ES2190225T3 - Procedimiento de destilacion de amoniaco. - Google Patents

Procedimiento de destilacion de amoniaco.

Info

Publication number
ES2190225T3
ES2190225T3 ES99929490T ES99929490T ES2190225T3 ES 2190225 T3 ES2190225 T3 ES 2190225T3 ES 99929490 T ES99929490 T ES 99929490T ES 99929490 T ES99929490 T ES 99929490T ES 2190225 T3 ES2190225 T3 ES 2190225T3
Authority
ES
Spain
Prior art keywords
equal
ammonia
amoniac
column
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES99929490T
Other languages
English (en)
Inventor
Gerald Bocquenet
Patrick Houssier
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Polyamide Intermediates SAS
Original Assignee
Rhodia Polyamide Intermediates SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=9529011&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=ES2190225(T3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Rhodia Polyamide Intermediates SAS filed Critical Rhodia Polyamide Intermediates SAS
Application granted granted Critical
Publication of ES2190225T3 publication Critical patent/ES2190225T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/08—Preparation of ammonia from nitrogenous organic substances
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/28—Evaporating with vapour compression
    • B01D1/289—Compressor features (e.g. constructions, details, cooling, lubrication, driving systems)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/28—Evaporating with vapour compression
    • B01D1/284—Special features relating to the compressed vapour
    • B01D1/2856—The compressed vapour is used for heating a reboiler or a heat exchanger outside an evaporator
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/10—Separation of ammonia from ammonia liquors, e.g. gas liquors
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/08—Waste heat

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)

Abstract

Procedimiento de separación por destilación del amoníaco contenido en una solución acuosa de caprolactama, caracterizado porque se destila con la ayuda de una columna, con una temperatura en el fondo inferior o igual a 160°C y a una presión absoluta inferior o igual a 5 bares, siendo comprimido el amoníaco destilado por la cabeza de columna a una presión superior o igual a 10 bares y luego condensado a una temperatura de 25°C a 60°C.
ES99929490T 1998-07-22 1999-07-15 Procedimiento de destilacion de amoniaco. Expired - Lifetime ES2190225T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9809530A FR2781476B1 (fr) 1998-07-22 1998-07-22 Procede de distillation d'ammoniac contenu dans un melange comprenant du caprolactame

Publications (1)

Publication Number Publication Date
ES2190225T3 true ES2190225T3 (es) 2003-07-16

Family

ID=9529011

Family Applications (1)

Application Number Title Priority Date Filing Date
ES99929490T Expired - Lifetime ES2190225T3 (es) 1998-07-22 1999-07-15 Procedimiento de destilacion de amoniaco.

Country Status (19)

Country Link
US (1) US6482297B1 (es)
EP (1) EP1102720B1 (es)
JP (1) JP3854069B2 (es)
KR (1) KR100421265B1 (es)
CN (1) CN1151965C (es)
AT (1) ATE235423T1 (es)
BR (1) BR9912346A (es)
CA (1) CA2337321C (es)
CZ (1) CZ2001257A3 (es)
DE (1) DE69906309T2 (es)
ES (1) ES2190225T3 (es)
FR (1) FR2781476B1 (es)
ID (1) ID28543A (es)
PL (1) PL345596A1 (es)
RU (1) RU2186026C1 (es)
SK (1) SK283702B6 (es)
TW (1) TW469260B (es)
UA (1) UA54612C2 (es)
WO (1) WO2000005173A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10004311A1 (de) * 2000-02-01 2001-08-02 Basf Ag Destillative Reinigung von Ammoniak
MY127068A (en) * 2000-06-05 2006-11-30 Basf Ag Removal of ammonia from solutions including caprolactam and ammonia
DE10253095A1 (de) * 2002-11-13 2004-06-17 Basf Ag Verfahren zur Reinigung von Caprolactam
US8066971B2 (en) * 2005-04-04 2011-11-29 Los Angeles Biomedical Reseach Institute at Harbor UCLA Medical Center Targeting pulmonary epithelium using ADRP
US9994457B2 (en) 2014-04-07 2018-06-12 The Boeing Company System and method for ammonia distillation
GB2608159B (en) * 2021-06-24 2026-03-25 Process Ltd A system and method for recovering ammonia from an ammonia-containing liquid

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2108914A (en) * 1935-05-01 1938-02-22 Hercules Powder Co Ltd Method of concentrating aqueous ammonia solutions
US2519451A (en) * 1946-06-08 1950-08-22 Lummus Co Ammonia distillation
US2805984A (en) * 1956-07-09 1957-09-10 Clair John C St Process for distilling cuprammonium rayon used spinning liquors
US3054726A (en) * 1959-10-29 1962-09-18 United States Steel Corp Method of recovering ammonia from aqueous ammonia vapors by a twostage steam distillation operation
US3595615A (en) * 1969-03-26 1971-07-27 Gulf Research Development Co Recovery of high purity ammonia and hydrogen sulfide from ammonium sulfides
US4140586A (en) * 1976-06-14 1979-02-20 Bethlehem Steel Corporation Method and apparatus for distillation
FR2526005A1 (fr) * 1982-04-29 1983-11-04 Quiri Usines Unite de recuperation d'ammoniac a haut rendement pour installation de traitement utilisant l'ammoniac comme produit actif
RU2035453C1 (ru) * 1992-02-03 1995-05-20 Акционерное общество "Куйбышевазот" Способ получения капролактама бекмановской перегруппировкой циклогексаноноксима
BE1007298A3 (nl) * 1993-07-19 1995-05-09 Dsm Nv Werkwijze voor het zuiveren van een water-epsilon-caprolactam mengsel.
DE19548289A1 (de) * 1995-12-22 1997-06-26 Basf Ag Verfahren zur gleichzeitigen Herstellung von Caprolactam und Hexamethylendiamin
FR2755132B1 (fr) * 1996-10-24 1998-11-27 Rhone Poulenc Fibres Procede de traitement de lactames

Also Published As

Publication number Publication date
TW469260B (en) 2001-12-21
US6482297B1 (en) 2002-11-19
DE69906309T2 (de) 2004-01-22
BR9912346A (pt) 2002-01-15
EP1102720A1 (fr) 2001-05-30
SK283702B6 (sk) 2003-12-02
WO2000005173A1 (fr) 2000-02-03
RU2001104897A (ru) 2004-02-20
DE69906309D1 (de) 2003-04-30
JP2002521349A (ja) 2002-07-16
CN1318034A (zh) 2001-10-17
CA2337321C (fr) 2003-02-11
JP3854069B2 (ja) 2006-12-06
FR2781476A1 (fr) 2000-01-28
ID28543A (id) 2001-05-31
CN1151965C (zh) 2004-06-02
SK1082001A3 (en) 2001-09-11
EP1102720B1 (fr) 2003-03-26
KR20010071011A (ko) 2001-07-28
CZ2001257A3 (cs) 2001-09-12
ATE235423T1 (de) 2003-04-15
PL345596A1 (en) 2001-12-17
CA2337321A1 (fr) 2000-02-03
RU2186026C1 (ru) 2002-07-27
KR100421265B1 (ko) 2004-03-09
FR2781476B1 (fr) 2000-09-22
UA54612C2 (uk) 2003-03-17

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