ES2130294T3 - Procedimiento para la obtencion de tocoferoles y esteroles a partir de fuentes naturales. - Google Patents

Procedimiento para la obtencion de tocoferoles y esteroles a partir de fuentes naturales.

Info

Publication number
ES2130294T3
ES2130294T3 ES94101257T ES94101257T ES2130294T3 ES 2130294 T3 ES2130294 T3 ES 2130294T3 ES 94101257 T ES94101257 T ES 94101257T ES 94101257 T ES94101257 T ES 94101257T ES 2130294 T3 ES2130294 T3 ES 2130294T3
Authority
ES
Spain
Prior art keywords
procedure
fat
sterols
obtaining
distillation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94101257T
Other languages
English (en)
Inventor
Christian Fizet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
F Hoffmann La Roche AG
Original Assignee
F Hoffmann La Roche AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by F Hoffmann La Roche AG filed Critical F Hoffmann La Roche AG
Application granted granted Critical
Publication of ES2130294T3 publication Critical patent/ES2130294T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
    • C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
    • C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
    • C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
    • C07D311/70—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with two hydrocarbon radicals attached in position 2 and elements other than carbon and hydrogen in position 6
    • C07D311/72—3,4-Dihydro derivatives having in position 2 at least one methyl radical and in position 6 one oxygen atom, e.g. tocopherols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07J—STEROIDS
    • C07J9/00—Normal steroids containing carbon, hydrogen, halogen or oxygen substituted in position 17 beta by a chain of more than two carbon atoms, e.g. cholane, cholestane, coprostane
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/17—Saline water conversion

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Pyrane Compounds (AREA)
  • Steroid Compounds (AREA)
  • Fats And Perfumes (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

LA INVENCION SE REFIERE A UN NUEVO PROCEDIMIENTO PARA OBTENER TOCOFENOLES Y ESTEROLES DE FUENTES NATURALES, PARTICULARMENTE FUENTES VEGETALES. EN ESTE PROCEDIMIENTO SE TRATA PARTICULARMENTE DE UN PROCEDIMIENTO PARA SEPARAR TOCOFENOLES Y ESTEROLES DE LA GRASA SEPARADORA DE VAHOS A TRAVES DE DESTILACION DE ESA GRASA SEPARADORA DE VAHOS, EN LA QUE ANTES DE LA DESTILACION DEL ESTEROL PRESENTE EN LA GRASA SEPARADORA DE VAHOS SE ESTERIFICA CON ACIDOS GRASOS PRESENTES EVENTUALMENTE. LA MEZCLA RESULTANTE SE DESTILA PARA OBTENER EL ACIDO GRASO SOBRANTE Y A CONTINUACION OBTENCION DE TOCOFENOLES, POR LO QUE LOS ESTERES ESTEROLES FORMADOS EN LA ESTERIFICACION SE DEVUELVEN A ESTA DESTILACION EN RESIDUOS Y DESPUES LOS TOCOFENOLES SE AISLAN DEL DESTILADO Y DE LOS ESTEROLES DESPUES DE LA DISOCIACION DE LOS ESTERES EN LOS RESIDUOS DE DESTILACION.
ES94101257T 1993-02-11 1994-01-28 Procedimiento para la obtencion de tocoferoles y esteroles a partir de fuentes naturales. Expired - Lifetime ES2130294T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH46793 1993-02-11

Publications (1)

Publication Number Publication Date
ES2130294T3 true ES2130294T3 (es) 1999-07-01

Family

ID=4187684

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94101257T Expired - Lifetime ES2130294T3 (es) 1993-02-11 1994-01-28 Procedimiento para la obtencion de tocoferoles y esteroles a partir de fuentes naturales.

Country Status (7)

Country Link
US (1) US5487817A (es)
EP (1) EP0610742B1 (es)
JP (1) JP2648450B2 (es)
AT (1) ATE178061T1 (es)
DE (1) DE59407982D1 (es)
DK (1) DK0610742T3 (es)
ES (1) ES2130294T3 (es)

Families Citing this family (52)

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EP0992500B1 (en) * 1993-08-06 2002-02-13 Henkel Corporation Recovery of tocopherols
GB9318271D0 (en) * 1993-09-03 1993-10-20 Scotia Holdings Plc Tocopherols
US5582692A (en) * 1994-10-07 1996-12-10 Artisan Industries, Inc. Method for the purification of vitamin E
US5512691A (en) * 1994-11-07 1996-04-30 Eastman Chemical Company Process for the production of tocopherol concentrates
US5660691A (en) * 1995-11-13 1997-08-26 Eastman Chemical Company Process for the production of tocotrienol/tocopherol blend concentrates
JPH09157342A (ja) * 1995-12-07 1997-06-17 Nof Corp ポリウレタン樹脂の水系分散物、ポリウレタン樹脂グラフト重合体の水系分散物および水系塗料組成物
US5917068A (en) * 1995-12-29 1999-06-29 Eastman Chemical Company Polyunsaturated fatty acid and fatty acid ester mixtures free of sterols and phosphorus compounds
US6063946A (en) * 1996-01-26 2000-05-16 Eastman Chemical Company Process for the isolation of polyunsaturated fatty acids and esters thereof from complex mixtures which contain sterols and phosphorus compounds
US5883273A (en) * 1996-01-26 1999-03-16 Abbott Laboratories Polyunsaturated fatty acids and fatty acid esters free of sterols and phosphorus compounds
JP3792309B2 (ja) * 1996-08-30 2006-07-05 サントリー株式会社 不飽和脂肪酸含有油脂の製造方法
CN1295568A (zh) * 1998-01-29 2001-05-16 伊斯曼化学公司 从含有母育酚的混合物中分离生育三烯酚的方法及其组合物
US6706898B2 (en) 1998-01-29 2004-03-16 Archer-Daniels-Midland Company Methods for separating a tocopherol from a tocopherol-containing mixture
US20050107582A1 (en) * 2003-07-30 2005-05-19 Alfred Wong Method for the preparation of phytosterols from tall oil pitch
US6011131A (en) * 1998-05-19 2000-01-04 Henkel Corporation Process for the preparation of polyamides
US6281373B1 (en) 1998-05-19 2001-08-28 Henkel Corporation Process for the preparation of dimeric fatty acid C1-4 alkyl esters
US6178466B1 (en) * 1998-06-12 2001-01-23 Unisys Corporation System for maximizing bandpass on an interface directly coupling two units where the interface has independently operative data and address interconnections, and computer sysem employing same.
US6844458B2 (en) 1998-11-20 2005-01-18 Ip Holdings, L.L.C. Vegetable oil refining
DE19906551C1 (de) 1999-02-13 2000-06-29 Cognis Deutschland Gmbh Verfahren zur Herstellung von Phytosterinen
DE19916034C1 (de) * 1999-04-09 2000-08-03 Cognis Deutschland Gmbh Verfahren zur Gewinnung von Phytosterinen
WO2001032682A1 (en) * 1999-11-04 2001-05-10 Kao Corporation Process for the purification of phytosterol from fatty acids and their esters
US6160143A (en) * 2000-02-18 2000-12-12 Artisan Industries Inc. Method for the concentration and separation of sterols
AU2001255286A1 (en) 2000-04-14 2001-10-30 Mars, Incorporated Extraction of sterols from cocoa hulls
ES2177401B1 (es) * 2000-06-28 2004-09-16 Vitae-Caps, S.A. Procedimiento de extraccion y purificacion de tocoferoles naturales y esteroles por esterificacion con trimetilol propano.
US6429320B1 (en) 2000-08-04 2002-08-06 Cognis Corporation Processes for the purification of tocopherol and/or sterol compounds and compositions containing orthoborate ester mixtures
DE10038457B4 (de) * 2000-08-07 2008-09-25 Cognis Ip Management Gmbh Verfahren zur Gewinnung von Sterinen und Tocopherolen
DE10038442A1 (de) 2000-08-07 2002-02-21 Cognis Deutschland Gmbh Verfahren zur Gewinnung von Sterinen aus fettsäurehaltigen Rückständen
US6838104B2 (en) * 2000-12-20 2005-01-04 Archer Daniels Midland Company Process for the production of tocotrienols
EP1417288B1 (en) * 2001-07-23 2018-08-29 Cargill, Incorporated Method and apparatus for processing vegetable oils
US6750359B1 (en) 2001-09-04 2004-06-15 Ip Holdings, L.L.C. Methods for treating deodorizer distillate
WO2003037884A2 (en) * 2001-09-19 2003-05-08 Archer-Daniels-Midland Company Process for separation of tocopherols
US6673945B2 (en) * 2001-11-08 2004-01-06 Archer-Daniels Midland Company Process for production of high purity tocopherols
US20040030166A1 (en) * 2002-03-18 2004-02-12 Dick Copeland Methods for treating deodorizer distillate
MY142319A (en) * 2002-08-20 2010-11-15 Malaysian Palm Oil Board Mpob Extraction of palm vitamin e, phytosterols and squalene from palm oil
AU2004272561A1 (en) * 2003-09-10 2005-03-24 Eastman Chemical Company Process for the recovery of a phytolipid composition
US7416756B2 (en) * 2003-09-10 2008-08-26 Eastman Chemical Company Process for the recovery of a phytolipid composition
FR2885744B1 (fr) * 2005-05-10 2007-07-20 Thales Sa Dispositif de mesure optique actif avec amplification de faible signal
US20080015367A1 (en) * 2006-07-11 2008-01-17 Wiley Organics, Inc. Process for isolating phytosterols and tocopherols from deodorizer distillate
EP2155888B1 (en) * 2007-05-24 2014-07-09 Loders Croklaan B.V. Process for producing compositions comprising tocopherols and tocotrienols
FR2933403B1 (fr) * 2008-07-07 2010-08-27 Sophim Procede d'extration de squalene, de stereols et de vitamine e contenus dans des condensats de raffinage physique et/ou dans des distillats de desodorisation d'huiles vegetales
DE102010011606B4 (de) * 2010-03-16 2020-12-03 Air Liquide Global E&C Solutions Germany Gmbh Verfahren zur Aufarbeitung von Biodieselschlamm
CN103965155B (zh) * 2014-04-15 2018-10-16 江苏玺鑫维生素有限公司 一种天然维生素e的制备工艺
DE102014009237A1 (de) 2014-06-24 2015-12-24 Weylchem Wiesbaden Gmbh Verfahren zur Gewinnung von Vitamin E, Sterolen und/oder Terpenen aus öligen oder fettigen Gemischen biologischer Herkunft
WO2016149692A1 (en) 2015-03-19 2016-09-22 Inventure Renewables, Inc. Complete saponification and acidulation of natural oil processing byproducts and treatment of reaction products
US9745541B1 (en) 2016-09-09 2017-08-29 Inventure Renewables, Inc. Methods for making free fatty acids from soaps using thermal hydrolysis followed by acidification
IT201600116065A1 (it) * 2016-11-17 2018-05-17 Green Oleo Srl Processo per la purificazione della frazione insaponificabile di oli vegetali
EP3813539A4 (en) 2018-05-03 2022-04-06 Renewable Energy Group, Inc. PROCESSES AND EQUIPMENT FOR THE PRODUCTION OF BIODIESEL, DIESEL SERIES HYDROCARBONS AND PRODUCTS OBTAINED FROM THEM
CN108912089B (zh) * 2018-06-21 2022-07-15 江苏科鼐生物制品有限公司 一种50ve和甾醇离心分离的方法及其结晶过滤联合系统
EP3877355A4 (en) 2018-11-06 2022-08-03 Inventure International (Pte) Limited PROCESS FOR PRODUCTION OF FREE FATTY ACIDS AND FATTY ACID DERIVATIVES FROM MIXED LIPID RAW MATERIALS OR SOAP STICKS
CN114450386A (zh) 2019-09-27 2022-05-06 巴斯夫欧洲公司 用于生产甾醇和/或生育酚并回收副产物的方法
CA3146079A1 (en) 2019-09-27 2021-04-01 Valerie Eychenne Process for the production and purification of sterols
CN114502568B (zh) 2019-09-27 2025-06-13 巴斯夫欧洲公司 用于纯化植物甾醇的方法
CN116059690B (zh) * 2023-01-13 2023-10-31 山东兴泉油脂有限公司 一种从玉米胚芽油脱臭馏出物提取生物活性成分的方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
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US2704764A (en) * 1952-02-19 1955-03-22 Benjamin Clayton Treatment of fatty material
US2866797A (en) * 1954-11-01 1958-12-30 Gen Mills Inc Improved process of isolating sterols
US3122565A (en) * 1960-10-22 1964-02-25 Eisai Co Ltd Purification process of tocopherol containing materials
US3108120A (en) * 1961-02-23 1963-10-22 Eastman Kodak Co Process for recovery of tocopherols and sterols
US3153054A (en) * 1962-03-20 1964-10-13 Eastman Kodak Co Process for separating tocopherols and sterols from deodorizer sludge and the like
US3153055A (en) * 1962-03-20 1964-10-13 Eastman Kodak Co Process for separating tocopherols and sterols from deodorizer sludge and the like
US3335154A (en) * 1963-06-04 1967-08-08 Eastman Kodak Co Separation of tocopherols and sterols from deodorizer sludge and the like

Also Published As

Publication number Publication date
US5487817A (en) 1996-01-30
EP0610742B1 (de) 1999-03-24
JP2648450B2 (ja) 1997-08-27
DE59407982D1 (de) 1999-04-29
EP0610742A1 (de) 1994-08-17
DK0610742T3 (da) 1999-10-18
JPH072827A (ja) 1995-01-06
ATE178061T1 (de) 1999-04-15

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