ES2185678T3 - Procedimiento para la preparacion de 2-vinil-1,3-dioxolano. - Google Patents
Procedimiento para la preparacion de 2-vinil-1,3-dioxolano.Info
- Publication number
- ES2185678T3 ES2185678T3 ES95113232T ES95113232T ES2185678T3 ES 2185678 T3 ES2185678 T3 ES 2185678T3 ES 95113232 T ES95113232 T ES 95113232T ES 95113232 T ES95113232 T ES 95113232T ES 2185678 T3 ES2185678 T3 ES 2185678T3
- Authority
- ES
- Spain
- Prior art keywords
- dioxolane
- vinyl
- ethylene glycol
- procedure
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- KKBHSBATGOQADJ-UHFFFAOYSA-N 2-ethenyl-1,3-dioxolane Chemical compound C=CC1OCCO1 KKBHSBATGOQADJ-UHFFFAOYSA-N 0.000 title abstract 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 9
- HGINCPLSRVDWNT-UHFFFAOYSA-N Acrolein Chemical compound C=CC=O HGINCPLSRVDWNT-UHFFFAOYSA-N 0.000 abstract 2
- WNXJIVFYUVYPPR-UHFFFAOYSA-N 1,3-dioxolane Chemical compound C1COCO1 WNXJIVFYUVYPPR-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
- 239000011973 solid acid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/12—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with only hydrogen atoms or radicals containing only hydrogen and carbon atoms, directly attached to ring carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
LA INVENCION SE DIRIGE A UN PROCESO PARA LA ELABORACION DE 2 VINIL - 1,3 - DIOXOLANO MEDIANTE TRANSFORMACION DE ACROLEINA CON UN ETILENGLICOL EN PRESENCIA DE UN CATALIZADOR ACIDO SOLIDO Y TRATAMIENTO DE LA MEZCLA DE REACCION. LA SELECTIVIDAD SE ELEVA EN CONTRA DE LOS PROCESOS CONOCIDOS, DONDE LA TRANSFORMACION SE REALIZA EN PRESENCIA DE UN CATALIZADOR ACIDO SOLIDO EN UNA TEMPERATURA POR DEBAJO DE 50 TRAE LA MEZCLA DE REACCION LIBERADA DEL CATALIZADOR BAJO UTILIZACION DE UN ETILENGLICOL EN PRESENCIA DE DISOLVENTES ORGANICOS NO DISUELTOS CON UN PUNTO DE EBULLICION POR ENCIMA DE 130 DONDE LA EXTRACCION OBTENIDA EN AMBAS FASES SE TRATA DE FORMA DESTILATIVA Y LOS PRODUCTOS OBTENIDOS DE NUEVO Y EL DISOLVENTE ORGANICO SE RECICLAN.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4435009A DE4435009A1 (de) | 1994-09-30 | 1994-09-30 | Verfahren zur Herstellung von 2-Vinyl-1,3-dioxolan |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2185678T3 true ES2185678T3 (es) | 2003-05-01 |
Family
ID=6529637
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES95113232T Expired - Lifetime ES2185678T3 (es) | 1994-09-30 | 1995-08-23 | Procedimiento para la preparacion de 2-vinil-1,3-dioxolano. |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5688973A (es) |
| EP (1) | EP0704441B1 (es) |
| JP (1) | JPH08113568A (es) |
| AT (1) | ATE226950T1 (es) |
| AU (1) | AU677918B2 (es) |
| DE (2) | DE4435009A1 (es) |
| ES (1) | ES2185678T3 (es) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP7227711B2 (ja) * | 2017-08-07 | 2023-02-22 | ファームハンノン・カンパニー・リミテッド | 2-(2-ハロエチル)-1,3-ジオキソランの製造方法 |
| EP3904327A1 (de) | 2020-04-30 | 2021-11-03 | Röhm GmbH | Verfahren zur herstellung von hydroxyalkyl(meth)acrylsäureestern durch oxidative spaltung von methacrolein-acetalen |
| EP4428116A1 (de) | 2023-03-07 | 2024-09-11 | Röhm GmbH | Neues verfahren zur herstellung von methylmethacrylat über acetalische zwischenstufen |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2862007A (en) * | 1957-09-27 | 1958-11-25 | Union Carbide Corp | Triply unsaturated 1,3-dioxolanes and process for their preparation |
| US3014924A (en) * | 1958-04-15 | 1961-12-26 | Du Pont | Catalytic process for making unsaturated cyclic acetals |
| US4108869A (en) * | 1977-08-25 | 1978-08-22 | E. I. Du Pont De Nemours And Company | Preparation of an acetal from a diol and acrolein |
| DE4040362A1 (de) * | 1990-12-17 | 1992-06-25 | Degussa | Verfahren zur herstellung von gemischen cyclischer acroleinglycerinacetale |
-
1994
- 1994-09-30 DE DE4435009A patent/DE4435009A1/de not_active Withdrawn
-
1995
- 1995-08-23 AT AT95113232T patent/ATE226950T1/de not_active IP Right Cessation
- 1995-08-23 DE DE59510436T patent/DE59510436D1/de not_active Expired - Lifetime
- 1995-08-23 ES ES95113232T patent/ES2185678T3/es not_active Expired - Lifetime
- 1995-08-23 EP EP95113232A patent/EP0704441B1/de not_active Expired - Lifetime
- 1995-09-05 US US08/523,339 patent/US5688973A/en not_active Expired - Fee Related
- 1995-09-26 JP JP7248008A patent/JPH08113568A/ja not_active Abandoned
- 1995-09-29 AU AU32983/95A patent/AU677918B2/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| EP0704441B1 (de) | 2002-10-30 |
| AU677918B2 (en) | 1997-05-08 |
| ATE226950T1 (de) | 2002-11-15 |
| DE4435009A1 (de) | 1996-04-04 |
| EP0704441A2 (de) | 1996-04-03 |
| US5688973A (en) | 1997-11-18 |
| EP0704441A3 (de) | 1997-01-08 |
| JPH08113568A (ja) | 1996-05-07 |
| DE59510436D1 (de) | 2002-12-05 |
| AU3298395A (en) | 1996-04-18 |
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