ES2154873T3 - Procedimiento para la preparacion continua de metilmercaptano. - Google Patents
Procedimiento para la preparacion continua de metilmercaptano.Info
- Publication number
- ES2154873T3 ES2154873T3 ES97121628T ES97121628T ES2154873T3 ES 2154873 T3 ES2154873 T3 ES 2154873T3 ES 97121628 T ES97121628 T ES 97121628T ES 97121628 T ES97121628 T ES 97121628T ES 2154873 T3 ES2154873 T3 ES 2154873T3
- Authority
- ES
- Spain
- Prior art keywords
- heat
- reaction
- methylmercaptane
- procedure
- gas mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title abstract 2
- LSDPWZHWYPCBBB-UHFFFAOYSA-N methyl mercaptane Natural products SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 6
- 238000006243 chemical reaction Methods 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 abstract 2
- 239000007789 gas Substances 0.000 abstract 2
- 229910000037 hydrogen sulfide Inorganic materials 0.000 abstract 2
- 238000006555 catalytic reaction Methods 0.000 abstract 1
- 230000006835 compression Effects 0.000 abstract 1
- 238000007906 compression Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C319/00—Preparation of thiols, sulfides, hydropolysulfides or polysulfides
- C07C319/02—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols
- C07C319/08—Preparation of thiols, sulfides, hydropolysulfides or polysulfides of thiols by replacement of hydroxy groups or etherified or esterified hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
LA PRESENTE INVENCION TRATA DE UN PROCEDIMIENTO PARA LA FABRICACION CONTINUA DE METILMERCAPTANO MEDIANTE REACCION CATALITICA DE METANOL Y SULFURO DE HIDROGENO. LA INVENCION INCLUYE PERFECCIONAMIENTOS IMPORTANTES EN LO REFERENTE A LA PREPARACION DE LA MEZCLA DE GAS DE EDUCTOS, ASI COMO EN LO REFERENTE AL APROVECHAMIENTO DEL CALOR DE LA REACCION Y DE LA TERMICIDAD DE LA MEZCLA DE GAS DE PRODUCTOS. LA ENERGIA NECESARIA PARA LA EVAPORACION DEL METANOL SE APLICA EN PARTE APROVECHANDO EL CALOR DE COMPRESION DEL SULFURO DE HIDROGENO, ASI COMO MEDIANTE LA TERMICIDAD DEL GAS DE PRODUCTOS QUE ABANDONA EL REACTOR. EL CALOR DE LA REACCION SE APROVECHA PARA CALENTAR LA MEZCLA DE GAS DE EDUCTOS HASTA LA TEMPERATURA DE REACCION CON LA AYUDA DE UN CALENTADOR DE GAS.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19654515A DE19654515C1 (de) | 1996-12-27 | 1996-12-27 | Verfahren zur kontinuierlichen Herstellung von Methylmercaptan |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2154873T3 true ES2154873T3 (es) | 2001-04-16 |
Family
ID=7816317
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES97121628T Expired - Lifetime ES2154873T3 (es) | 1996-12-27 | 1997-12-09 | Procedimiento para la preparacion continua de metilmercaptano. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5886230A (es) |
| EP (1) | EP0850922B1 (es) |
| JP (1) | JP3893206B2 (es) |
| CN (1) | CN1186067A (es) |
| BR (1) | BR9706465A (es) |
| DE (2) | DE19654515C1 (es) |
| ES (1) | ES2154873T3 (es) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6403684B1 (en) * | 1998-12-16 | 2002-06-11 | General Electric Company | Polyetherimide resin/polyester resin blends having improved visual clarity |
| RU2157366C1 (ru) * | 1999-03-10 | 2000-10-10 | Наумейко Анатолий Васильевич | Способ производства метилмеркаптана, способ получения катализатора для производства метилмеркаптана и способ получения сероводорода для производства метилмеркаптана |
| WO2001010776A1 (en) | 1999-08-05 | 2001-02-15 | Novus International, Inc. | Reductive combustion of ammonium salts of sulfuric acid |
| DE10338887A1 (de) * | 2003-08-23 | 2005-03-17 | Degussa Ag | Katalysator zur Synthese von Alkylmercaptan und Verfahren zu seiner Herstellung |
| RU2394023C2 (ru) | 2003-10-10 | 2010-07-10 | Эвоник Дегусса Гмбх | Способ получения метилмеркаптана |
| DE10359636A1 (de) * | 2003-12-18 | 2005-07-28 | Degussa Ag | Verfahren zur Abtrennung von Methylmercaptan aus Reaktionsgemischen |
| DE102005016369A1 (de) * | 2005-04-09 | 2006-10-12 | Degussa Ag | Verfahren zur kontinuierlichen Herstellung von Methylmercaptan |
| NO324110B1 (no) * | 2005-07-05 | 2007-08-27 | Aker Subsea As | System og fremgangsmate for rengjoring av kompressor, for a hindre hydratdannelse og/eller for a oke kompressorytelsen. |
| DE102005043151A1 (de) * | 2005-09-10 | 2007-03-22 | Degussa Ag | Verfahren zur Herstellung von Methylmercaptan |
| DE102006032635A1 (de) * | 2006-07-13 | 2008-01-17 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Alkylmercaptanen in einem Mehrzonenfestbettreaktor |
| EP1982764A1 (en) | 2007-04-17 | 2008-10-22 | Evonik Degussa GmbH | Catalyst for the preparation of methyl mercaptan |
| SG171866A1 (en) | 2008-12-23 | 2011-07-28 | Basf Se | Method for compressing gases containing hydrogen sulfide |
| KR20130029064A (ko) * | 2010-03-18 | 2013-03-21 | 바스프 에스이 | 이소시아네이트의 제조 방법 |
| DE102010064250A1 (de) | 2010-12-28 | 2012-06-28 | Evonik Degussa Gmbh | Verfahren zur Herstellung von Methylmercaptopropionaldehyd |
| EP2765127A1 (de) | 2013-02-06 | 2014-08-13 | Evonik Industries AG | Verfahren zur Abtrennung von Acrolein aus dem Prozessgas einer heterogen katalysierten Oxidation von Propen |
| CA3020740A1 (en) | 2016-05-31 | 2017-12-07 | Novus International Inc. | Process for producing methyl mercaptan from dimethyl sulfide |
| CN112552217A (zh) * | 2020-12-26 | 2021-03-26 | 查都(海南)科技有限公司 | 一种甲硫醇提纯装置 |
| CN112979516B (zh) * | 2021-04-20 | 2023-12-08 | 查都(海南)科技有限公司 | 一种节能的甲硫醇合成装置 |
| CN113149877A (zh) * | 2021-04-26 | 2021-07-23 | 新疆兴发化工有限公司 | 一种二甲基硫醚的生产工艺 |
| CN114478334B (zh) * | 2022-02-25 | 2023-11-10 | 新疆广汇陆友硫化工有限公司 | 一种甲硫醇硫化法生产二甲基二硫的方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2822401A (en) * | 1955-06-22 | 1958-02-04 | American Oil Co | Methyl mercaptan production process |
| GB810017A (en) * | 1957-02-19 | 1959-03-04 | Arthur Abbey | Improvements in and relating to the manufacture of methyl sulphide and methyl mercaptan |
| US3547983A (en) * | 1967-06-29 | 1970-12-15 | Air Reduction | Preparation of unsaturated esters |
| DE1768826B1 (de) * | 1968-07-04 | 1971-08-26 | Degussa | Verfahren zur Gewinnung von niederen aliphatischen Mercaptanen |
| FR2253013B1 (es) * | 1973-11-30 | 1980-01-04 | Rhone Progil | |
| FR2477538A2 (fr) * | 1980-03-06 | 1981-09-11 | Rhone Poulenc Ind | Procede de preparation de methylmercaptan a partir d'hydrogene sulfure et de methanol |
-
1996
- 1996-12-27 DE DE19654515A patent/DE19654515C1/de not_active Expired - Fee Related
-
1997
- 1997-06-30 US US08/885,044 patent/US5886230A/en not_active Expired - Lifetime
- 1997-12-09 ES ES97121628T patent/ES2154873T3/es not_active Expired - Lifetime
- 1997-12-09 DE DE59703011T patent/DE59703011D1/de not_active Expired - Lifetime
- 1997-12-09 EP EP97121628A patent/EP0850922B1/de not_active Expired - Lifetime
- 1997-12-25 JP JP35662197A patent/JP3893206B2/ja not_active Expired - Fee Related
- 1997-12-26 CN CN97123454A patent/CN1186067A/zh active Pending
- 1997-12-26 BR BR9706465A patent/BR9706465A/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JP3893206B2 (ja) | 2007-03-14 |
| DE59703011D1 (de) | 2001-03-29 |
| US5886230A (en) | 1999-03-23 |
| DE19654515C1 (de) | 1998-10-01 |
| BR9706465A (pt) | 1999-06-01 |
| MX9710336A (es) | 1998-06-30 |
| JPH10195040A (ja) | 1998-07-28 |
| EP0850922B1 (de) | 2001-02-21 |
| CN1186067A (zh) | 1998-07-01 |
| EP0850922A1 (de) | 1998-07-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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