ES2188105T3 - Procedimiento de fabricacion en continuo de (met) acrilatos de dialquilaminoalquilo. - Google Patents
Procedimiento de fabricacion en continuo de (met) acrilatos de dialquilaminoalquilo.Info
- Publication number
- ES2188105T3 ES2188105T3 ES99400855T ES99400855T ES2188105T3 ES 2188105 T3 ES2188105 T3 ES 2188105T3 ES 99400855 T ES99400855 T ES 99400855T ES 99400855 T ES99400855 T ES 99400855T ES 2188105 T3 ES2188105 T3 ES 2188105T3
- Authority
- ES
- Spain
- Prior art keywords
- column
- met
- acrylate
- directed towards
- dialquilaminoalquil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title 1
- 238000005809 transesterification reaction Methods 0.000 abstract 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 abstract 1
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 abstract 1
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 1
- BAPJBEWLBFYGME-UHFFFAOYSA-N acrylic acid methyl ester Natural products COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- WCYWZMWISLQXQU-UHFFFAOYSA-N methyl Chemical class [CH3] WCYWZMWISLQXQU-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 abstract 1
- VFHDDANHQLKHJQ-UHFFFAOYSA-N prop-2-enoic acid Chemical compound OC(=O)C=C.OC(=O)C=C.OC(=O)C=C VFHDDANHQLKHJQ-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
LA PRESENTE INVENCION SE REFIERE A LA FABRICACION DE UN (MET)ACRILATO DE DIALQUILAMINOALQUILO POR TRANSESTERIFICACION DE (MET)ACRILATO METILICO O ETILICO CON UN AMINOALCOHOL. EL CATALIZADOR DE TRANSESTERIFICACION SE ESCOGE ENTRE LOS TITANATOS TETRABUTILICOS, TETRAETILICOS Y TETRA (2 - ETILEXILO). SE CONTROLA LA REACCION EN UN REACTOR AGITADO A 90 - 120 GRADOS C, Y LUEGO SE DIRIGE LA MEZCLA BRUTA REACCIONAL HACIA UNA COLUMNA DE COLA (C1), SE DIRIGE EL FLUJO DE CABEZA DE ESTA COLUMNA HACIA UNA COLUMNA DE CABEZA (C2), Y LUEGO SE DIRIGE EL FLUJO DE PIE DE ESTA COLUMNA HACIA LA COLUMNA DE RECTIFICACION FINAL (C3). SE LLEGA DE ESTE MODO A UN (MET)ACRILATO DE DIALQUILAMINOALQUILO DE ALTA PUREZA.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9804964A FR2777561B1 (fr) | 1998-04-21 | 1998-04-21 | Procede de fabrication en continu de (meth)acrylates de dialkylaminoalkyle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2188105T3 true ES2188105T3 (es) | 2003-06-16 |
Family
ID=9525479
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES99400855T Expired - Lifetime ES2188105T3 (es) | 1998-04-21 | 1999-04-08 | Procedimiento de fabricacion en continuo de (met) acrilatos de dialquilaminoalquilo. |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US6437173B1 (es) |
| EP (1) | EP0960877B1 (es) |
| JP (1) | JP3009666B2 (es) |
| KR (1) | KR19990083363A (es) |
| CN (1) | CN1190412C (es) |
| AR (1) | AR018192A1 (es) |
| AT (1) | ATE229494T1 (es) |
| AU (1) | AU2386499A (es) |
| BR (1) | BR9901374A (es) |
| CA (1) | CA2269305A1 (es) |
| DE (1) | DE69904391T2 (es) |
| ES (1) | ES2188105T3 (es) |
| FR (1) | FR2777561B1 (es) |
| TW (1) | TWI250140B (es) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10029517A1 (de) | 2000-06-21 | 2002-01-17 | Stockhausen Chem Fab Gmbh | Verfahren zur Herstellung von Aminoalkyl(meth)acrylaten |
| FR2811986B1 (fr) * | 2000-07-18 | 2004-02-27 | Atofina | Procede de fabrication en continu de (meth)acrylates de dialkylaminoalkyle |
| DE10127938A1 (de) | 2001-06-08 | 2002-07-25 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| DE10127941A1 (de) | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| DE10127939A1 (de) * | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| DE10301007A1 (de) * | 2003-01-13 | 2004-07-22 | Röhm GmbH & Co. KG | Verbessertes Verfahren zur kontinuierlichen Herstellung von Alkyl(meth)acrylaten mit mehrfacher Katalysatorrezyklierung. |
| DE10323699A1 (de) * | 2003-05-22 | 2004-12-09 | Röhm GmbH & Co. KG | Verfahren zur kontinuierlichen Herstellung von Alkylamino(meth)acrylamiden |
| WO2004106278A1 (ja) | 2003-05-28 | 2004-12-09 | Mitsubishi Rayon Co., Ltd. | (メタ)アクリル酸n−アルキルアミノアルキルエステルの製造方法 |
| TWI253636B (en) * | 2003-11-19 | 2006-04-21 | Mediatek Inc | Apparatus with switching servo gain and offset for optical disk device and method thereof |
| FR2876375B1 (fr) * | 2004-10-12 | 2007-02-02 | Arkema Sa | Procede de preparation d'esters ou d'anydrides (meth) acryliques |
| GB0523340D0 (en) * | 2005-11-16 | 2005-12-28 | Ciba Sc Holding Ag | Manufacture of esters |
| FR2909377A1 (fr) | 2006-12-05 | 2008-06-06 | Arkema France | Procede de synthese d'esters (meth)acryliques catalyse par un titanate de polyol |
| JP5369438B2 (ja) * | 2008-01-10 | 2013-12-18 | 東亞合成株式会社 | ジアルキルアミノアルキル(メタ)アクリレートの連続製造方法 |
| FR2934261B1 (fr) * | 2008-07-25 | 2015-04-10 | Arkema France | Procede de synthese d'esters de l'acide acrylique |
| DE102009002239A1 (de) | 2009-04-07 | 2010-10-14 | Evonik Röhm Gmbh | Verfahren zur kontinuierlichen Herstellung von Alkylamino(meth)acrylamiden |
| US7829738B1 (en) * | 2009-05-19 | 2010-11-09 | Nalco Company | Production of N,N-dialklylaminoethyl (meth)acrylates |
| JP5585100B2 (ja) * | 2010-01-29 | 2014-09-10 | 東亞合成株式会社 | アミノ基含有(メタ)アクリレートの連続製造方法 |
| KR20130136993A (ko) * | 2010-09-23 | 2013-12-13 | 바스프 에스이 | N,n-치환된 아미노 알콜의 (메트)아크릴산 에스테르를 제조하기 위한 방법 |
| FR2985999B1 (fr) * | 2012-01-23 | 2014-01-31 | Arkema France | Procede de production d'acrylate de 2-octyle par transesterification |
| FR2985998B1 (fr) | 2012-01-23 | 2014-01-31 | Arkema France | Procede de production d'acrylate de 2-octyle par transesterification |
| FR3002771B1 (fr) * | 2013-03-01 | 2015-02-27 | Arkema France | Procede de production d'acrylate de 2-propyl heptyle par transesterefication |
| FR3050731B1 (fr) * | 2016-04-28 | 2018-04-20 | Arkema France | Composition d'acrylate de n,n-dimethyl aminoethyle stabilisee vis-a-vis de la coloration |
| EP3263551B1 (de) | 2016-06-28 | 2020-10-14 | Evonik Operations GmbH | Herstellung von n,n-(di)alkylaminoalkyl(meth)acrylamid bzw. n,n-(di)alkylaminoalkyl(meth)acrylat und deren quarternären ammoniumsalzen als flockungshilfsmittel und gelbildner |
| SG11201900007VA (en) | 2016-08-05 | 2019-02-27 | Basf Se | Macromonomers containing polyisobutene groups, and homopolymers or copolymers thereof |
| FR3069538B1 (fr) | 2017-07-25 | 2020-05-15 | Arkema France | Procede de purification d'esters (meth)acryliques. |
| FR3104155B1 (fr) | 2019-12-09 | 2021-10-29 | Arkema France | Procede de fabrication en continu d’acrylates d’alkyle lourds |
| FR3125040B1 (fr) | 2021-07-09 | 2024-04-26 | Snf Sa | Procédé d’obtention de bio-monomère à partir de diméthylaminoethanol d’origine renouvelable |
| CN117729967A (zh) | 2021-07-29 | 2024-03-19 | 巴斯夫欧洲公司 | 丙烯酸酯连续蒸馏的方法 |
| CN115340467A (zh) * | 2022-08-05 | 2022-11-15 | 北京恒聚化工集团有限责任公司 | 一种丙烯酸二甲氨基乙酯的制备方法 |
| FR3144991A1 (fr) | 2023-01-12 | 2024-07-19 | Arkema France | Procede de fabrication d’esters (meth)acryliques a partir d’aminoalcools par transesterification enzymatique |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BR8701337A (pt) * | 1987-03-24 | 1988-09-27 | Ciquine Companhia Petroquimica | Processo para producao de esteres acrilicos |
| FR2617840B1 (fr) * | 1987-07-08 | 1989-09-01 | Charbonnages Ste Chimique | Procede de fabrication de (meth)acrylate de dialkylaminoalkyle |
| JPH0713050B2 (ja) * | 1989-09-26 | 1995-02-15 | 東亞合成株式会社 | ジメチルアミノエチルアクリレートの製造方法 |
-
1998
- 1998-04-21 FR FR9804964A patent/FR2777561B1/fr not_active Expired - Lifetime
-
1999
- 1999-04-08 ES ES99400855T patent/ES2188105T3/es not_active Expired - Lifetime
- 1999-04-08 EP EP99400855A patent/EP0960877B1/fr not_active Expired - Lifetime
- 1999-04-08 AT AT99400855T patent/ATE229494T1/de not_active IP Right Cessation
- 1999-04-08 DE DE69904391T patent/DE69904391T2/de not_active Expired - Lifetime
- 1999-04-15 CA CA002269305A patent/CA2269305A1/fr not_active Abandoned
- 1999-04-20 AU AU23864/99A patent/AU2386499A/en not_active Abandoned
- 1999-04-20 BR BR9901374A patent/BR9901374A/pt not_active IP Right Cessation
- 1999-04-21 AR ARP990101829A patent/AR018192A1/es not_active Application Discontinuation
- 1999-04-21 CN CNB991073851A patent/CN1190412C/zh not_active Expired - Lifetime
- 1999-04-21 JP JP11113442A patent/JP3009666B2/ja not_active Expired - Lifetime
- 1999-04-21 US US09/295,332 patent/US6437173B1/en not_active Expired - Lifetime
- 1999-04-21 KR KR1019990014172A patent/KR19990083363A/ko not_active Ceased
- 1999-05-20 TW TW088106384A patent/TWI250140B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| EP0960877A3 (fr) | 2000-03-01 |
| DE69904391D1 (de) | 2003-01-23 |
| JP3009666B2 (ja) | 2000-02-14 |
| CN1235961A (zh) | 1999-11-24 |
| KR19990083363A (ko) | 1999-11-25 |
| CN1190412C (zh) | 2005-02-23 |
| TWI250140B (en) | 2006-03-01 |
| JPH11322680A (ja) | 1999-11-24 |
| DE69904391T2 (de) | 2003-10-09 |
| AU2386499A (en) | 1999-10-28 |
| AR018192A1 (es) | 2001-10-31 |
| BR9901374A (pt) | 2000-03-21 |
| ATE229494T1 (de) | 2002-12-15 |
| FR2777561A1 (fr) | 1999-10-22 |
| US6437173B1 (en) | 2002-08-20 |
| EP0960877B1 (fr) | 2002-12-11 |
| CA2269305A1 (fr) | 1999-10-21 |
| FR2777561B1 (fr) | 2000-06-02 |
| EP0960877A2 (fr) | 1999-12-01 |
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