ES2128256B1 - Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano. - Google Patents
Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano.Info
- Publication number
- ES2128256B1 ES2128256B1 ES9700910A ES9700910A ES2128256B1 ES 2128256 B1 ES2128256 B1 ES 2128256B1 ES 9700910 A ES9700910 A ES 9700910A ES 9700910 A ES9700910 A ES 9700910A ES 2128256 B1 ES2128256 B1 ES 2128256B1
- Authority
- ES
- Spain
- Prior art keywords
- synthesis
- trifluorpropen
- pentafluorpropane
- fluoration
- chlorine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- MSSNHSVIGIHOJA-UHFFFAOYSA-N pentafluoropropane Chemical compound FC(F)CC(F)(F)F MSSNHSVIGIHOJA-UHFFFAOYSA-N 0.000 title abstract 3
- 230000015572 biosynthetic process Effects 0.000 title abstract 2
- 238000003786 synthesis reaction Methods 0.000 title abstract 2
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 abstract 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000003682 fluorination reaction Methods 0.000 abstract 1
- 239000007791 liquid phase Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
- 230000009466 transformation Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/21—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms with simultaneous increase of the number of halogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Síntesis de 1-cloro-3,3,3-triflúorpropeno y su fluoración en 1,1,1,3,3-pentaflúorpropano con ácido fluorhídrico anhidro. La reacción se realiza en dos etapas: la primera en fase gaseosa que proporciona esencialmente el 1-cloro-3,3,3-triflúorpropeno y la segunda en fase líquida que permite transformar el 1-cloro-3,3,3-triflúorpropeno en 1,1,1,3,3-pentafluorpropano.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9605908A FR2748473B1 (fr) | 1996-05-13 | 1996-05-13 | Synthese du 1-chloro-3,3,3 trifluoropropene et sa fluoration en 1,1,1,3,3 pentafluoropropane |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2128256A1 ES2128256A1 (es) | 1999-05-01 |
| ES2128256B1 true ES2128256B1 (es) | 2000-01-16 |
Family
ID=9492063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES9700910A Expired - Lifetime ES2128256B1 (es) | 1996-05-13 | 1997-04-28 | Sintesis del 1-cloro-3,3,3-trifluorpropeno y su fluoracion en 1,1,1,3,3-pentafluorpropano. |
Country Status (7)
| Country | Link |
|---|---|
| JP (1) | JPH1087523A (es) |
| CN (1) | CN1166479A (es) |
| CA (1) | CA2203433A1 (es) |
| DE (1) | DE19716337A1 (es) |
| ES (1) | ES2128256B1 (es) |
| FR (1) | FR2748473B1 (es) |
| GB (1) | GB2313118A (es) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5710352A (en) * | 1996-09-19 | 1998-01-20 | Alliedsignal Inc. | Vapor phase process for making 1,1,1,3,3-pentafluoropropane and 1-chloro-3,3,3-trifluoropropene |
| US5777184A (en) * | 1997-06-25 | 1998-07-07 | Alliedsignal Inc. | Preparation of fluoroalkyl compounds and their derivatives |
| BE1011765A3 (fr) * | 1998-02-26 | 2000-01-11 | Solvay | Procede d'hydrofluoration d'hydrocarbures. |
| JP3154702B2 (ja) | 1998-02-26 | 2001-04-09 | セントラル硝子株式会社 | 1,1,1,3,3−ペンタフルオロプロパンの製造方法 |
| DE69909860T2 (de) * | 1998-02-26 | 2004-05-27 | Central Glass Co., Ltd., Ube | Verfahren zur Herstellung von fluorierten Propanen |
| DE69919536T2 (de) * | 1998-06-02 | 2005-09-01 | E.I. Du Pont De Nemours And Co., Wilmington | Verfahren zur herstellung von hexafluorpropen und gegebenenfalls weiteren halogenierten fluor enthaltenden kohlenwasserstoffen |
| CN1225441C (zh) | 1998-06-02 | 2005-11-02 | 纳幕尔杜邦公司 | 从CClF2CClFCF3和CClF2CClFCF3同HF共沸物制备六氟丙烯的方法 |
| EP1132365B1 (en) * | 1998-11-13 | 2007-11-07 | Daikin Industries, Ltd. | Azeotropic composition comprising 1,1,1,3,3-pentafluoropropane and 1,1,1-trifluoro-3-chloro-2-propene, method of separation and purification of the same, and process for producing 1,1,1,3,3-pentafluoropropane and 1,1,1-trifluoro-3-chloro-2-propene |
| AU6359400A (en) * | 1999-07-21 | 2001-02-13 | Halocarbon Products Corporation | Production of aliphatic fluorocarbons |
| EP1153906B1 (en) * | 2000-05-08 | 2003-05-21 | Atofina Chemicals, Inc. | Preparation of 245fa |
| ATE556124T1 (de) * | 2002-10-25 | 2012-05-15 | Honeywell Int Inc | Fluorsubstituierte olefine enthaltendezusammensetzungen |
| US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
| US9499729B2 (en) * | 2006-06-26 | 2016-11-22 | Honeywell International Inc. | Compositions and methods containing fluorine substituted olefins |
| CN110003859A (zh) * | 2005-03-04 | 2019-07-12 | 科慕埃弗西有限公司 | 包含氟代烯烃的组合物 |
| TWI482748B (zh) * | 2005-06-24 | 2015-05-01 | Honeywell Int Inc | 含有經氟取代之烯烴之組合物 |
| PL3336074T3 (pl) | 2006-01-03 | 2025-10-20 | Honeywell International Inc. | Sposób produkcji fluorowanych związków organicznych |
| WO2007079435A2 (en) * | 2006-01-03 | 2007-07-12 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
| ES2607226T3 (es) * | 2007-03-29 | 2017-03-29 | Arkema Inc. | Espuma de células cerradas y procedimiento |
| US8071826B2 (en) * | 2008-04-04 | 2011-12-06 | Honeywell International Inc. | Process for the preparation of 2,3,3,3-tetrafluoropropene (HFO-1234yf) |
| US9340758B2 (en) | 2008-05-12 | 2016-05-17 | Arkema Inc. | Compositions of hydrochlorofluoroolefins |
| TR201906881T4 (tr) * | 2008-05-12 | 2019-05-21 | Arkema Inc | Hidroklorofluoroolefinlerin bileşimleri. |
| US8293954B2 (en) * | 2010-03-10 | 2012-10-23 | Honeywell International Inc. | Catalyst life improvement for the vapor phase manufacture of 1-chloro-3,3,3-trifluoropropene |
| US8426656B2 (en) * | 2010-04-05 | 2013-04-23 | Honeywell International Inc. | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene and trans-1,3,3,3-tetrafluoropropene |
| CN101913983B (zh) * | 2010-09-07 | 2013-04-17 | 西安近代化学研究所 | 1,1,1,3,3-五氟丙烷的制备方法 |
| CN105367377B (zh) * | 2010-10-22 | 2018-10-30 | 阿克马法国公司 | 通过五氯丙烷的气相氟化制造2-氯-3,3,3-三氟丙烯的方法 |
| US8648221B2 (en) * | 2011-01-19 | 2014-02-11 | Honeywell International Inc. | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene, trans-1,3,3,3-tetrafluoropropene, and 1,1,1,3,3-pentafluoropropane |
| US8436217B2 (en) | 2011-04-25 | 2013-05-07 | Honeywell International Inc. | Integrated process to co-produce 1,1,1,3,3-pentafluoropropane, trans-1-chloro-3,3,3-trifluoropropene and trans-1,3,3,3-tetrafluoropropene |
| US9000240B2 (en) * | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
| US8664456B2 (en) | 2012-03-28 | 2014-03-04 | Honeywell International Inc. | Integrated process for the co-production of trans-1-chloro-3,3,3-trifluoropropene, trans-1,3,3,3-tetrafluoropropene, and 1,1,1,3,3-pentafluoropropane |
| CN104058928B (zh) * | 2014-06-19 | 2017-11-21 | 巨化集团技术中心 | 一种含溴氟代烷烃合成中提高装置生产能力的方法 |
| JP6274314B2 (ja) | 2014-07-15 | 2018-02-07 | セントラル硝子株式会社 | トランス−1−クロロ−3,3,3−トリフルオロプロペンの製造方法 |
| FR3027304B1 (fr) | 2014-10-16 | 2018-02-23 | Arkema France | Compositions a base de 1,1,1,3,3-pentachloropropane |
| US20160332935A1 (en) * | 2015-05-12 | 2016-11-17 | Honeywell International Inc. | Integrated Process for Making HCFO-1233zd and HFC-245fa |
| CN112239704B (zh) * | 2015-09-04 | 2022-04-01 | Agc株式会社 | 溶剂组合物、清洗方法和涂膜的形成方法 |
| JP6826280B2 (ja) | 2016-01-15 | 2021-02-03 | セントラル硝子株式会社 | トランス−1−クロロ−3,3,3−トリフルオロプロペンの製造方法 |
| CN115850020B (zh) * | 2022-11-16 | 2025-06-10 | 江西中欣埃克盛新材料有限公司 | 连续联产制备HFO1234ze、HCFO1233zd(E、Z)的方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1252182B (es) * | 1962-01-13 | 1967-10-19 | ||
| JP3369604B2 (ja) * | 1992-09-04 | 2003-01-20 | ダイキン工業株式会社 | 1,1,1,2,3,3−ヘキサフルオロプロパンの製造方法及びテトラフルオロクロロプロペンの製造方法 |
| ES2104521T3 (es) * | 1994-07-11 | 1999-05-01 | Allied Signal Inc | Proceso para la fabricacion de 1,1,1,3,3-pentafluoropropano. |
| US5414165A (en) * | 1994-07-29 | 1995-05-09 | E. I. Du Pont De Nemours And Company | Process for the manufacture of 1,1,1,3,3,3,-hexafluoropropane |
| FR2724928B1 (fr) * | 1994-09-26 | 1996-10-31 | Atochem Elf Sa | Synthese de 1,1,1,3,3-pentafluoropropane |
| US5616819A (en) * | 1995-08-28 | 1997-04-01 | Laroche Industries Inc. | Process for preparing fluorinated aliphatic compounds |
| FR2740132B1 (fr) * | 1995-10-23 | 1997-12-19 | Solvay | Procede pour la preparation de 1,1,1,3,3-pentafluoropropane |
-
1996
- 1996-05-13 FR FR9605908A patent/FR2748473B1/fr not_active Expired - Fee Related
-
1997
- 1997-04-20 DE DE1997116337 patent/DE19716337A1/de not_active Withdrawn
- 1997-04-22 CA CA 2203433 patent/CA2203433A1/fr not_active Abandoned
- 1997-04-28 ES ES9700910A patent/ES2128256B1/es not_active Expired - Lifetime
- 1997-05-06 GB GB9709202A patent/GB2313118A/en not_active Withdrawn
- 1997-05-13 CN CN 97111593 patent/CN1166479A/zh active Pending
- 1997-05-13 JP JP12245397A patent/JPH1087523A/ja active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| CA2203433A1 (fr) | 1997-11-13 |
| ES2128256A1 (es) | 1999-05-01 |
| DE19716337A1 (de) | 1997-11-20 |
| CN1166479A (zh) | 1997-12-03 |
| FR2748473A1 (fr) | 1997-11-14 |
| JPH1087523A (ja) | 1998-04-07 |
| FR2748473B1 (fr) | 1998-07-24 |
| GB2313118A (en) | 1997-11-19 |
| GB9709202D0 (en) | 1997-06-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EC2A | Search report published |
Date of ref document: 19990501 Kind code of ref document: A1 Effective date: 19990501 |
|
| FA2A | Application withdrawn |
Effective date: 20001025 |