ES2170224T3 - Procedimiento para preparar haluros de alilo. - Google Patents

Procedimiento para preparar haluros de alilo.

Info

Publication number
ES2170224T3
ES2170224T3 ES96908591T ES96908591T ES2170224T3 ES 2170224 T3 ES2170224 T3 ES 2170224T3 ES 96908591 T ES96908591 T ES 96908591T ES 96908591 T ES96908591 T ES 96908591T ES 2170224 T3 ES2170224 T3 ES 2170224T3
Authority
ES
Spain
Prior art keywords
area
reactor
alilo
ovoform
oval
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96908591T
Other languages
English (en)
Other versions
ES2170224T5 (es
Inventor
Max M Tirtowidjojo
Paul C Beckett
John F Baker
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Chemical Co
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=23784905&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2170224(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of ES2170224T3 publication Critical patent/ES2170224T3/es
Application granted granted Critical
Publication of ES2170224T5 publication Critical patent/ES2170224T5/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/0066—Stirrers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/0073—Sealings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/04—Chloro-alkenes
    • C07C21/067—Allyl chloride; Methallyl chloride
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B01J2219/00063—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/0015—Controlling the temperature by thermal insulation means
    • B01J2219/00155—Controlling the temperature by thermal insulation means using insulating materials or refractories
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1942—Details relating to the geometry of the reactor round circular or disk-shaped spherical
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/141—Feedstock

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

SE PRODUCE CLORURO DE ALILO CON ALTOS RENDIMIENTOS Y PUREZA Y MINIMA FORMACION DE CARBON UTILIZANDO UN PROCESO DE: (1) INICIALMENTE HACER REACCIONAR PROPILENO Y HALOGENO MOLECULAR EN UNA RELACION MOLAR DE AL MENOS 2.5:1 EN UNA ZONA DE "REACTOR DE TANQUE CON AGITACION CONTINUA" (CSTR) BAJO LAS CONDICIONES ADECUADAS PARA PROPORCIONAR UNA TEMPERATURA DE REACCION DE 400 (GRADOS) C A 525 (GRADOS) C PARA CONVERTIR PARCIALMENTE PROPILENO Y CLORO A CLORURO DE ALILO, Y (2) ALIMENTAR UN EFLUENTE DEL PASO (1) A UNA ZONA DE REACTOR DE FLUJO DE PISTON DONDE LA REACCION CONTINUA A UNA TEMPERATURA DE 400 (GRADOS) C A 525 (GRADOS) C HASTA QUE SE CONSUME ESENCIALMENTE TODO EL CLORO. UN REACTOR PREFERIDO PARA EL PROCESO CONTIENE: (1) UNA ZONA DE REACTOR ESFERICA, OVAL U OVOFORME; (2) UNA ZONA DE REACTOR TUBULAR ADJUNTA A LA ZONA DE REACTOR ESFERICA, OVAL U OVOFORME; (3) UNA O MAS ENTRADAS PARA INYECTAR REACTIVOS GASEOSOS EN LA ZONA DE REACTOR ESFERICA, OVAL U OVOFORME; Y (4) UNA O MAS SALIDAS EN LA ZONA DE REACTOR TUBULAR PARA LA RETIRADA DEL PRODUCTO GASEOSO.
ES96908591T 1995-05-24 1996-02-27 Procedimiento para preparar haluros de alilo. Expired - Lifetime ES2170224T5 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/449,635 US5504266A (en) 1995-05-24 1995-05-24 Process to make allyl chloride and reactor useful in that process
US449635 1995-05-24

Publications (2)

Publication Number Publication Date
ES2170224T3 true ES2170224T3 (es) 2002-08-01
ES2170224T5 ES2170224T5 (es) 2006-11-16

Family

ID=23784905

Family Applications (1)

Application Number Title Priority Date Filing Date
ES96908591T Expired - Lifetime ES2170224T5 (es) 1995-05-24 1996-02-27 Procedimiento para preparar haluros de alilo.

Country Status (12)

Country Link
US (1) US5504266A (es)
EP (2) EP1018366B1 (es)
JP (1) JP4047381B2 (es)
KR (1) KR100415889B1 (es)
CN (1) CN1080712C (es)
CZ (1) CZ291902B6 (es)
DE (2) DE69631493T2 (es)
ES (1) ES2170224T5 (es)
PL (1) PL192831B1 (es)
RU (1) RU2162459C2 (es)
TW (1) TW334417B (es)
WO (1) WO1996037450A1 (es)

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US5552131A (en) * 1994-06-30 1996-09-03 Arco Chemical Technology, L.P. Oxidation of secondary alcohols
US6004517A (en) * 1995-05-24 1999-12-21 The Dow Chemical Company Process to make allyl chloride and reactor useful in that process
DE69703735T2 (de) * 1996-04-26 2001-05-31 Exxon Chemical Patents Inc., Linden Verfahren zur herstellung von hydroxycarbonylverbindungen
EP0977718B1 (en) * 1997-04-25 2002-04-10 Resolution Research Nederland B.V. Process for manufacturing allylhalide and equipment to be used therefor
US5986022A (en) * 1998-04-01 1999-11-16 Witco Corporation Continuous manufacture of silicone coploymers
RU2163904C1 (ru) * 1999-11-16 2001-03-10 Закрытое акционерное общество "Каустик" Реактор для получения аллилхлорида
WO2010045104A2 (en) 2008-10-13 2010-04-22 Dow Global Technologies, Inc. Process for the production of chlorinated and/or fluorinated propenes
KR20120093202A (ko) 2009-10-09 2012-08-22 다우 글로벌 테크놀로지스 엘엘씨 단열식 플러그 흐름 반응기 및 염화 및/또는 불화 프로펜 및 고급 알켄의 제조 방법
EP2485996B1 (en) 2009-10-09 2016-06-15 Blue Cube IP LLC Process for the production of chlorinated and/or fluorinated propenes
JP5767231B2 (ja) 2009-10-09 2015-08-19 ダウ グローバル テクノロジーズ エルエルシー 塩素化及び／又はフッ素化されたプロペン及びより高級なアルケンを製造するプロセス
JP5782038B2 (ja) 2009-10-09 2015-09-24 ダウ グローバル テクノロジーズ エルエルシー 等温多管式反応器及び該反応器を組み込んだプロセス
US9056808B2 (en) 2011-05-31 2015-06-16 Dow Global Technologies, Llc Process for the production of chlorinated propenes
CN103562164B (zh) 2011-05-31 2016-04-20 陶氏环球技术有限责任公司 生产氯化丙烯类的方法
KR102007722B1 (ko) 2011-06-08 2019-08-07 다우 글로벌 테크놀로지스 엘엘씨 염화 및/또는 불화 프로펜의 제조 방법
US8907148B2 (en) 2011-08-07 2014-12-09 Dow Global Technologies Llc Process for the production of chlorinated propenes
CN103717557A (zh) 2011-08-07 2014-04-09 陶氏环球技术有限责任公司 生产氯化的丙烯的方法
IN2014CN03748A (es) 2011-11-21 2015-09-25 Dow Global Technologies Llc
EP2785671B1 (en) 2011-12-02 2017-03-01 Blue Cube IP LLC Process for the production of chlorinated propanes
JP6059246B2 (ja) 2011-12-02 2017-01-11 ブルー キューブ アイピー エルエルシー 塩素化アルカンの製造方法
JP6170068B2 (ja) 2011-12-13 2017-07-26 ブルー キューブ アイピー エルエルシー 塩素化プロパン及びプロペンの製造方法
CN104011000A (zh) 2011-12-22 2014-08-27 陶氏环球技术有限责任公司 生产四氯甲烷的方法
BR112014015123A2 (pt) 2011-12-23 2017-06-13 Dow Global Technologies Llc processo para a produção de um ou mais alcenos ou compostos aromáticos
EP2897930A1 (en) 2012-09-20 2015-07-29 Dow Global Technologies LLC Process for the production of chlorinated propenes
EP2897932A1 (en) 2012-09-20 2015-07-29 Dow Global Technologies LLC Process for the production of chlorinated propenes
JP6272878B2 (ja) 2012-09-30 2018-01-31 ブルー キューブ アイピー エルエルシー せきクエンチおよびそれを組み込んだ方法
EP2911773B1 (en) 2012-10-26 2017-10-04 Blue Cube IP LLC Mixer and reactor and process incorporating the same
CA2893841C (en) 2012-12-18 2018-07-24 Dow Global Technologies Llc Process for the production of chlorinated propenes
WO2014100039A1 (en) 2012-12-19 2014-06-26 Dow Global Technologies, Llc Process for the production of chlorinated propenes
JP2016507590A (ja) 2013-02-27 2016-03-10 ブルー キューブ アイピー エルエルシー 塩素化プロペンを生成するための方法
WO2014164368A1 (en) 2013-03-09 2014-10-09 Dow Global Technologies Llc Process for the production of chlorinated alkanes
CN103724157A (zh) * 2013-12-19 2014-04-16 山东海益化工科技有限公司 一种氯丙烯生产中的氯化工艺
CN103724155B (zh) * 2013-12-19 2015-08-19 山东海益化工科技有限公司 一种氯丙烯的生产工艺
CN103664505B (zh) * 2013-12-24 2015-06-24 山东海益化工科技有限公司 一种氯丙烯生产工艺
US9416073B2 (en) * 2014-10-06 2016-08-16 Honeywell International Inc. Method to improve halogenation reactions
CN104876792A (zh) * 2015-05-21 2015-09-02 山东海益化工科技有限公司 一种生产高纯度氯丙烯的方法
CN104876793A (zh) * 2015-05-21 2015-09-02 山东海益化工科技有限公司 一种氯丙烯的精制工艺
KR102371372B1 (ko) * 2017-12-01 2022-03-04 한화솔루션 주식회사 프로필렌의 기상 염소화 반응 장치
CN110003962B (zh) * 2019-05-06 2021-04-30 沈阳航空航天大学 一种轴向固定床甲烷化反应器
CN111285752A (zh) * 2020-03-23 2020-06-16 山东凯泰科技股份有限公司 一种氯丙烯生产用多级换热反应系统
KR102930262B1 (ko) * 2023-08-18 2026-02-23 한화솔루션 주식회사 염화 알릴 제조용 반응기

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Also Published As

Publication number Publication date
EP0837841B2 (en) 2006-05-03
RU2162459C2 (ru) 2001-01-27
CZ367697A3 (cs) 1998-05-13
CZ291902B6 (cs) 2003-06-18
EP0837841A1 (en) 1998-04-29
JPH11505834A (ja) 1999-05-25
PL192831B1 (pl) 2006-12-29
DE69631493D1 (de) 2004-03-11
PL323466A1 (en) 1998-03-30
KR100415889B1 (ko) 2004-06-26
CN1080712C (zh) 2002-03-13
EP1018366A2 (en) 2000-07-12
KR19990021869A (ko) 1999-03-25
DE69619820T3 (de) 2006-12-07
US5504266A (en) 1996-04-02
EP1018366A3 (en) 2000-07-26
CN1188466A (zh) 1998-07-22
DE69619820T2 (de) 2002-09-12
DE69631493T2 (de) 2004-12-23
TW334417B (en) 1998-06-21
ES2170224T5 (es) 2006-11-16
WO1996037450A1 (en) 1996-11-28
EP0837841B1 (en) 2002-03-13
JP4047381B2 (ja) 2008-02-13
DE69619820D1 (de) 2002-04-18
EP1018366B1 (en) 2004-02-04

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