ES2129793T3 - Recuperacion de un aminoacido. - Google Patents
Recuperacion de un aminoacido.Info
- Publication number
- ES2129793T3 ES2129793T3 ES95901510T ES95901510T ES2129793T3 ES 2129793 T3 ES2129793 T3 ES 2129793T3 ES 95901510 T ES95901510 T ES 95901510T ES 95901510 T ES95901510 T ES 95901510T ES 2129793 T3 ES2129793 T3 ES 2129793T3
- Authority
- ES
- Spain
- Prior art keywords
- amino acid
- desired amino
- solution
- resin
- produce
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 150000001413 amino acids Chemical class 0.000 title abstract 9
- 238000011084 recovery Methods 0.000 title 1
- 239000000243 solution Substances 0.000 abstract 5
- 239000012535 impurity Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 abstract 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 abstract 1
- 239000004472 Lysine Substances 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000003729 cation exchange resin Substances 0.000 abstract 1
- 150000001768 cations Chemical class 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 239000012467 final product Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P13/00—Preparation of nitrogen-containing organic compounds
- C12P13/04—Alpha- or beta- amino acids
- C12P13/08—Lysine; Diaminopimelic acid; Threonine; Valine
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
UN METODO PARA RECUPERAR UN AMINOACIDO DESEADO TAL COMO UNA LLISINA DE UNA SOLUCION ACUOSA QUE CONTIENE EL AMINOACIDO DESEADO E IMPUREZAS, QUE INCLUYE LOS PASOS DE PASAR LA SOLUCION A TRAVES DE UNA RESINA DE INTERCAMBIO DE CATIONES PRIMARIOS PARA ABSROVER EL AMINOACIDO DESEADO SOBRE LA RESINA A UN PH INFERIOR QUE EL PUNTO ISOELECTRICO DEL AMINOACIDO DESEADO; ELUCIENDO EL AMINOACIDO DESEADO DE LA RESINA UTILIZANDO UN ELUENTE APROPIADO CON UN PH SUPERIOR AL PUNTO ISOELECTRICO DEL AMINOACIDO DESEADO PARA PRODUCIR UNA PRIMERA SOLUCION, PASANDO LA PRIMERA SOLUCION A TRAVES DE UNA RESINA DE INTERCAMBIO DE CATIONES SECUNDARIOS PARA ABSORBER UNA O MAS DE LAS IMPUREZAS Y PRODUCIR UNA SEGUNDA SOLUCION DEJANDO LA RESINA, Y RECOGIENDO LA SEGUNDA SOLUCION HASTA QUE EL INDICE DE CONCENTRACION DE UNA IMPUREZA SELECCIONADA AL AMINOACIDO DESEADO, ALCANCE UN VALOR ELEGIDO PARA PRODUCIR UNA TERCERA SOLUCION QUE CONTENGA UN NIVEL INFERIOR DE IMPUREZAS QUE LA PRIMERA, Y RECUPERANDO EL AMINOACIDO DESEADO DE LA TERCERA SOLUCION. ESTE METODO EVITA LA NECESIDAD DE UN PASO DE CRISTALIZACION COSTOSO PARA PRODUCIR EL PRODUCTO FINAL.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA938660 | 1993-11-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2129793T3 true ES2129793T3 (es) | 1999-06-16 |
Family
ID=25583439
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES95901510T Expired - Lifetime ES2129793T3 (es) | 1993-11-19 | 1994-11-18 | Recuperacion de un aminoacido. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US5684190A (es) |
| EP (1) | EP0729451B1 (es) |
| CN (1) | CN1054839C (es) |
| AU (1) | AU682423B2 (es) |
| BR (1) | BR9408087A (es) |
| CZ (1) | CZ141496A3 (es) |
| DE (1) | DE69416526T2 (es) |
| ES (1) | ES2129793T3 (es) |
| SK (1) | SK281263B6 (es) |
| WO (1) | WO1995014002A1 (es) |
| ZA (1) | ZA949059B (es) |
Families Citing this family (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IL120923A0 (en) * | 1997-05-27 | 1997-09-30 | Amylum Nv | A combined process for the production of lysine and its salts and of a further weak acid and a salt thereof |
| US20060106226A1 (en) * | 1998-02-26 | 2006-05-18 | Aminopath Labs, Llc And A Patent License Agreement | Isolation of amino acids and related isolates |
| KR100578426B1 (ko) * | 1999-02-10 | 2006-05-11 | 씨제이 주식회사 | 연속결정화법에 의한 엘-라이신 제조 방법 |
| ATE406345T1 (de) * | 1999-12-09 | 2008-09-15 | Archer Daniels Midland Co | Reinigung von aminosäuren durch chromatographische simulierte wanderbetttrennung |
| KR100726204B1 (ko) | 2000-03-29 | 2007-06-11 | 아처 다니엘 미드랜드 캄파니 | 발효 브로쓰로부터 염기성 아미노산을 분리하는 방법 |
| US20070161784A1 (en) * | 2006-01-11 | 2007-07-12 | Aminopath Labs, Llc | Methods and products of amino acid isolation |
| DE102006061479A1 (de) * | 2006-12-23 | 2008-06-26 | Evonik Degussa Gmbh | Verfahren zur Herstellung verschiedener, eine Zielsubstanz enthaltender Produkte |
| BRPI0703692B1 (pt) * | 2006-12-25 | 2016-12-27 | Ajinomoto Kk | método para se obter os cristais de um hidrocloreto de aminoácido básico compreendendo gerar um aminoácido básico usando células microbianas por fermentação em um caldo de fermentação ou por um método enzimático em uma solução de reação de enzima usando as células como catalisadores |
| CN101343239B (zh) * | 2008-09-04 | 2012-11-07 | 湖北新生源生物工程股份有限公司 | 从生产l-胱氨酸排放母液中分离l-赖氨酸的方法 |
| CN102206167B (zh) * | 2011-03-25 | 2014-02-26 | 中粮生物化学(安徽)股份有限公司 | 一种赖氨酸的提纯方法 |
| CN102206169B (zh) * | 2011-03-25 | 2014-02-26 | 中粮生物化学(安徽)股份有限公司 | 一种赖氨酸的纯化方法 |
| CN103145573A (zh) * | 2013-03-27 | 2013-06-12 | 中粮生物化学(安徽)股份有限公司 | 一种赖氨酸的纯化方法 |
| CN103819352B (zh) * | 2014-03-13 | 2015-04-22 | 孟州市华兴生物化工有限责任公司 | 一种缬氨酸连续结晶方法 |
| CN104447155B (zh) * | 2014-11-26 | 2016-04-27 | 嘉应学院医学院 | 一种应用于金花茶氨基酸活性成分的梯次分离方法 |
| US10032223B2 (en) | 2015-03-20 | 2018-07-24 | Bank Of America Corporation | System for account linking and future event integration into retirement score calculation |
| US9830660B2 (en) | 2015-03-20 | 2017-11-28 | Bank Of America Corporation | System for augmenting a retirement score with health information |
| US10049406B2 (en) | 2015-03-20 | 2018-08-14 | Bank Of America Corporation | System for sharing retirement scores between social groups of customers |
| US10019760B2 (en) | 2015-03-20 | 2018-07-10 | Bank Of America Corporation | System for utilizing a retirement score to receive benefits |
| US20160297747A1 (en) | 2015-04-08 | 2016-10-13 | Invista North America S.A.R.L. | Materials and methods for the selective recovery of monovalent products from aqueous solutions using continuous ion exchange |
| WO2016164767A1 (en) * | 2015-04-10 | 2016-10-13 | Invista North America S.A.R.L. | Process for separation of diamines and/or omega-aminoacids from a feed mixture |
| CN104926701B (zh) * | 2015-06-30 | 2017-05-03 | 西安蓝晓科技新材料股份有限公司 | 一种蛋氨酸纯化的工艺 |
| US10669233B2 (en) | 2017-12-28 | 2020-06-02 | Sunresin New Materials Co. Ltd., Xi'an | Process of purifying methionine |
| KR20190092951A (ko) * | 2018-01-31 | 2019-08-08 | 씨제이제일제당 (주) | 연속식 크로마토그래피 공정을 이용한 천연 l-시스테인 결정의 제조 방법 |
| CN108929248B (zh) * | 2018-07-02 | 2021-06-11 | 无锡晶海氨基酸股份有限公司 | 一种l-精氨酸盐酸盐的制备方法 |
| CN113015578B (zh) | 2018-09-18 | 2023-11-21 | 英威达纺织(英国)有限公司 | 用于从水性混合物中回收胺及其衍生物的系统和方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2894026A (en) * | 1956-08-01 | 1959-07-07 | Du Pont | Purification of lysine |
| JPS6124548A (ja) * | 1984-07-11 | 1986-02-03 | Ajinomoto Co Inc | 塩基性アミノ酸分離法におけるイオン交換樹脂操作法 |
| JPS6261592A (ja) * | 1985-09-13 | 1987-03-18 | Ajinomoto Co Inc | 塩基性アミノ酸の分離方法 |
| JPH0617346B2 (ja) * | 1986-03-14 | 1994-03-09 | 味の素株式会社 | 陽イオン交換樹脂を用いるアミノ酸の回収方法 |
-
1994
- 1994-11-15 ZA ZA949059A patent/ZA949059B/xx unknown
- 1994-11-18 AU AU10710/95A patent/AU682423B2/en not_active Ceased
- 1994-11-18 EP EP95901510A patent/EP0729451B1/en not_active Expired - Lifetime
- 1994-11-18 WO PCT/GB1994/002544 patent/WO1995014002A1/en not_active Ceased
- 1994-11-18 DE DE69416526T patent/DE69416526T2/de not_active Expired - Fee Related
- 1994-11-18 BR BR9408087A patent/BR9408087A/pt not_active Application Discontinuation
- 1994-11-18 SK SK644-96A patent/SK281263B6/sk unknown
- 1994-11-18 CN CN94194710A patent/CN1054839C/zh not_active Expired - Fee Related
- 1994-11-18 CZ CZ961414A patent/CZ141496A3/cs unknown
- 1994-11-18 ES ES95901510T patent/ES2129793T3/es not_active Expired - Lifetime
- 1994-11-18 US US08/640,909 patent/US5684190A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0729451A1 (en) | 1996-09-04 |
| BR9408087A (pt) | 1998-07-14 |
| AU682423B2 (en) | 1997-10-02 |
| SK64496A3 (en) | 1996-12-04 |
| DE69416526D1 (de) | 1999-03-25 |
| WO1995014002A1 (en) | 1995-05-26 |
| CZ141496A3 (en) | 1996-09-11 |
| SK281263B6 (sk) | 2001-01-18 |
| DE69416526T2 (de) | 1999-06-17 |
| AU1071095A (en) | 1995-06-06 |
| EP0729451B1 (en) | 1999-02-10 |
| CN1054839C (zh) | 2000-07-26 |
| CN1139918A (zh) | 1997-01-08 |
| ZA949059B (en) | 1995-07-19 |
| US5684190A (en) | 1997-11-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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