerante y procedimiento para producir refrigeracion mediante su empleo.
ES2152990T3 (es) Principios activos y microparticulas que contienen gases.
DK0799209T3 (da) Sulfonamider
ES2167908T3 (es) Procedimiento para la preparacion de hidrofluorocarbonos.
BR9805691A (pt) Utilização de um solvente polifluorado volátil, como agente acelerador de secagem, em produtos cosméticos.
ES2160716T3 (es) Procedimiento para estabilizar la respuesta de un biosensor.
ES2124373T3 (es) Procedimiento para la preparacion de derivados del acido n-acil-n,n',n'-etilendiamintriacetico.
BRPI0216109B8 (pt) dispositivo expansível para uso em um ambiente de furo de poço, método de expansão de uma tubulação, e dispositivo tubular para uso em um furo de poço
EP0738142A4 (en) Perfluorocarbons as an anti-inflammatory agent
DK0711140T3 (da) Antimykotisk opløsning til negle
DK0869965T3 (da) Steroidnitritesterderivater anvendelige som antiinflammatoriske lægemidler
ES2164361T3 (es) Separacion de fluoruro de hidrogeno a partir de una mezcla azeotropica fluorocarbono/fluoruro de hidrogeno por acido sulfurico.
MX172711B (es) Procedimiento para la fabricacion de cloro-1-difluor-1,1 etano
NO901535L (no) Molekylaersikter og anvendelse derav som oksydasjonskatalysator.
ES2044382T3 (es) Procedimiento para la fabricacion de 1, 1, 1, 3, 3, 3,-hexafluoropropano y 2-cloro- 1, 1, 1, 3, 3, 3-hexafluoropropano.
DK0449099T3 (da) Hidtil ukendt retinoid heraf og anvendelser heraf til lægemidler
ES2167419T3 (es) Procedimiento de fabricacion de un epoxido.
DE60227006D1 (de) Flüssigphasenverfahren zur herstellung von hcfc-123
ID27774A (id) Turunan-turunan imidazol dengan substitusi bifenilsulfonil, metoda pembuatannya dan penggunaannya sebagai obat atau zat diagnostik
ATE316520T1 (de) Herstellung von fluorkohlenwasserstoffen
ES2194994T3 (es) Procedimiento para la obtencion de caprolactama.

Legal Events

Date Code Title Description
EC2A Search report published

Date of ref document: 19990501

Kind code of ref document: A1

Effective date: 19990501

FA2A Application withdrawn

Effective date: 20001025