ES2142006T3 - Proceso para la produccion de acido tereftalico. - Google Patents

Proceso para la produccion de acido tereftalico.

Info

Publication number
ES2142006T3
ES2142006T3 ES96115916T ES96115916T ES2142006T3 ES 2142006 T3 ES2142006 T3 ES 2142006T3 ES 96115916 T ES96115916 T ES 96115916T ES 96115916 T ES96115916 T ES 96115916T ES 2142006 T3 ES2142006 T3 ES 2142006T3
Authority
ES
Spain
Prior art keywords
acid
area
acetic acid
thereftalic
deposit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96115916T
Other languages
English (en)
Inventor
Eric Hindmarsh
John Arthur Turner
Alan Macpherson Ure
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Application granted granted Critical
Publication of ES2142006T3 publication Critical patent/ES2142006T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
    • C07C63/14—Monocyclic dicarboxylic acids
    • C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
    • C07C63/26—1,4 - Benzenedicarboxylic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

UNA SUSPENSION ACUOSA ESPESA DE ACIDO TEREFTALICO EN ACIDO ACETICO QUE SE PRODUCE MEDIANTE LA OXIDACION DE P-XILENO EN ACIDO ACETICO, ELIMINADO AGUA MEDIANTE LA EVAPORACION DE UNA CORRIENTE DE AGUA Y ACIDO ACETICO Y DEVOLVIENDO ACIDO ACETICO A LA FASE DE OXIDACION. EL ACIDO TEREFTALICO SE SEPARA DEL MEDIO DE REACCION EN UNA PRIMERA ZONA PARA DEJAR UN DEPOSITO EN UNA BANDA, EL DEPOSITO SE LAVA CON UN PRIMER MEDIO ACUOSO EN UNA SEGUNDA ZONA, SE ELIMINA DE LA BANDA EN UNA TERCERA ZONA Y SE MEZCLA CON UN SEGUNDO MEDIO ACUOSO. EL MEDIO DE REACCION SE PASA DESDE LA PRIMERA ZONA A LA FASE DE OXIDACION Y SE RECUPERA ACIDO TEREFTALICO, PREFERENTEMENTE TRAS UNA NUEVA PURIFICACION.
ES96115916T 1991-03-07 1992-02-02 Proceso para la produccion de acido tereftalico. Expired - Lifetime ES2142006T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB919104776A GB9104776D0 (en) 1991-03-07 1991-03-07 Process for the production of terephthalic acid
IDP97064092A ID19108A (id) 1991-03-07 1992-06-08 Proses produksi asam tereftalat (pecahan dari p-002451)

Publications (1)

Publication Number Publication Date
ES2142006T3 true ES2142006T3 (es) 2000-04-01

Family

ID=32599058

Family Applications (2)

Application Number Title Priority Date Filing Date
ES96115916T Expired - Lifetime ES2142006T3 (es) 1991-03-07 1992-02-02 Proceso para la produccion de acido tereftalico.
ES92301413T Expired - Lifetime ES2093189T3 (es) 1991-03-07 1992-02-20 Proceso para la produccion de acido tereftalico.

Family Applications After (1)

Application Number Title Priority Date Filing Date
ES92301413T Expired - Lifetime ES2093189T3 (es) 1991-03-07 1992-02-20 Proceso para la produccion de acido tereftalico.

Country Status (15)

Country Link
US (4) US5563293A (es)
EP (3) EP0754673B1 (es)
JP (1) JPH0565246A (es)
KR (1) KR100225371B1 (es)
CN (2) CN1038409C (es)
CA (1) CA2062063C (es)
DE (2) DE69230569T2 (es)
EG (1) EG19876A (es)
ES (2) ES2142006T3 (es)
GB (2) GB9104776D0 (es)
ID (1) ID19108A (es)
MX (1) MX9200997A (es)
RU (1) RU2106337C1 (es)
SG (1) SG66231A1 (es)
ZA (1) ZA921380B (es)

Families Citing this family (103)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9310070D0 (en) * 1992-05-29 1993-06-30 Ici Plc Process for the production of purified terephthalic acid
GB9400570D0 (en) * 1994-01-13 1994-03-09 Ici Plc Handling of materials at elevated pressure
TW299318B (es) * 1994-11-15 1997-03-01 Mitsubishi Chem Corp
US5961942A (en) * 1995-06-05 1999-10-05 E. I. Du Pont De Nemours And Company Effluent gas treatment
BR9608398A (pt) * 1995-06-05 1999-01-05 Ici Plc Processos para o tratamento de um fluxo de gás efluente e de ácido policarboxílico
US6054610A (en) 1995-06-07 2000-04-25 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid and isophthalic acid from mixed xylenes
US6013835A (en) * 1995-06-07 2000-01-11 Hfm International, Inc. Method and apparatus for preparing purified terephthalic acid
US5767311A (en) 1995-06-07 1998-06-16 Glitsch International, Inc. Method and apparatus for preparing purified terephtalic acid
US5929274A (en) 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
TW442461B (en) * 1996-02-22 2001-06-23 Du Pont Process for the production of an aromatic carboxylic acid
EP0882009B1 (en) * 1996-02-22 2001-05-16 E.I. Du Pont De Nemours And Company Production of aromatic polycarboxylic acids
GB9705349D0 (en) 1997-03-14 1997-04-30 Ici Plc Treatment of effluent streams
AU729150B2 (en) * 1997-12-12 2001-01-25 Mitsubishi Heavy Industries, Ltd. Rolling system and rolling method
KR20010033086A (ko) * 1997-12-15 2001-04-25 오노 알버어스 방향족 카복실산의 제조방법
TW483886B (en) * 1998-08-11 2002-04-21 Du Pont Method for recovering methyl acetate and residual acetic acid in the production of pure terephtalic acid
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IT1319169B1 (it) 2000-07-14 2003-09-26 Eurotecnica Dev & Licensing Sr Procedimento per la purificazione di acidi carbossilici aromatici.
US6765113B2 (en) 2000-07-19 2004-07-20 E.I. Du Pont De Nemours And Company Production of aromatic carboxylic acids
US6384262B1 (en) 2000-12-14 2002-05-07 General Electric Company Process for the production of diaryl carbonates
US6420589B1 (en) 2000-12-14 2002-07-16 General Electric Company Process for the production of diaryl carbonates
US6521777B2 (en) 2000-12-14 2003-02-18 General Electric Company Process for the production of diaryl carbonates
ES2295644T3 (es) * 2002-07-09 2008-04-16 Invista Technologies S.A.R.L. Procedimiento para producir acidos dicarboxilicos aromaticos en condiciones supercriticas.
US7276625B2 (en) * 2002-10-15 2007-10-02 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US7161027B2 (en) 2002-12-09 2007-01-09 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
WO2004052821A1 (en) * 2002-12-09 2004-06-24 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
US7132566B2 (en) * 2003-09-22 2006-11-07 Eastman Chemical Company Process for the purification of a crude carboxylic acid slurry
KR100498490B1 (ko) * 2003-02-28 2005-07-01 삼성전자주식회사 인페이스 신호와 쿼드러쳐 신호 간의 위상차를 가변시킬수 있는 쿼드러쳐 전압제어 발진기
US7193109B2 (en) * 2003-03-06 2007-03-20 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US20050059709A1 (en) * 2003-09-15 2005-03-17 Meythaler Jay M. Treatment of a neuropathy with rapid release aminopyridine
US7214760B2 (en) * 2004-01-15 2007-05-08 Eastman Chemical Company Process for production of a carboxylic acid/diol mixture suitable for use in polyester production
US7546747B2 (en) 2004-01-15 2009-06-16 Eastman Chemical Company Process for production of a dried carboxylic acid cake suitable for use in polyester production
US20050283022A1 (en) * 2004-06-18 2005-12-22 Sheppard Ronald B Filtrate preparation process for terephthalic acid filtrate treatment
US7692037B2 (en) 2004-09-02 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7504535B2 (en) 2004-09-02 2009-03-17 Eastman Chemical Company Optimized liquid-phase oxidation
US7381836B2 (en) * 2004-09-02 2008-06-03 Eastman Chemical Company Optimized liquid-phase oxidation
US7563926B2 (en) 2004-09-02 2009-07-21 Eastman Chemical Company Optimized liquid-phase oxidation
US7390921B2 (en) * 2004-09-02 2008-06-24 Eastman Chemical Company Optimized liquid-phase oxidation
US7371894B2 (en) 2004-09-02 2008-05-13 Eastman Chemical Company Optimized liquid-phase oxidation
US7608732B2 (en) 2005-03-08 2009-10-27 Eastman Chemical Company Optimized liquid-phase oxidation
US7568361B2 (en) * 2004-09-02 2009-08-04 Eastman Chemical Company Optimized liquid-phase oxidation
US7692036B2 (en) 2004-11-29 2010-04-06 Eastman Chemical Company Optimized liquid-phase oxidation
US7741515B2 (en) 2004-09-02 2010-06-22 Eastman Chemical Company Optimized liquid-phase oxidation
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US7304178B2 (en) 2005-05-19 2007-12-04 Eastman Chemical Company Enriched isophthalic acid composition
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CN100368370C (zh) * 2006-03-29 2008-02-13 中国石化仪征化纤股份有限公司 对二甲苯氧化母液中悬浮物的回收系统装置
US8115029B2 (en) 2006-11-02 2012-02-14 University Of Kansas Cobalt-catalyzed oxidations in volumetrically expanded liquids by compressed gases
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CN101417943B (zh) * 2008-12-08 2010-11-10 中国纺织工业设计院 高效回收利用pta装置精制母液的简易方法和系统
CN101914013B (zh) * 2010-07-30 2015-03-18 浙江大学 一种节水的对苯二甲酸生产方法
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CN103459376B (zh) * 2011-03-28 2015-03-18 帝斯曼知识产权资产管理有限公司 制备三聚氰胺的缩合产物的方法
US20140175025A1 (en) * 2012-12-21 2014-06-26 Eastman Chemical Company Generation of low-solids second mother liquor from terephthalic acid production filter
CN104338499B (zh) * 2013-07-31 2016-01-20 沅江华龙催化科技有限公司 一种液固多相反应分离同步反应器
CN104338500B (zh) * 2013-07-31 2015-12-02 沅江华龙催化科技有限公司 一种气液固多相反应分离同步反应器
US9428436B2 (en) 2013-12-18 2016-08-30 Bp Corporation North America Inc. Process and apparatus for manufacturing aromatic carboxylic acids
CA2934789C (en) 2013-12-30 2021-03-02 Thomas M. Bartos Pressurized crude aromatic carboxylic acid feed mixes
CN103772182B (zh) * 2014-01-26 2015-06-17 沅江华龙催化科技有限公司 基于气液固多相反应分离同步反应器的利用空气氧化对二甲苯生产对苯二甲酸的方法
JP2015140342A (ja) * 2014-01-30 2015-08-03 株式会社日立製作所 精製テレフタル酸の製造方法
CN103936581A (zh) * 2014-04-24 2014-07-23 天华化工机械及自动化研究设计院有限公司 一种提高cta溶剂交换效率的方法
CN105085231A (zh) * 2014-05-20 2015-11-25 天华化工机械及自动化研究设计院有限公司 一种pta工业装置氧化单元中醋酸溶剂的处理方法
CN115867683A (zh) 2020-08-14 2023-03-28 科氏技术英国有限公司 从氧化剂清洗流中回收金属催化剂
WO2023021347A1 (en) 2021-08-20 2023-02-23 Koch Technology Solutions UK Limited Nickel and cobalt separation in a pta process

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Also Published As

Publication number Publication date
CA2062063C (en) 2002-07-09
CN1064676A (zh) 1992-09-23
DE69214859D1 (de) 1996-12-05
DE69230569T2 (de) 2000-07-27
EP0502628B1 (en) 1996-10-30
DE69214859T2 (de) 1997-02-27
KR100225371B1 (ko) 1999-10-15
GB9104776D0 (en) 1991-04-17
ES2093189T3 (es) 1996-12-16
SG66231A1 (en) 1999-10-19
EP0754673A1 (en) 1997-01-22
EP0722927A1 (en) 1996-07-24
JPH0565246A (ja) 1993-03-19
EG19876A (en) 1996-06-30
US5679846A (en) 1997-10-21
DE69230569D1 (de) 2000-02-17
CA2062063A1 (en) 1992-09-08
MX9200997A (es) 1992-10-01
CN1150945A (zh) 1997-06-04
CN1067977C (zh) 2001-07-04
KR920018005A (ko) 1992-10-21
EP0502628A3 (en) 1993-01-27
GB9203674D0 (en) 1992-04-08
RU2106337C1 (ru) 1998-03-10
US5877346A (en) 1999-03-02
US5563293A (en) 1996-10-08
ID19108A (id) 1998-06-18
US5527957A (en) 1996-06-18
EP0502628A2 (en) 1992-09-09
EP0754673B1 (en) 2000-01-12
ZA921380B (en) 1993-08-25
CN1038409C (zh) 1998-05-20

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