ES2144143T3 - Proceso de purificacion para productos de hexafluoroetano. - Google Patents

Proceso de purificacion para productos de hexafluoroetano.

Info

Publication number
ES2144143T3
ES2144143T3 ES95932354T ES95932354T ES2144143T3 ES 2144143 T3 ES2144143 T3 ES 2144143T3 ES 95932354 T ES95932354 T ES 95932354T ES 95932354 T ES95932354 T ES 95932354T ES 2144143 T3 ES2144143 T3 ES 2144143T3
Authority
ES
Spain
Prior art keywords
hexafluoroethane
distillation
hcl
azeotropic
sub
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES95932354T
Other languages
English (en)
Inventor
Ralph Newton Miller
Mark Richard Deschere
Barry Asher Mahler
Olagappan Muthu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
EIDP Inc
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Application granted granted Critical
Publication of ES2144143T3 publication Critical patent/ES2144143T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C19/00—Acyclic saturated compounds containing halogen atoms
    • C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/07—Purification ; Separation
    • C01B7/0706—Purification ; Separation of hydrogen chloride
    • C01B7/0712—Purification ; Separation of hydrogen chloride by distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/19—Fluorine; Hydrogen fluoride
    • C01B7/191—Hydrogen fluoride
    • C01B7/195—Separation; Purification
    • C01B7/196—Separation; Purification by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
    • C07C17/386—Separation; Purification; Stabilisation; Use of additives by distillation with auxiliary compounds
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

LA DESCRIPCION SE REFIERE A LA ELIMINACION DE IMPUREZAS DE HEXAFLUOROETANO (CF{SUB,3}CF{SUB,3}), TAMBIEN CONOCIDO COMO PERFLUOROCARBONO 116 (PFC-116), O FLUOROCARBONO 116 (FC-116), UTILIZANDO LA DESTILACION AZEOTROPICA, FORMANDOSE UN PRODUCTO SALIENTE, EN LA PARTE ALTA DE LA COLUMNA DE DESTILACION, CONSISTENTE ESENCIALMENTE EN HCL-HEXAFLUOROETANO. DICHA FASE DE DESTILACION, SE COMBINA OPCIONALMENTE CON UNA ETAPA DE SEPARACION DE FASES, PARA DESCOMPONER EL HCL-HEXAFLUOROETANO AZEOTROPICO, O LA COMPOSICION AZEOTROPICA, PERMITIENDO ASI LA RECUPERACION DE HEXAFLUOROETANO SUSTANCIALMENTE PURO. EL FLUORURO DE HIDROGENO QUE NO HA REACCIONADO (HF), SE PUEDE ELIMINAR A PARTIR DEL HEXAFLUOROETANO DURANTE LA DESTILACION AZEOTROPICA CON HCL ANTERIORMENTE DESCRITA, O, ALTERNATIVAMENTE, MEDIANTE UNA DESTILACION AZEOTROPICA EN CONDICIONES TALES QUE, EN LA PARTE ALTA DE LA COLUMNA SE LIBERA LA COMPOSICION AZEOTROPA O PSEUDOAZEOTROPA DE HCL-HEXAFLUOROETANO, Y, EN EL FLUJO DE BASE SALE HF SUSTANCIALMENTE PURO.
ES95932354T 1994-09-20 1995-09-13 Proceso de purificacion para productos de hexafluoroetano. Expired - Lifetime ES2144143T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/309,376 US5718807A (en) 1994-09-20 1994-09-20 Purification process for hexafluoroethane products

Publications (1)

Publication Number Publication Date
ES2144143T3 true ES2144143T3 (es) 2000-06-01

Family

ID=23197975

Family Applications (1)

Application Number Title Priority Date Filing Date
ES95932354T Expired - Lifetime ES2144143T3 (es) 1994-09-20 1995-09-13 Proceso de purificacion para productos de hexafluoroetano.

Country Status (9)

Country Link
US (3) US5718807A (es)
EP (1) EP0782557B1 (es)
JP (3) JP3811185B2 (es)
KR (1) KR100324063B1 (es)
CN (1) CN1165509A (es)
AU (1) AU3542195A (es)
DE (1) DE69515678T2 (es)
ES (1) ES2144143T3 (es)
WO (1) WO1996009271A1 (es)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2768717B1 (fr) * 1997-09-24 1999-11-12 Solvay Procede de separation de fluorure d'hydrogene de ses melanges avec un hydrofluoroalcane contenant de 3 a 6 atomes de carbone
US5856595A (en) * 1998-03-03 1999-01-05 Alliedsignal Inc. Purified 1,1,1,3,3,3-hexafluoropropane and method for making same
JP4492764B2 (ja) * 1999-05-24 2010-06-30 日本ゼオン株式会社 プラズマ反応用ガス及びその製造方法
JP4703865B2 (ja) * 2001-02-23 2011-06-15 昭和電工株式会社 パーフルオロカーボン類の製造方法およびその用途
CN1301947C (zh) * 2001-02-23 2007-02-28 昭和电工株式会社 全氟化碳的生产方法及其用途
EP2093187A1 (en) * 2001-06-01 2009-08-26 Honeywell International Inc. Process for the Removal of 1,1,1,3,3-Pentafluorobutane
MXPA03010885A (es) * 2001-06-01 2004-02-17 Honeywell Int Inc COMPOSICIONES DE TIPO AZEOTROPO Y PROCESOS PARA LA SEPARACIoN DE PENTAFLUOROETANO Y CLORURO DE HIDRoGENO.
US7329786B2 (en) * 2001-09-28 2008-02-12 Great Lakes Chemical Corporation Processes for producing CF3CFHCF3
US6912872B2 (en) * 2002-08-23 2005-07-05 The Boc Group, Inc. Method and apparatus for producing a purified liquid
US6889508B2 (en) * 2002-10-02 2005-05-10 The Boc Group, Inc. High pressure CO2 purification and supply system
US7223351B2 (en) * 2003-04-17 2007-05-29 Great Lakes Chemical Corporation Fire extinguishing mixtures, methods and systems
US20050011442A1 (en) * 2003-06-24 2005-01-20 International Business Machines Corporation Plasma processing material reclamation and reuse
US20050038302A1 (en) * 2003-08-13 2005-02-17 Hedrick Vicki E. Systems and methods for producing fluorocarbons
US20050077501A1 (en) * 2003-10-14 2005-04-14 Honeywell International, Inc. Azeotrope-like compositions of trifluoroethane and hydrogen fluoride
US20110144395A1 (en) * 2008-08-29 2011-06-16 E.I. Du Pont De Nemours And Company Process to remove hf from 1,1,1,2,2,3,4,5,5,5-decafluoropentane
US9926244B2 (en) * 2008-10-28 2018-03-27 Honeywell International Inc. Process for drying HCFO-1233zd
CN103772136B (zh) * 2012-10-24 2016-02-10 中化蓝天集团有限公司 六氟乙烷的生产工艺
CN103910599B (zh) * 2013-01-06 2017-04-12 中化蓝天集团有限公司 超高纯六氟乙烷的制备方法
US9659787B2 (en) 2013-03-07 2017-05-23 Zeon Corporation High-purity 2-fluorobutane
CN104529692B (zh) * 2015-01-07 2016-04-20 黎明化工研究设计院有限责任公司 一种纯化六氟乙烷的方法
FR3048429B1 (fr) * 2016-03-04 2019-09-27 Arkema France Composition azeotropique ou quasi-azeotropique comprenant de la trifluoropropyne
CN110035988A (zh) * 2016-12-02 2019-07-19 霍尼韦尔国际公司 用于干燥hcfo-1233zd的方法
CN109970509A (zh) * 2017-12-27 2019-07-05 浙江蓝天环保高科技股份有限公司 一种工业级六氟乙烷的提纯方法
US11624556B2 (en) 2019-05-06 2023-04-11 Messer Industries Usa, Inc. Impurity control for a high pressure CO2 purification and supply system
CN114684856B (zh) * 2022-03-07 2024-01-23 中船(邯郸)派瑞特种气体股份有限公司 一种去除六氟化钨中氟化氢的方法及装置
CN116281950B (zh) * 2023-03-31 2025-01-10 大连科利德光电子材料有限公司 碳氟类气体的分离纯化方法
CN121159361A (zh) * 2025-11-21 2025-12-19 山东东岳绿冷科技有限公司 全氟气体的纯化方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3505233A (en) * 1968-11-12 1970-04-07 Union Carbide Corp Chloropentafluoroethane-pentafluoroethane azeotropic compositions
US4365102A (en) * 1980-09-29 1982-12-21 E. I. Du Pont De Nemours And Company Method of manufacturing perfluoromethane and perfluoroethane
US4950364A (en) * 1989-05-04 1990-08-21 Pennwalt Corporation Process for the separation of 1,1-dichloro-1-fluoroethane and 1,1,1,3,3-pentafluorobutane
US5036036A (en) * 1989-06-13 1991-07-30 E. I. Du Pont De Nemours And Company Chromium oxide catalyst composition
US5211867A (en) * 1989-06-28 1993-05-18 Allied-Signal Inc. Azeotrope-like compositions of pentafluoroethane and 1,1,1-trifluoroethane
GB9105407D0 (en) * 1991-03-14 1991-05-01 Ici Plc Separation process
US5087329A (en) * 1991-05-16 1992-02-11 E. I. Du Pont De Nemours And Company Process for separating pentafluoroethane from a mixture of halogenated hydrocarbons containing chloropentafluoroethane
JPH0532568A (ja) * 1991-07-31 1993-02-09 Daikin Ind Ltd フツ化水素とジクロロフルオロメタンの混合物からフツ化水素を除去する方法
US5196616A (en) * 1991-10-18 1993-03-23 E. I. Du Pont De Nemours And Company Process for separating and recovering fluorocarbons and hydrogen fluoride from mixtures thereof
JPH05255144A (ja) * 1991-11-15 1993-10-05 Hoechst Ag 弗化水素および１−クロロ−２，２，２−トリフルオロエタンを含有する混合物の分離方法
JP2661441B2 (ja) * 1991-11-27 1997-10-08 ダイキン工業株式会社 １，１，１−トリフルオロ−２−クロロエタンおよび／または１，１，１，２−テトラフルオロエタンの製法
JPH05178768A (ja) * 1991-12-16 1993-07-20 Showa Denko Kk １，１，１，２−テトラフルオロエタンとフッ化水素の分離方法
US5523499A (en) * 1992-03-10 1996-06-04 E. I. Du Pont De Nemours And Company Purification of hexafluoroethane products
KR100352680B1 (ko) * 1992-04-13 2002-09-16 다이낑 고오교 가부시키가이샤 플루오르화수소의 제거 방법
JP3182869B2 (ja) * 1992-05-18 2001-07-03 ダイキン工業株式会社 ペンタフルオロエタンとペンタフルオロクロロエタンとの共沸混合物およびペンタフルオロクロロエタンの分離方法
GB9311742D0 (en) * 1992-06-10 1993-07-21 Ici Plc Production of hydrofluoroalkanes
US5258561A (en) * 1992-11-06 1993-11-02 E. I. Du Pont De Nemours And Company Catalytic chlorofluorination process for producing CF3 CHClF and CF3 CHF2
US5346595A (en) * 1993-02-23 1994-09-13 Alliedsignal Inc. Process for the purification of a pentafluoroethane azeotrope
FR2701943B1 (fr) * 1993-02-24 1995-05-12 Atochem Elf Sa Purification du pentafluoroéthane.
US5421964A (en) * 1993-04-30 1995-06-06 E. I. Du Pont De Nemours And Company Process for separating HCl and halocarbons
US5340490A (en) * 1993-07-14 1994-08-23 Alliedsignal Inc. Azeotrope-like compositions of trifluoromethane and carbon dioxide or hexafluoroethane and carbon dioxide
US5928479A (en) * 1994-04-08 1999-07-27 Imperial Chemical Industries Plc Process for the purification of pentafluoroethane

Also Published As

Publication number Publication date
EP0782557A1 (en) 1997-07-09
US6221830B1 (en) 2001-04-24
JP3811185B2 (ja) 2006-08-16
AU3542195A (en) 1996-04-09
JPH10506107A (ja) 1998-06-16
JP5049320B2 (ja) 2012-10-17
US5718807A (en) 1998-02-17
EP0782557B1 (en) 2000-03-15
WO1996009271A1 (en) 1996-03-28
JP2006249437A (ja) 2006-09-21
KR100324063B1 (ko) 2002-11-27
US5723699A (en) 1998-03-03
JP4463230B2 (ja) 2010-05-19
JP2009221228A (ja) 2009-10-01
DE69515678D1 (de) 2000-04-20
DE69515678T2 (de) 2000-11-09
CN1165509A (zh) 1997-11-19

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