ES2199697B1 - Procedimiento para regenerar aceites usados por desmetalizacion y destilacion. - Google Patents
Procedimiento para regenerar aceites usados por desmetalizacion y destilacion.Info
- Publication number
- ES2199697B1 ES2199697B1 ES200302203A ES200302203A ES2199697B1 ES 2199697 B1 ES2199697 B1 ES 2199697B1 ES 200302203 A ES200302203 A ES 200302203A ES 200302203 A ES200302203 A ES 200302203A ES 2199697 B1 ES2199697 B1 ES 2199697B1
- Authority
- ES
- Spain
- Prior art keywords
- distillation
- oil
- demetalization
- procedure
- regenerating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000004821 distillation Methods 0.000 title abstract 5
- 239000003921 oil Substances 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 3
- 230000001172 regenerating effect Effects 0.000 title abstract 2
- 239000010913 used oil Substances 0.000 abstract 2
- 229910001854 alkali hydroxide Inorganic materials 0.000 abstract 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- 150000001450 anions Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 239000003153 chemical reaction reagent Substances 0.000 abstract 1
- 150000004679 hydroxides Chemical class 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000314 lubricant Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 150000002739 metals Chemical class 0.000 abstract 1
- 239000002480 mineral oil Substances 0.000 abstract 1
- 235000010446 mineral oil Nutrition 0.000 abstract 1
- 239000003208 petroleum Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M175/00—Working-up used lubricants to recover useful products ; Cleaning
- C10M175/02—Working-up used lubricants to recover useful products ; Cleaning mineral-oil based
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M175/00—Working-up used lubricants to recover useful products ; Cleaning
- C10M175/0016—Working-up used lubricants to recover useful products ; Cleaning with the use of chemical agents
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M175/00—Working-up used lubricants to recover useful products ; Cleaning
- C10M175/0025—Working-up used lubricants to recover useful products ; Cleaning by thermal processes
- C10M175/0033—Working-up used lubricants to recover useful products ; Cleaning by thermal processes using distillation processes; devices therefor
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Lubricants (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Fats And Perfumes (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Procedimiento para regenerar aceites usados por desmetalización y destilación. La presente invención se refiere a un procedimiento para regenerar aceites usados de origen petrolífero que comprende las siguientes etapas: (a) desmetalización del aceite mineral usado mediante tratamiento químico de dicho aceite con una solución acuosa de un reactivo químico que contiene aniones que forman sales poco solubles con los metales del aceite, seguido de separación del aceite desmetalizado; (b) destilación del aceite desmetalizado obtenido en la etapa (a) a presión atmosférica y en presencia de hidróxidos alcalinos; y (c) destilación del residuo líquido obtenido en la destilación atmosférica de la etapa (b) a vacío y en presencia de hidróxidos alcalinos para obtener bases lubricantes.
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200302203A ES2199697B1 (es) | 2003-09-23 | 2003-09-23 | Procedimiento para regenerar aceites usados por desmetalizacion y destilacion. |
| US10/573,012 US7431829B2 (en) | 2003-09-23 | 2004-09-23 | Method for regenerating used oils by demetallization and distillation |
| AT04766956T ATE440934T1 (de) | 2003-09-23 | 2004-09-23 | Altílregenerationsverfahren mit demetallisation und destillation |
| DE602004022872T DE602004022872D1 (de) | 2003-09-23 | 2004-09-23 | Altölregenerationsverfahren mit demetallisation und destillation |
| CN200480031509.7A CN1871330B (zh) | 2003-09-23 | 2004-09-23 | 脱金属和蒸馏再生废油的方法 |
| RU2006113706/04A RU2356939C2 (ru) | 2003-09-23 | 2004-09-23 | Способ регенерации отработанных масел путем деметаллизации и дистилляции |
| PCT/ES2004/000418 WO2005028600A1 (es) | 2003-09-23 | 2004-09-23 | Procedimiento para regenerar aceites usados por desmetalizacion y destilacion |
| EP04766956A EP1712608B1 (en) | 2003-09-23 | 2004-09-23 | Method for regenerating used oils by demetallization and distillation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200302203A ES2199697B1 (es) | 2003-09-23 | 2003-09-23 | Procedimiento para regenerar aceites usados por desmetalizacion y destilacion. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2199697A1 ES2199697A1 (es) | 2004-02-16 |
| ES2199697B1 true ES2199697B1 (es) | 2005-02-01 |
Family
ID=31897138
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES200302203A Expired - Fee Related ES2199697B1 (es) | 2003-09-23 | 2003-09-23 | Procedimiento para regenerar aceites usados por desmetalizacion y destilacion. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US7431829B2 (es) |
| EP (1) | EP1712608B1 (es) |
| CN (1) | CN1871330B (es) |
| AT (1) | ATE440934T1 (es) |
| DE (1) | DE602004022872D1 (es) |
| ES (1) | ES2199697B1 (es) |
| RU (1) | RU2356939C2 (es) |
| WO (1) | WO2005028600A1 (es) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2010138110A1 (en) | 2009-05-26 | 2010-12-02 | Fluid-Quip, Inc. | Methods for producing a high protein corn meal from a whole stillage byproduct and system therefore |
| FR2961521B1 (fr) * | 2010-06-22 | 2013-07-12 | Conception D Equipements Pour L Environnement Et L Ind Soc D | Procede de purification d'une charge hydrocarbonee usagee |
| CN103242950B (zh) * | 2013-05-20 | 2014-08-06 | 宁波市蓝润能源科技有限公司 | 一种无污染的废润滑油再生工艺 |
| CN103266008B (zh) * | 2013-05-30 | 2014-10-01 | 山东信诺润滑油有限公司 | 一种废润滑油再生方法 |
| CN104371759A (zh) * | 2013-08-14 | 2015-02-25 | 宁波北仑千和环保工程有限公司 | 一种废矿物油综合利用装置 |
| EP3078730A4 (en) | 2013-11-08 | 2017-07-19 | Sener Ingenieria Y Sistemas, S.A. | Method for increasing the yield of lubricating bases in the regeneration of used oils |
| RU2630486C1 (ru) * | 2016-06-27 | 2017-09-11 | Общество с ограниченной ответственностью "Нитро-Технологии Саяны" (ООО "НТ Саяны") | Способ обработки отработанных жидких нефтепродуктов для изготовления смесевых взрывчатых веществ, содержащих окислитель в виде солей - нитратов |
| US10961466B2 (en) * | 2017-07-27 | 2021-03-30 | Basis Energy Purification, Llc | Purification of renewable oils |
| CA3025239A1 (en) | 2017-11-27 | 2019-05-27 | Fluid Quip Process Technologies, Llc | Method and system for reducing the unfermentable solids content in a protein portion at the back end of a corn dry milling process |
| CN108998194B (zh) * | 2018-09-14 | 2021-07-27 | 闽江学院 | 一种废润滑油脱色方法 |
| US10875889B2 (en) | 2018-12-28 | 2020-12-29 | Fluid Quip Technologies, Llc | Method and system for producing a zein protein product from a whole stillage byproduct produced in a corn dry-milling process |
| CN112725059A (zh) * | 2019-10-28 | 2021-04-30 | 苏州九发节能环保科技有限公司 | 一种长效导轨油及其制备方法 |
| EP4139424A1 (en) * | 2020-04-20 | 2023-03-01 | ExxonMobil Technology and Engineering Company | Membrane separation of used oil and compositions generated |
| CN111876197A (zh) * | 2020-07-28 | 2020-11-03 | 湖北润驰环保科技有限公司 | 一种化学精制法处理废润滑油的预处理工艺 |
| CN115109614B (zh) * | 2021-03-23 | 2023-11-17 | 李晶 | 废矿物油再生基础油防结焦防夹带工艺方法 |
| US12213497B2 (en) | 2021-05-12 | 2025-02-04 | Fluid Quip Technologies, Llc | Method and system for producing a protein and fiber feed product from a whole stillage byproduct produced in a corn dry milling process |
| CN114250106B (zh) * | 2021-12-28 | 2023-01-10 | 安徽国孚生态工程技术有限公司 | 一种废内燃机油蒸馏脱金属方法 |
| CN117070247A (zh) * | 2023-09-13 | 2023-11-17 | 宜昌升华新能源科技有限公司 | 一种废矿物油脱金属预处理方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3930988A (en) * | 1975-02-24 | 1976-01-06 | Phillips Petroleum Company | Reclaiming used motor oil |
| US6117306A (en) * | 1996-10-02 | 2000-09-12 | Institut Francais Du Petrole | Catalytic process for conversion of a petroleum residue using a fixed bed hydrodemetallization catalyst |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3879282A (en) * | 1974-02-26 | 1975-04-22 | Phillips Petroleum Co | Reclaiming used motor oil by chemical treatment with ammonium phosphate |
| US4071438A (en) * | 1976-06-03 | 1978-01-31 | Vacsol Corporation | Method of reclaiming waste oil by distillation and extraction |
| US4151072A (en) * | 1977-05-16 | 1979-04-24 | Phillips Petroleum Company | Reclaiming used lubricating oils |
| US4247389A (en) * | 1979-11-07 | 1981-01-27 | Phillips Petroleum Company | De-ashing lubricating oils |
| US4204946A (en) * | 1979-02-12 | 1980-05-27 | Turbo Resources Ltd. | Process for removing metal contaminants from used lubricating oils |
| US4224142A (en) * | 1979-06-29 | 1980-09-23 | Phillips Petroleum Company | Treatment of recycled ammonium sulfate-bisulfate solution |
| US4411774A (en) * | 1981-01-16 | 1983-10-25 | Turbo Resources Ltd. | Process for removing contaminants from waste lubricating oil by chemical treatment |
| US4381992A (en) * | 1981-06-15 | 1983-05-03 | Phillips Petroleum Company | Reclaiming used lubricating oil |
| US4420389A (en) * | 1982-09-14 | 1983-12-13 | Phillips Petroleum Company | De-ashing lubricating oils |
| CH657867A5 (de) * | 1983-09-21 | 1986-09-30 | Buss Ag | Verfahren zur wiederaufbereitung von altoel und destillations-vorrichtung zur durchfuehrung des verfahrens. |
| US4834868A (en) * | 1988-01-29 | 1989-05-30 | Breslube Usa, Inc. | Neutralizing oxidation product components in continuous rerefining of used oil stocks |
| IT1255534B (it) | 1992-09-30 | 1995-11-09 | Processo di riraffinazione di oli usati | |
| IT1263961B (it) * | 1993-02-24 | 1996-09-05 | Eniricerche Spa | Procedimento per la deasfaltazione e la demetallazione di residui petroliferi |
| FR2703067B1 (fr) * | 1993-03-22 | 1995-08-04 | Sotulub | Procédé et installation de régénération d'huiles lubrifiantes. |
| FR2725725B1 (fr) * | 1994-10-17 | 1996-12-13 | Inst Francais Du Petrole | Procede et installation pour la purification des huiles usagees |
| FR2735785B1 (fr) * | 1995-06-22 | 1997-08-08 | Chavet Bernard | Procede de raffinage d'huiles usagees par traitement alcalin |
| US5795463A (en) * | 1996-08-05 | 1998-08-18 | Prokopowicz; Richard A. | Oil demetalizing process |
| FR2757175B1 (fr) | 1996-12-13 | 1999-03-05 | Tunisienne De Lubrifiants Sotu | Procede et installation de regeneration d'huiles lubrifiantes a hautes performances |
| CN1107109C (zh) * | 2000-10-26 | 2003-04-30 | 中国石油化工股份有限公司 | 一种废油的回收方法 |
| PT1559768E (pt) | 2002-07-15 | 2006-09-29 | Sener Grupo De Ingenier A S A | Metodo de regeneracao de oleos usados atraves de extraccao com solventes |
-
2003
- 2003-09-23 ES ES200302203A patent/ES2199697B1/es not_active Expired - Fee Related
-
2004
- 2004-09-23 CN CN200480031509.7A patent/CN1871330B/zh not_active Expired - Fee Related
- 2004-09-23 AT AT04766956T patent/ATE440934T1/de not_active IP Right Cessation
- 2004-09-23 DE DE602004022872T patent/DE602004022872D1/de not_active Expired - Lifetime
- 2004-09-23 RU RU2006113706/04A patent/RU2356939C2/ru not_active IP Right Cessation
- 2004-09-23 EP EP04766956A patent/EP1712608B1/en not_active Expired - Lifetime
- 2004-09-23 WO PCT/ES2004/000418 patent/WO2005028600A1/es not_active Ceased
- 2004-09-23 US US10/573,012 patent/US7431829B2/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3930988A (en) * | 1975-02-24 | 1976-01-06 | Phillips Petroleum Company | Reclaiming used motor oil |
| US6117306A (en) * | 1996-10-02 | 2000-09-12 | Institut Francais Du Petrole | Catalytic process for conversion of a petroleum residue using a fixed bed hydrodemetallization catalyst |
Also Published As
| Publication number | Publication date |
|---|---|
| ATE440934T1 (de) | 2009-09-15 |
| US7431829B2 (en) | 2008-10-07 |
| WO2005028600A1 (es) | 2005-03-31 |
| CN1871330A (zh) | 2006-11-29 |
| CN1871330B (zh) | 2010-10-06 |
| EP1712608B1 (en) | 2009-08-26 |
| ES2199697A1 (es) | 2004-02-16 |
| US20070039853A1 (en) | 2007-02-22 |
| DE602004022872D1 (de) | 2009-10-08 |
| RU2006113706A (ru) | 2007-11-20 |
| RU2356939C2 (ru) | 2009-05-27 |
| EP1712608A1 (en) | 2006-10-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EC2A | Search report published |
Date of ref document: 20040216 Kind code of ref document: A1 |
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Ref document number: 2199697B1 Country of ref document: ES |
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| FD2A | Announcement of lapse in spain |
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