ES2180955T3 - Procedimiento para la separacion de isomeros de isocianatos. - Google Patents

Procedimiento para la separacion de isomeros de isocianatos.

Info

Publication number
ES2180955T3
ES2180955T3 ES97913174T ES97913174T ES2180955T3 ES 2180955 T3 ES2180955 T3 ES 2180955T3 ES 97913174 T ES97913174 T ES 97913174T ES 97913174 T ES97913174 T ES 97913174T ES 2180955 T3 ES2180955 T3 ES 2180955T3
Authority
ES
Spain
Prior art keywords
isomers
separation
isocianates
procedure
crystals
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97913174T
Other languages
English (en)
Inventor
Rudiger Drope
Dieter Grenner
Hartmut Hetzel
Hans-Peter Schal
Gerhard Wegener
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Application granted granted Critical
Publication of ES2180955T3 publication Critical patent/ES2180955T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C263/00—Preparation of derivatives of isocyanic acid
    • C07C263/18—Separation; Purification; Stabilisation; Use of additives
    • C07C263/20—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)

Abstract

LA INVENCION SE REFIERE A UN PROCESO PARA LA OBTENCION DE ISOMEROS DE ISOCIANATOS PUROS A PARTIR DE UNA MEZCLA DE ISOMEROS DE ISOCIANATOS POR CRISTALIZACION EN SUSPENSION Y SEPARACION DE CRISTALES ISOMERICAMENTE PUROS. EL PROCESO SE CARACTERIZA PORQUE, ANTES DE LA SEPARACION DE LOS CRISTALES, SE FUSIONAN DE NUEVO ENTRE UN 5 Y UN 40% EN PESO DE LOS CRISTALES PRODUCIDOS, MIENTRAS SE AUMENTA SIMULTANEAMENTE LA TEMPERATURA DE LA SUSTANCIA CRISTALINA ENTRE 4,5 Y 9 C.
ES97913174T 1996-11-06 1997-10-24 Procedimiento para la separacion de isomeros de isocianatos. Expired - Lifetime ES2180955T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19645659A DE19645659A1 (de) 1996-11-06 1996-11-06 Verfahren zur Isomerentrennung von Isocyanaten

Publications (1)

Publication Number Publication Date
ES2180955T3 true ES2180955T3 (es) 2003-02-16

Family

ID=7810756

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97913174T Expired - Lifetime ES2180955T3 (es) 1996-11-06 1997-10-24 Procedimiento para la separacion de isomeros de isocianatos.

Country Status (9)

Country Link
US (1) US6271414B1 (es)
EP (1) EP0937033B1 (es)
JP (1) JP2001503419A (es)
AU (1) AU5051798A (es)
BR (1) BR9712749A (es)
DE (2) DE19645659A1 (es)
ES (1) ES2180955T3 (es)
TW (1) TW402584B (es)
WO (1) WO1998019993A1 (es)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10322439A1 (de) * 2003-05-19 2004-12-09 Bayer Ag Verfahren und Vorrichtung zur Bestimmung der Isomerenzusammensetzung bei Isocyanat-Herstellprozessen
DE102004018048A1 (de) * 2004-04-08 2005-11-10 Henkel Kgaa Verfahren zur Herstellung von Polyurethan-Prepolymeren
CN108479103A (zh) * 2018-05-28 2018-09-04 浙江东瓯过滤机制造有限公司 一种带搅拌过滤浓缩装置及其搅拌过滤浓缩方法
CN109970604B (zh) * 2019-04-25 2021-03-19 青岛科技大学 一种提纯2,4-甲苯二异氰酸酯的工艺

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3144474A (en) * 1964-08-11 Purification process for isocyanates
US2831012A (en) * 1957-03-29 1958-04-15 Du Pont Chemical process
US3232069A (en) * 1962-02-01 1966-02-01 Phillips Petroleum Co Cooling control in fractional crystal-lization responsive to solids measurement
US3217024A (en) * 1963-03-22 1965-11-09 Allied Chem Conversion of mixtures of 2, 4-and 2, 6-toluene diisocyanates to other mixtures of different isomer ratio
US3591617A (en) * 1968-03-07 1971-07-06 Lummus Co Purification of toluene diisocyanate
US4004886A (en) 1969-12-12 1977-01-25 Stamicarbon B.V. Two stage continuous process and apparatus for crystallization
US3777892A (en) 1971-01-27 1973-12-11 H Thijssen Apparatus for the separation and treatment of solid particles from a liquid suspension
US3872009A (en) * 1971-06-25 1975-03-18 Henricus Alexis Corne Thijssen Apparatus for the separation and treatment of solid particles from a liquid suspension
US4246187A (en) * 1979-07-17 1981-01-20 E. I. Du Pont De Nemours And Company Separation of 2,4-tolylene diisocyanate from mixtures of 2,4- and 2,6-tolylene diisocyanate
US4459144A (en) 1980-10-30 1984-07-10 Grasso's Koniklijke Machine Fabrieken, N.V. Multi-stage counter-current concentration system and method
US4430104A (en) 1980-10-30 1984-02-07 Grasso's Koniklijke Machine Fabrieken, N.V. Multi-stage countercurrent concentrating system and method and separator
US4316368A (en) 1980-10-30 1982-02-23 Grasso's Koniklijke Machinefabrieken, N.V. Multi-stage counter-current concentrating method
DE3220439A1 (de) * 1982-05-29 1983-12-01 Bayer Ag, 5090 Leverkusen Verfahren zur abtrennung von technisch reinem 2,4-diisocyanatotoluol oder von, einen erhoehten gehalt an 2,4-diisocyanatotoluol aufweisenden, isomerengemischen von, im wesentlichen aus 2,4- und 2,6-diisocyanatotoluol bestehenden, isomerengemischen
US4787985A (en) 1987-08-25 1988-11-29 Grenco Process Technology B.V. Multi-stage purification unit process
FR2717800B1 (fr) * 1994-03-25 1996-05-31 Rhone Poulenc Chimie Obtention de 2.6-toluylene diisocyanate à partir d'un mélange comprenant du 2.6-toluylene diisocyanate et du 2.4-toluylene diisocyanate.

Also Published As

Publication number Publication date
TW402584B (en) 2000-08-21
EP0937033A1 (de) 1999-08-25
DE59708080D1 (de) 2002-10-02
MX9904140A (es) 1999-12-01
US6271414B1 (en) 2001-08-07
AU5051798A (en) 1998-05-29
EP0937033B1 (de) 2002-08-28
JP2001503419A (ja) 2001-03-13
BR9712749A (pt) 1999-10-19
DE19645659A1 (de) 1998-05-07
WO1998019993A1 (de) 1998-05-14

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