ES2132854T3 - Procedimiento de purificacion del acido acrilico obtenido por oxidacion catalitica del propileno. - Google Patents

Procedimiento de purificacion del acido acrilico obtenido por oxidacion catalitica del propileno.

Info

Publication number
ES2132854T3
ES2132854T3 ES96401590T ES96401590T ES2132854T3 ES 2132854 T3 ES2132854 T3 ES 2132854T3 ES 96401590 T ES96401590 T ES 96401590T ES 96401590 T ES96401590 T ES 96401590T ES 2132854 T3 ES2132854 T3 ES 2132854T3
Authority
ES
Spain
Prior art keywords
acrylic acid
column
heavy
head
solvent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96401590T
Other languages
English (en)
Inventor
Michel Fauconet
Marc Esch
Yves Samuel
Denis Laurent
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Elf Atochem SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Elf Atochem SA filed Critical Elf Atochem SA
Application granted granted Critical
Publication of ES2132854T3 publication Critical patent/ES2132854T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

SE PURIFICA EL ACIDO ACRILICO OBTENIDO POR OXIDACION CATALITICA DEL PROPILENO, EXTRAIDO POR LAVADO A CONTRACORRIENTE DE LOS GASES DE REACCION POR AL MENOS UN SOLVENTE PESADO HIDROFOBO EN UNA COLUMNA DE EXTRACCION (C1). A ESTE EFECTO, SE CONDUCE, EN UNA COLUMNA (C3), UNA DESTILACION DEL FLUJO (5) OBTENIDO EN PIE DE COLUMNA (C1), DE MANERA QUE OBTENGA UN FLUJO MUY PURO DE ACIDO ACRILICO (6) EN CABEZA DE LA COLUMNA (C3), DEJANDO PASAR ACIDO ACRILICO EN PIE (7); SE ENVIA EL FLUJO DE PIE (7) DE ALIMENTACION A LA PARTE INFERIOR DE UNA COLUMNA DE DESTILACION (C4) DE DONDE SE TRASIEGA LATERALMENTE, SOBRE UN PLATO SITUADO ENTRE LA ALIMENTACION Y LA CABEZA DE COLUMNA, UN FLUJO (9) RICO EN ANHIDRIDO MALEICO E IMPUREZAS A TEMPERATURAS DE EBULLICION SITUADAS ENTRE LA DEL ACIDO ACRILICO Y LA DEL SOLVENTE PESADO: SE DESTILA EN CABEZA DE LA COLUMNA (C4), UN FLUJO (8) RICO EN ACIDO ACRILICO QUE SE REENVIA COMO ALIMENTACION DE LA COLUMNA (C3); Y SE RECUPERA, EN PIE DE LA COLUMNA (C4); UN FLUJO (1) QUE CONTIENE SOLVENTE PESADO E IMPUREZAS PESADAS, QUE SE RECICLA EN CABEZA DE LA COLUMNA (C1).
ES96401590T 1995-07-18 1996-07-17 Procedimiento de purificacion del acido acrilico obtenido por oxidacion catalitica del propileno. Expired - Lifetime ES2132854T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9508672A FR2736912B1 (fr) 1995-07-18 1995-07-18 Procede de purification de l'acide acrylique obtenu par oxydation catalytique du propylene

Publications (1)

Publication Number Publication Date
ES2132854T3 true ES2132854T3 (es) 1999-08-16

Family

ID=9481089

Family Applications (1)

Application Number Title Priority Date Filing Date
ES96401590T Expired - Lifetime ES2132854T3 (es) 1995-07-18 1996-07-17 Procedimiento de purificacion del acido acrilico obtenido por oxidacion catalitica del propileno.

Country Status (15)

Country Link
US (1) US5705688A (es)
EP (1) EP0754671B1 (es)
JP (1) JP3053575B2 (es)
KR (1) KR100205270B1 (es)
CN (1) CN1063426C (es)
AT (1) ATE178308T1 (es)
CA (1) CA2181508C (es)
CZ (1) CZ288198B6 (es)
DE (1) DE69601902T2 (es)
DK (1) DK0754671T3 (es)
ES (1) ES2132854T3 (es)
FR (1) FR2736912B1 (es)
GR (1) GR3030552T3 (es)
MY (1) MY132188A (es)
SG (1) SG52823A1 (es)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3948855B2 (ja) * 1999-06-10 2007-07-25 株式会社日本触媒 （メタ）アクリル酸の製造方法
DE10138150A1 (de) * 2001-08-03 2003-02-13 Basf Ag Verfahren zur Herstellung wasserabsorbierender Harze
CN100389848C (zh) * 2001-10-30 2008-05-28 三菱化学株式会社 一种薄膜蒸发器及其在（甲基）丙烯酸精制方法中的应用
BRPI0411842B1 (pt) * 2003-06-26 2014-01-14 Processo para separação e recuperação de ácido 3-hidroxipropiônico e ácido acrílico
FR2861725B1 (fr) * 2003-11-04 2005-12-30 Arkema Procede de purification de l'acide (meth)acrylique obtenu par oxydation d'un substrat gazeux
CN1304354C (zh) * 2005-02-06 2007-03-14 蓝仁水 萃取与共沸精馏相结合提纯（甲基）丙烯酸的工艺方法
CN1907543B (zh) * 2005-07-13 2010-05-12 中国石油兰州石油化工公司 气体脱杂质塔及气体脱杂质的方法
CN101260036B (zh) * 2008-03-21 2011-01-26 中国石油集团工程设计有限责任公司东北分公司 丙烯两步加氧法制丙烯酸生产装置中精制单元的改进工艺
US20130274520A1 (en) 2012-04-11 2013-10-17 The Procter & Gamble Company Purification Of Bio Based Acrylic Acid To Crude And Glacial Acrylic Acid
FR3008971B1 (fr) * 2013-07-29 2016-08-19 Arkema France Procede de production en continu d'acrylates legers par esterification d'un acide acrylique de grade ester brut
JP6847843B2 (ja) 2015-02-13 2021-03-24 ノボマー， インコーポレイテッド ポリプロピオラクトンの生成のためのプロセスおよびシステム
MA41510A (fr) 2015-02-13 2017-12-19 Novomer Inc Procédé de production d'acide acrylique
JP2018506546A (ja) 2015-02-13 2018-03-08 ノボマー， インコーポレイテッド 融通性のある化学物質生成プラットフォーム
MA41508A (fr) 2015-02-13 2017-12-19 Novomer Inc Systèmes et procédés de production d'acide polyacrylique
EP3696161A1 (en) 2015-02-13 2020-08-19 Novomer, Inc. Continuous carbonylation processes
MA41513A (fr) 2015-02-13 2017-12-19 Novomer Inc Procédé de distillation pour la production d'acide acrylique
MA41507A (fr) 2015-02-13 2017-12-19 Novomer Inc Systèmes et procédés de production de polymères
BR112018002143A2 (pt) 2015-07-31 2018-09-18 Novomer Inc sistema de produção/processo de produção para ácido acrílico e precursores do mesmo
KR102080287B1 (ko) * 2016-12-06 2020-02-21 주식회사 엘지화학 (메트)아크릴산의 회수 방법
FR3089222A1 (fr) * 2018-11-29 2020-06-05 Arkema France Purification de solutions aqueuses contenant du formaldehyde, et utilisation de la solution purifiee dans un procede de production d’acide acrylique
KR20210137037A (ko) 2019-03-08 2021-11-17 노보머, 인코포레이티드 아미드 및 니트릴 화합물을 생산하기 위한 통합 방법 및 시스템

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3555082A (en) * 1966-12-15 1971-01-12 Knapsack Ag Process for isolating acrylic acid from the reaction gases obtained by oxidation of propylene or acrolein
DE1668362B2 (de) * 1968-02-17 1976-11-11 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung aliphatischer acrylsaeureester
DE2005163A1 (de) * 1970-02-05 1971-08-19 Knapsack Ag, 5033 Knapsack Verfahren zur Abtrennung von Acrylsäure aus wäßriger Rohacrylsaure
BE786398A (fr) * 1971-07-21 1973-01-18 Basf Ag Procede de preparation de l'acide acrylique anhydre
DE2241714A1 (de) * 1972-08-24 1974-03-28 Basf Ag Verfahren zur abtrennung von acrylsaeure aus den reaktionsgasen der propylenoder acroleinoxydation
US4166774A (en) * 1977-12-05 1979-09-04 The Standard Oil Company Acrylic acid recovery and purification

Also Published As

Publication number Publication date
ATE178308T1 (de) 1999-04-15
CN1143069A (zh) 1997-02-19
JP3053575B2 (ja) 2000-06-19
CA2181508A1 (fr) 1997-01-19
CA2181508C (fr) 1999-07-13
KR100205270B1 (ko) 1999-07-01
DK0754671T3 (da) 1999-10-18
CZ288198B6 (en) 2001-05-16
US5705688A (en) 1998-01-06
FR2736912A1 (fr) 1997-01-24
EP0754671B1 (fr) 1999-03-31
JPH09118645A (ja) 1997-05-06
MY132188A (en) 2007-09-28
CZ214196A3 (en) 1997-02-12
KR970006252A (ko) 1997-02-19
CN1063426C (zh) 2001-03-21
DE69601902T2 (de) 1999-08-19
GR3030552T3 (en) 1999-10-29
DE69601902D1 (de) 1999-05-06
SG52823A1 (en) 1998-09-28
FR2736912B1 (fr) 1997-08-22
EP0754671A1 (fr) 1997-01-22

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