ES2177986T3 - Procedimiento de fabricacion de 2,3-dihalopropanoles. - Google Patents

Procedimiento de fabricacion de 2,3-dihalopropanoles.

Info

Publication number
ES2177986T3
ES2177986T3 ES97929694T ES97929694T ES2177986T3 ES 2177986 T3 ES2177986 T3 ES 2177986T3 ES 97929694 T ES97929694 T ES 97929694T ES 97929694 T ES97929694 T ES 97929694T ES 2177986 T3 ES2177986 T3 ES 2177986T3
Authority
ES
Spain
Prior art keywords
epihalohidrine
dihalopropanol
dihalopropanal
make
react
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97929694T
Other languages
English (en)
Inventor
P J Thomas
R Garth Pews
Paul C Vosejpka
George J Frycek
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Chemical Co
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Application granted granted Critical
Publication of ES2177986T3 publication Critical patent/ES2177986T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/24—Synthesis of the oxirane ring by splitting off HAL—Y from compounds containing the radical HAL—C—C—OY
    • C07D301/26—Y being hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/14—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group
    • C07C29/141—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of a —CHO group with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/63—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of halogen; by substitution of halogen atoms by other halogen atoms
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Abstract

UN 2,3 - DIHALOPROPANOL SE OBTIENE HACIENDO REACCIONAR 2,3 DIHALOPROPANAL CON UN AGENTE DE HIDROGENACION, EN PRESENCIA DE UN CATALIZADOR QUE CONTIENE UN METAL DE TRANSICION, EN CONDICIONES TALES QUE HACEN QUE SE FORME EL 2,3 DIHALOPROPANOL. LA REACCION ES PARTICULARMENTE UTIL, POR EJEMPLO, COMO PASO (3) EN UN PROCESO PARA OBTENER EPIHALOHIDRINA, QUE PODRIA PREPARARSE GENERALMENTE DEL SIGUIENTE MODO: (1) HACER REACCIONAR UN HIDROCARBURO DE 3 ATOMOS DE CARBONO CON UN AGENTE OXIDANTE, PARA OBTENER ACROLEINA; (2) HACER REACCIONAR ACROLEINA CON UN HALOGENO MOLECULAR PARA OBTENER 2,3 - DIHALOPROPANAL; (3) REDUCIR EL 2,3 DIHALOPROPANAL PARA FORMAR 2,3 - DIHALOPROPANOL; Y (4) SOMETER A VARIOS CICLOS EL 2,3 - DIHALOPROPANOL PARA OBTENER EPIHALOHIDRINA. EL PROCESO PRODUCE EPIHALOHIDRINA USANDOSE UNICAMENTE ALREDEDOR DE UN MOL DE HALOGENO POR MOL DE EPIHALOHIDRINA Y UTILIZA TAMBIEN UNA CANTIDAD MUCHO MENOR DE AGUA QUE LOS ACTUALES PROCESOS.
ES97929694T 1996-06-19 1997-06-05 Procedimiento de fabricacion de 2,3-dihalopropanoles. Expired - Lifetime ES2177986T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/667,526 US5744655A (en) 1996-06-19 1996-06-19 Process to make 2,3-dihalopropanols

Publications (1)

Publication Number Publication Date
ES2177986T3 true ES2177986T3 (es) 2002-12-16

Family

ID=24678573

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97929694T Expired - Lifetime ES2177986T3 (es) 1996-06-19 1997-06-05 Procedimiento de fabricacion de 2,3-dihalopropanoles.

Country Status (8)

Country Link
US (2) US5744655A (es)
EP (1) EP0918738B1 (es)
JP (1) JP4283343B2 (es)
CN (1) CN1092173C (es)
DE (1) DE69713894T2 (es)
ES (1) ES2177986T3 (es)
PL (1) PL330753A1 (es)
WO (1) WO1997048667A1 (es)

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PL1772446T3 (pl) * 2003-11-20 2011-03-31 Solvay Proces wytwarzania związków organicznych z gliceryny, pochodzącej z surowców odnawialnych
JP4638482B2 (ja) * 2004-03-31 2011-02-23 ダウ グローバル テクノロジーズ インコーポレイティド １，３−ジクロロアセトンの製造方法
US20080021229A1 (en) * 2004-05-21 2008-01-24 Maughon Bob R Process for Preparing Epichlorhydrin from Ethane
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EA013681B1 (ru) * 2005-05-20 2010-06-30 Солвей (Сосьете Аноним) Способ получения дихлорпропанола, способ получения эпихлоргидрина и способ получения эпоксидных смол
CN101068761B (zh) 2005-11-08 2011-11-23 索尔维公司 通过甘油的氯化制备二氯丙醇的方法
EP2043984A1 (en) 2006-06-14 2009-04-08 Solvay S.A. Crude glycerol-based product, process for its purification and its use in the manufacture of dichloropropanol
US20100032617A1 (en) * 2007-02-20 2010-02-11 Solvay (Societe Anonyme) Process for manufacturing epichlorohydrin
FR2913421B1 (fr) * 2007-03-07 2009-05-15 Solvay Procede de fabrication de dichloropropanol.
FR2913684B1 (fr) * 2007-03-14 2012-09-14 Solvay Procede de fabrication de dichloropropanol
TW200911740A (en) 2007-06-01 2009-03-16 Solvay Process for manufacturing a chlorohydrin
TW200911693A (en) 2007-06-12 2009-03-16 Solvay Aqueous composition containing a salt, manufacturing process and use
TWI500609B (zh) * 2007-06-12 2015-09-21 Solvay 含有環氧氯丙烷的產品，其製備及其不同應用中的用途
FR2918058A1 (fr) * 2007-06-28 2009-01-02 Solvay Produit a base de glycerol, procede pour sa purification et son utilisation dans la fabrication de dichloropropanol
KR20100089835A (ko) 2007-10-02 2010-08-12 솔베이(소시에떼아노님) 용기의 내부식성 향상을 위한 실리콘-함유 조성물의 용도
FR2925045B1 (fr) 2007-12-17 2012-02-24 Solvay Produit a base de glycerol, procede pour son obtention et son utilisation dans la fabrication de dichloropropanol
TWI478875B (zh) * 2008-01-31 2015-04-01 Solvay 使水性組成物中之有機物質降解之方法
WO2009121853A1 (en) 2008-04-03 2009-10-08 Solvay (Société Anonyme) Composition comprising glycerol, process for obtaining same and use thereof in the manufacture of dichloropropanol
KR20090128886A (ko) * 2008-06-11 2009-12-16 삼성정밀화학 주식회사 무용매 상태하에서, 그리고 헤테로폴리산 촉매 및/또는흡수제의 존재하에서 글리세롤로부터 디클로로프로판올을제조하는 방법
FR2935968B1 (fr) 2008-09-12 2010-09-10 Solvay Procede pour la purification de chlorure d'hydrogene
CN107759771A (zh) 2010-09-30 2018-03-06 索尔维公司 天然来源的环氧氯丙烷的衍生物
CN102766070B (zh) * 2012-04-26 2014-06-18 江苏克胜集团股份有限公司 一种制备哌虫啶中间体的前体2-氯-2-氯甲基-4-氰基丁醛的方法
EP2669247A1 (en) 2012-06-01 2013-12-04 Solvay Sa Process for manufacturing dichloropropanol
EP2669307A1 (en) 2012-06-01 2013-12-04 Solvay Sa Process for manufacturing an epoxide
EP2669306B1 (en) 2012-06-01 2015-08-12 Solvay Sa Process for manufacturing an epoxy resin
EP2669305A1 (en) 2012-06-01 2013-12-04 Solvay Sa Process for manufacturing an epoxy resin
EP2669308A1 (en) 2012-06-01 2013-12-04 Solvay Sa Process for manufacturing an epoxy resin
KR102090992B1 (ko) 2013-11-20 2020-03-20 솔베이(소시에떼아노님) 에폭시 수지의 제조 방법
CN103641684B (zh) * 2013-12-18 2016-04-06 绍兴文理学院 高纯度氯乙醇及其制备方法
CN104030890B (zh) * 2014-06-30 2015-10-21 重庆科技学院 一种制备对苯二酚的方法
CN110437820B (zh) * 2019-08-15 2021-06-15 山东滨州昱诚化工科技有限公司 一种油田压裂酸化用防乳化剂的制备方法及其应用

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Also Published As

Publication number Publication date
EP0918738B1 (en) 2002-07-10
CN1092173C (zh) 2002-10-09
JP2000512654A (ja) 2000-09-26
PL330753A1 (en) 1999-05-24
CN1222136A (zh) 1999-07-07
US6008419A (en) 1999-12-28
JP4283343B2 (ja) 2009-06-24
EP0918738A1 (en) 1999-06-02
DE69713894D1 (de) 2002-08-14
WO1997048667A1 (en) 1997-12-24
US5744655A (en) 1998-04-28
DE69713894T2 (de) 2003-02-06

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