ES2181933T3 - Procedimiento para la obtencion de disoluciones acuosas de hidroxilamina libre. - Google Patents

Procedimiento para la obtencion de disoluciones acuosas de hidroxilamina libre.

Info

Publication number
ES2181933T3
ES2181933T3 ES96944616T ES96944616T ES2181933T3 ES 2181933 T3 ES2181933 T3 ES 2181933T3 ES 96944616 T ES96944616 T ES 96944616T ES 96944616 T ES96944616 T ES 96944616T ES 2181933 T3 ES2181933 T3 ES 2181933T3
Authority
ES
Spain
Prior art keywords
hydroxylamine
procedure
free hydroxylamine
obtaining water
water dissolutions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96944616T
Other languages
English (en)
Inventor
Otto Watzenberger
Hans-Michael Schneider
Bernd Leutner
Albrecht Wilhelm Friederang
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
BASF Corp
Original Assignee
BASF SE
BASF Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US08/688,281 external-priority patent/US5837107A/en
Application filed by BASF SE, BASF Corp filed Critical BASF SE
Application granted granted Critical
Publication of ES2181933T3 publication Critical patent/ES2181933T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C01B21/1409—Preparation
    • C01B21/1445—Preparation of hydoxylamine from its salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146—Multiple effect distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/38—Steam distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C01B21/1463—Concentration
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C01B21/1472—Separation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Disintegrating Or Milling (AREA)
  • Seasonings (AREA)
  • Gas Separation By Absorption (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

LA PRESENTE INVENCION SE REFIERE A UN PROCEDIMIENTO PARA LA PRODUCCION DE UNA SOLUCION ACUOSA DE HIDROXILAMINA LIBRE, DONDE LA SOLUCION OBTENIDA POR TRATAMIENTO DE UNA SAL DE HIDROXILAMONIO CON UNA BASE, SE SEPARA UNA FRACCION DE HIDROXIALMINA ACUOSA Y UNA FRACCION SALINA MEDIANTE TRATAMIENTO CON AGUA O VAPOR DE AGUA A UNA TEMPERATURA DE 80 (GRADOS) C. EL PROCEDIMIENTO DE LA INVENCION ES SENCILLO Y SE PUEDE IMPLEMENTAR A GRAN ESCALA FACILMENTE. DEBIDO AL PEQUEÑO ESTRES TERMICO, A LA BAJA CONCENTRACION DE HIDROXILAMINA Y AL CORTO TIEMPO DE ESPERA EN EL PROCESO, EL PELIGRO DE DESCOMPOSICION ESTA MINIMIZADO.
ES96944616T 1995-12-20 1996-12-20 Procedimiento para la obtencion de disoluciones acuosas de hidroxilamina libre. Expired - Lifetime ES2181933T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19547758 1995-12-20
US08/688,281 US5837107A (en) 1995-12-20 1996-07-29 Process for production of aqueous solutions of free hydroxylamine

Publications (1)

Publication Number Publication Date
ES2181933T3 true ES2181933T3 (es) 2003-03-01

Family

ID=26021480

Family Applications (2)

Application Number Title Priority Date Filing Date
ES96944615T Expired - Lifetime ES2177828T3 (es) 1995-12-20 1996-12-20 Procedimiento para la separacion de productos de punto de ebullicion medio a partir de una mezcla constituida por productos de punto de ebullicion bajo, medio y elevado.
ES96944616T Expired - Lifetime ES2181933T3 (es) 1995-12-20 1996-12-20 Procedimiento para la obtencion de disoluciones acuosas de hidroxilamina libre.

Family Applications Before (1)

Application Number Title Priority Date Filing Date
ES96944615T Expired - Lifetime ES2177828T3 (es) 1995-12-20 1996-12-20 Procedimiento para la separacion de productos de punto de ebullicion medio a partir de una mezcla constituida por productos de punto de ebullicion bajo, medio y elevado.

Country Status (16)

Country Link
EP (2) EP0868398B1 (es)
JP (2) JP2000505033A (es)
CN (2) CN1102531C (es)
AT (1) ATE222565T1 (es)
AU (2) AU704998B2 (es)
BR (2) BR9612053A (es)
CA (2) CA2239253C (es)
DE (2) DE59609239D1 (es)
DK (1) DK0868399T3 (es)
ES (2) ES2177828T3 (es)
HR (1) HRP960601B1 (es)
IL (2) IL124739A (es)
NO (2) NO319309B1 (es)
PT (1) PT868399E (es)
TR (2) TR199801163T2 (es)
WO (2) WO1997022550A1 (es)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19725851A1 (de) * 1997-06-18 1998-12-24 Basf Ag Verfahren zur Herstellung hochreiner, wässriger Hydroxylaminlösungen
US5788946A (en) * 1997-07-16 1998-08-04 Ashland Inc. Purification of hydroxylamine
DE19733681A1 (de) * 1997-08-04 1999-02-11 Basf Ag Verfahren zur Herstellung einer wäßrigen Lösung von freiem Hydroxylamin
DE19806578A1 (de) * 1998-02-17 1999-08-19 Basf Ag Verfahren zur Herstellung wäßriger, im wesentlichen metallionenfreier Hydroxylaminlösungen
US6235162B1 (en) 1998-05-28 2001-05-22 Sachem, Inc. Ultrapure hydroxylamine compound solutions and process of making same
DE19936594A1 (de) 1999-08-04 2001-02-08 Basf Ag Verfahren zur Herstellung von hochreinen stabilisierten Hydroxylaminlösungen
DE10004818A1 (de) * 2000-02-04 2001-08-09 Basf Ag Verfahren zum Recycling hydroxylaminhaltiger Stripperlösungen
JP3503115B2 (ja) * 2000-06-27 2004-03-02 東レ・ファインケミカル株式会社 フリーヒドロキシルアミン水溶液の製造方法
DE10037774A1 (de) * 2000-08-03 2002-02-14 Bayer Ag Verfahren und Vorrichtung zur Gewinnung organischer Substanzen aus einem diese Substanzen enthaltenden Gasgemisch
DE10131788A1 (de) 2001-07-04 2003-01-16 Basf Ag Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung
DE10131787A1 (de) * 2001-07-04 2003-01-16 Basf Ag Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung
DE10134389A1 (de) * 2001-07-04 2003-01-16 Basf Ag Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung
DE10314492B4 (de) * 2003-03-27 2008-10-16 Domo Caproleuna Gmbh Verfahren zur Herstellung einer wässrigen Lösung von Hydroxylamin
WO2005016817A2 (en) 2003-08-13 2005-02-24 Showa Denko K. K. Process for producing hydroxylamine
TW200508176A (en) * 2003-08-13 2005-03-01 Showa Denko Kk Process for producing hydroxylamine
JP4578885B2 (ja) * 2003-08-13 2010-11-10 昭和電工株式会社 ヒドロキシルアミンの製造方法
FR2860223B1 (fr) * 2003-09-26 2005-12-16 Jean Pierre Schirmann Procede de fabrication de solutions aqueuses d'hydroxylamine base
US7396519B2 (en) 2004-01-26 2008-07-08 San Fu Chemical Company, Ltd. Preparation of a high purity and high concentration hydroxylamine free base
RU2253612C1 (ru) * 2004-01-27 2005-06-10 Закрытое Акционерное Общество "Альянс-Гамма" Способ получения гидроксиламина
JP2005239702A (ja) * 2004-01-28 2005-09-08 Showa Denko Kk ヒドロキシルアミンの製造方法
JP2006056742A (ja) * 2004-08-19 2006-03-02 Hosoya Fireworks Co Ltd 硝酸ヒドロキシルアミン水溶液の製造方法
JP4578988B2 (ja) * 2005-01-21 2010-11-10 昭和電工株式会社 ヒドロキシルアミンの製造方法
JP2006219343A (ja) * 2005-02-10 2006-08-24 Showa Denko Kk ヒドロキシルアミンの製造方法
JP4578999B2 (ja) * 2005-02-10 2010-11-10 昭和電工株式会社 ヒドロキシルアミンの製造方法
JP4578998B2 (ja) * 2005-02-10 2010-11-10 昭和電工株式会社 ヒドロキシルアミンの製造方法
DE102005032430A1 (de) * 2005-07-12 2007-01-25 Bayer Materialscience Ag Verfahren zur Herstellung von Toluylendiamin
WO2017204935A1 (en) 2016-05-26 2017-11-30 Exxonmobil Chemical Patents Inc. Production of cyclic imides suitable for oxidation catalysis
WO2017204936A1 (en) 2016-05-26 2017-11-30 Exxonmobil Chemical Patents Inc. Production of cyclic imides suitable for oxidation catalysis
WO2018075176A1 (en) 2016-10-18 2018-04-26 Exxonmobil Chemical Patents Inc. Cyclic imide slurry compositions
CN108946741B (zh) * 2017-05-17 2020-05-12 新特能源股份有限公司 多晶硅冷氢化工艺中的含硅高沸物的回收工艺方法及冷氢化工艺

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4111759A (en) * 1976-07-08 1978-09-05 United States Steel Corporation Process for separating ammonia and acid gases from waste waters containing fixed ammonia salts
JPS597313B2 (ja) * 1980-02-08 1984-02-17 チツソエンジニアリング株式会社 アルコ−ルの蒸溜装置
DE3302525A1 (de) * 1983-01-26 1984-07-26 Basf Ag, 6700 Ludwigshafen Destillationskolonne zur destillativen zerlegung eines aus mehreren fraktionen bestehenden zulaufproduktes
DE3528463A1 (de) * 1985-08-08 1987-02-19 Basf Ag Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin
DE3814255A1 (de) * 1988-04-27 1989-11-09 Metallgesellschaft Ag Vorrichtung zum desodorieren von organischen fluessigkeiten
US5266290A (en) * 1992-07-10 1993-11-30 Thiokol Corporation Process for making high purity hydroxylammonium nitrate
DE4324410C1 (de) * 1993-07-21 1994-08-04 Enviro Consult Ingenieurgesell Verfahren zum Entfernen von Ammonium aus dem Zentratwasser einer biologischen Abwasserreinigungsanlage
US5385646A (en) * 1993-09-03 1995-01-31 Farmland Industries, Inc. Method of treating chemical process effluent

Also Published As

Publication number Publication date
NO982847L (no) 1998-08-17
CA2239791A1 (en) 1997-06-26
EP0868398A1 (de) 1998-10-07
CA2239253A1 (en) 1997-06-26
BR9612053A (pt) 1999-02-23
AU1304097A (en) 1997-07-14
WO1997022551A1 (de) 1997-06-26
CN1104376C (zh) 2003-04-02
EP0868399A1 (de) 1998-10-07
EP0868398B1 (de) 2002-05-22
AU707648B2 (en) 1999-07-15
TR199801154T2 (xx) 1998-12-21
CA2239791C (en) 2006-01-31
ES2177828T3 (es) 2002-12-16
MX9804788A (es) 1998-10-31
NO982847D0 (no) 1998-06-19
DK0868399T3 (da) 2002-10-07
CA2239253C (en) 2006-01-31
ATE222565T1 (de) 2002-09-15
NO322631B1 (no) 2006-11-06
NO982849L (no) 1998-08-19
IL124737A (en) 2001-06-14
NO982849D0 (no) 1998-06-19
IL124739A0 (en) 1999-01-26
WO1997022550A1 (de) 1997-06-26
EP0868399B1 (de) 2002-08-21
JP2000510385A (ja) 2000-08-15
DE59609239D1 (de) 2002-06-27
HRP960601A2 (en) 1998-04-30
JP4376969B2 (ja) 2009-12-02
CN1209108A (zh) 1999-02-24
CN1102531C (zh) 2003-03-05
PT868399E (pt) 2003-01-31
HRP960601B1 (en) 2001-12-31
JP2000505033A (ja) 2000-04-25
AU1303997A (en) 1997-07-14
BR9612073A (pt) 1999-02-17
CN1205677A (zh) 1999-01-20
DE59609580D1 (de) 2002-09-26
NO319309B1 (no) 2005-07-11
TR199801163T2 (xx) 1998-09-21
IL124739A (en) 2001-06-14
IL124737A0 (en) 1999-01-26
AU704998B2 (en) 1999-05-13

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