ES2130729T3 - Procedimiento para la esterificacion de acido (met)acrilico con un alcanol. - Google Patents

Procedimiento para la esterificacion de acido (met)acrilico con un alcanol.

Info

Publication number
ES2130729T3
ES2130729T3 ES96115455T ES96115455T ES2130729T3 ES 2130729 T3 ES2130729 T3 ES 2130729T3 ES 96115455 T ES96115455 T ES 96115455T ES 96115455 T ES96115455 T ES 96115455T ES 2130729 T3 ES2130729 T3 ES 2130729T3
Authority
ES
Spain
Prior art keywords
met
procedure
acrylic acid
esterification
alcanol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96115455T
Other languages
English (en)
Inventor
Heinrich Dr Aichinger
Michael Dr Fried
Gerhard Dr Nestler
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2130729T3 publication Critical patent/ES2130729T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/03—Preparation of carboxylic acid esters by reacting an ester group with a hydroxy group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
    • C07C67/317—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups
    • C07C67/327—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by splitting-off hydrogen or functional groups; by hydrogenolysis of functional groups by elimination of functional groups containing oxygen only in singly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/003—Esters of saturated alcohols having the esterified hydroxy group bound to an acyclic carbon atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

EN UN PROCEDIMIENTO PARA LA ESTERIFICACION DE ACIDO (MET)ACRILICO CON UN ALCANOL EN PRESENCIA DE UN CATALIZADOR DE ESTERIFICACION, EN EL CUAL SE SEPARAN POR DESTILACION LOS COMPUESTOS DE PARTIDA QUE NO HAN REACCIONADO Y EL ESTER DEL ACIDO (MET)ACRILICO QUE SE VA A FORMAR, APARECIENDO UN RESIDUO QUE CONTIENE UN OXIESTER, SE SEPARA PRIMERO EL RESIDUO, DESPUES SE SEPARA POR DESTILACION EL OXIESTER QUE LLEVA, Y EL DESTILADO SE DISOCIA EN PRESENCIA DE ACIDOS A ELEVADA TEMPERATURA. EL PROCEDIMIENTO SE PUEDE LLEVAR A CABO EN PRESENCIA DE OXIGENO MOLECULAR. EL DESTILADO SE DISOCIA A TEMPERATURAS DE 170 A 250 FERIBLEMENTE DE 180 A 230
ES96115455T 1995-09-28 1996-09-26 Procedimiento para la esterificacion de acido (met)acrilico con un alcanol. Expired - Lifetime ES2130729T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19536184A DE19536184A1 (de) 1995-09-28 1995-09-28 Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol

Publications (1)

Publication Number Publication Date
ES2130729T3 true ES2130729T3 (es) 1999-07-01

Family

ID=7773491

Family Applications (1)

Application Number Title Priority Date Filing Date
ES96115455T Expired - Lifetime ES2130729T3 (es) 1995-09-28 1996-09-26 Procedimiento para la esterificacion de acido (met)acrilico con un alcanol.

Country Status (12)

Country Link
US (1) US5767306A (es)
EP (1) EP0765860B1 (es)
JP (1) JPH09124552A (es)
KR (1) KR970015557A (es)
CN (1) CN1087013C (es)
CA (1) CA2184196A1 (es)
CZ (1) CZ270096A3 (es)
DE (2) DE19536184A1 (es)
ES (1) ES2130729T3 (es)
MX (1) MX9604040A (es)
SG (1) SG50764A1 (es)
TW (1) TW400324B (es)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19922722A1 (de) 1999-05-18 2000-11-23 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäureestern
BR0214697B1 (pt) 2001-12-04 2013-02-05 processo para produÇço de Ácidos (met)acrÍlicos.
CN1252030C (zh) * 2001-12-26 2006-04-19 三菱化学株式会社 生产(甲基)丙烯酸酯时的副产物分解方法
FR2901272B1 (fr) * 2006-05-18 2008-06-27 Arkema France Procede perfectionne de fabrication de (meth)acrylates d'alkyle en c1-c4
CN102850218A (zh) * 2012-09-28 2013-01-02 沈阳石蜡化工有限公司 一种丙烯酸正丁酯的生产方法
CN110372509A (zh) * 2019-07-19 2019-10-25 江门谦信化工发展有限公司 一种丙烯酸正丁酯重组分的裂解回收工艺
EP4015498B1 (de) 2020-12-18 2024-04-24 Basf Se Verfahren zur kontinuierlichen herstellung von acrylsäure-n-butylester
FR3128459B1 (fr) 2021-10-25 2023-09-22 Arkema France D’acrylate de butyle de purete elevee

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1178058B (de) * 1960-04-29 1964-09-17 Wacker Chemie Gmbh Verfahren zur Trennung einer azeotrope Gemische bildenden Mischung aus Acryl- oder ª‡-Alkylacrylsaeurealkylestern und Alkoholen
GB923595A (en) * 1960-12-03 1963-04-18 Distillers Co Yeast Ltd Improvements in and relating to the production of acrylic esters
US3868410A (en) * 1972-08-03 1975-02-25 Celanese Corp Conversion of oligomeric acrylates to acrylate monomers
DE2339529A1 (de) 1973-08-03 1975-02-13 Ardie Werk Gmbh Kraftstoffeinspritzpumpenverstellvorrichtung
JPS5762229A (en) * 1980-10-02 1982-04-15 Mitsubishi Petrochem Co Ltd Recovery of useful component from heavy substance obtained as by-product in preparation of acrylic ester
CN1058390A (zh) * 1990-07-13 1992-02-05 梁效成 含烷氧基丙酸酯废液的处理方法
JPH0768168B2 (ja) * 1991-07-12 1995-07-26 東亞合成株式会社 アクリル酸エステルのミカエル付加物の分解方法
CN1026104C (zh) * 1992-03-17 1994-10-05 侯玉里 丙烯酸酯类废油再生工艺
JP2943523B2 (ja) * 1992-08-12 1999-08-30 東亞合成株式会社 アクリル酸エステルのミカエル付加物から有用化合物を製造する方法
DE19547485A1 (de) * 1995-12-19 1996-05-09 Basf Ag Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol

Also Published As

Publication number Publication date
JPH09124552A (ja) 1997-05-13
CN1087013C (zh) 2002-07-03
TW400324B (en) 2000-08-01
KR970015557A (ko) 1997-04-28
US5767306A (en) 1998-06-16
CA2184196A1 (en) 1997-03-29
SG50764A1 (en) 1998-07-20
MX9604040A (es) 1997-03-29
CN1153769A (zh) 1997-07-09
CZ270096A3 (cs) 1998-05-13
EP0765860B1 (de) 1999-05-06
DE19536184A1 (de) 1997-04-03
EP0765860A1 (de) 1997-04-02
DE59601814D1 (de) 1999-06-10

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