ES2483115T3 - Procedimiento para la preparación de una composición que comprende ácido meso-tartárico - Google Patents
Procedimiento para la preparación de una composición que comprende ácido meso-tartárico Download PDFInfo
- Publication number
- ES2483115T3 ES2483115T3 ES10724031.9T ES10724031T ES2483115T3 ES 2483115 T3 ES2483115 T3 ES 2483115T3 ES 10724031 T ES10724031 T ES 10724031T ES 2483115 T3 ES2483115 T3 ES 2483115T3
- Authority
- ES
- Spain
- Prior art keywords
- tartaric acid
- alkali metal
- meso
- weight
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 title abstract 7
- 239000000203 mixture Substances 0.000 title abstract 6
- FEWJPZIEWOKRBE-XIXRPRMCSA-N Mesotartaric acid Chemical compound OC(=O)[C@@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-XIXRPRMCSA-N 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 abstract 9
- 229910052783 alkali metal Inorganic materials 0.000 abstract 5
- 150000001340 alkali metals Chemical class 0.000 abstract 3
- 229960001270 d- tartaric acid Drugs 0.000 abstract 3
- 229960001367 tartaric acid Drugs 0.000 abstract 3
- 235000002906 tartaric acid Nutrition 0.000 abstract 3
- 239000011975 tartaric acid Substances 0.000 abstract 3
- 150000003839 salts Chemical class 0.000 abstract 2
- 150000008044 alkali metal hydroxides Chemical class 0.000 abstract 1
- -1 alkali metal salt Chemical class 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D3/00—Halides of sodium, potassium or alkali metals in general
- C01D3/26—Preventing the absorption of moisture or caking of the crystals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
- C07C51/367—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of functional groups containing oxygen only in singly bound form
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/13—Crystalline forms, e.g. polymorphs
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Medicinal Preparation (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
Un proceso para la preparación de una composición que comprende ácido tartárico en la que entre el 55 y el 90% en peso del ácido tartárico es ácido meso-tartárico, que comprende las etapas de (i) preparar una mezcla acuosa que comprende entre el 35 y el 65% en peso de - una sal de dimetal alcalino de ácido L-tartárico, - una sal de dimetal alcalino de ácido D-tartárico, - una mezcla de sales de dimetal alcalino de ácido L-tartárico y ácido D-tartárico; o - una mezcla de sales de dimetal alcalino de ácido L-tartárico, ácido D-tartárico y ácido mesotartárico, y entre 2 y 15 % en peso de un metal alcalino o un hidróxido de metal alcalino, y (ii) agitar y calentar la mezcla acuosa hasta una temperatura de entre 100ºC y su punto de ebullición hasta que entre el 55 y el 90% en peso de ácido tartárico se ha convertido en ácido meso-tartárico.
Description
Claims (1)
-
imagen1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US183269P | 2000-02-17 | ||
| US18326909P | 2009-06-02 | 2009-06-02 | |
| EP09161723 | 2009-06-02 | ||
| EP09161723 | 2009-06-02 | ||
| PCT/EP2010/057287 WO2010139588A1 (en) | 2009-06-02 | 2010-05-27 | Process for the preparation of a composition comprising meso-tartaric acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2483115T3 true ES2483115T3 (es) | 2014-08-05 |
Family
ID=40996732
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES10724031.9T Active ES2483115T3 (es) | 2009-06-02 | 2010-05-27 | Procedimiento para la preparación de una composición que comprende ácido meso-tartárico |
Country Status (24)
| Country | Link |
|---|---|
| US (1) | US8759574B2 (es) |
| EP (1) | EP2438012B1 (es) |
| JP (1) | JP5437484B2 (es) |
| KR (1) | KR101809145B1 (es) |
| CN (1) | CN102099294B (es) |
| AU (1) | AU2010255850B2 (es) |
| BR (1) | BRPI1008276B1 (es) |
| CA (1) | CA2763612C (es) |
| DK (1) | DK2438012T3 (es) |
| EA (1) | EA020264B1 (es) |
| ES (1) | ES2483115T3 (es) |
| IL (1) | IL216106A (es) |
| MX (1) | MX2011012689A (es) |
| MY (1) | MY158515A (es) |
| PE (1) | PE20121053A1 (es) |
| PL (1) | PL2438012T3 (es) |
| PT (1) | PT2438012E (es) |
| SG (1) | SG176143A1 (es) |
| SI (1) | SI2438012T1 (es) |
| TN (1) | TN2011000598A1 (es) |
| TW (1) | TWI480259B (es) |
| UA (1) | UA106758C2 (es) |
| WO (1) | WO2010139588A1 (es) |
| ZA (1) | ZA201108234B (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AU2010255849B2 (en) * | 2009-06-02 | 2013-07-04 | Akzo Nobel Chemicals International B.V. | Non-caking salt composition, preparation process and use thereof |
| DK2512989T3 (en) * | 2009-12-16 | 2017-04-03 | Akzo Nobel Chemicals Int Bv | NON-CONSUMPTIONAL POTASSIUM CHLORIDE COMPOSITION, PROCEDURE FOR ITS PREPARATION AND APPLICATION |
| MX353523B (es) * | 2012-03-30 | 2018-01-16 | Akzo Nobel Chemicals Int Bv | Estabilización de una solución acuosa de una sal de hierro orgánica. |
| CN115524407B (zh) * | 2021-06-25 | 2024-10-29 | 武汉武药科技有限公司 | 一种有机酸的分离检测方法 |
| CN115286498B (zh) * | 2022-08-23 | 2024-08-16 | 佳化化学科技发展（上海）有限公司 | 一种内消旋酒石酸的制备方法 |
Family Cites Families (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2257284A (en) | 1938-11-26 | 1941-09-30 | Standard Brands Inc | Preparation of tartaric acids |
| US2947665A (en) | 1956-05-07 | 1960-08-02 | Jackson W Foster | Microbiological preparation of meso-tartaric acid |
| JPS5128616B2 (es) * | 1973-04-17 | 1976-08-20 | ||
| JPS5198215A (en) | 1975-02-19 | 1976-08-30 | Goseishusekisanno seizohoho | |
| DE2508228C3 (de) * | 1975-02-26 | 1987-01-22 | Degussa Ag, 6000 Frankfurt | Verfahren zur Herstellung von reiner Traubensäure und von Mesoweinsäure |
| FR2302293A1 (fr) * | 1975-02-26 | 1976-09-24 | Degussa | Procede pour la preparation d'acide tartrique rac |
| GB1520920A (en) | 1975-02-26 | 1978-08-09 | Degussa | Production of pure racemic acid and mesotartaric acid |
| DE2543333C2 (de) | 1975-09-29 | 1985-06-20 | Degussa Ag, 6000 Frankfurt | Verfahren zur gleichzeitigen Herstellung von reiner Traubensäure und von meso-Weinsäure |
| US3953504A (en) * | 1975-03-18 | 1976-04-27 | Nippon Peroxide Co., Ltd. | Racemization of optically active tartaric acid |
| JPS51108017A (ja) | 1975-03-20 | 1976-09-25 | Nippon Peroxide Co Ltd | Kogakukatsuseishusekisanenno rasemikaho |
| US4016207A (en) | 1975-11-05 | 1977-04-05 | Boise Cascade Corporation | Hydrolyzing di- and tricarboxy celluloses with sulfurous acid |
| US3998878A (en) | 1975-11-05 | 1976-12-21 | Boise Cascade Corporation | Selectively separating oxalic, tartaric, glyoxylic and erythronic acids from aqueous solutions containing the same |
| FI855185A7 (fi) | 1985-12-31 | 1987-07-01 | Vsesojuznoe Nauchno Proizvodstvennoe | Menetelmä jauhemaisen rautanatrium-tartraattikompleksin valmistamiseksi. |
| CN1172852C (zh) * | 1999-04-02 | 2004-10-27 | 阿克佐诺贝尔公司 | 不结块氯化钠晶体、制备它们的方法和它们在电解过程中的应用 |
| JP2004123685A (ja) | 2002-09-30 | 2004-04-22 | Yoshiyuki Akiyama | メゾ酒石酸カルシウムの触媒を用いた合成方法 |
| AU2010255849B2 (en) * | 2009-06-02 | 2013-07-04 | Akzo Nobel Chemicals International B.V. | Non-caking salt composition, preparation process and use thereof |
-
2010
- 2010-05-27 MX MX2011012689A patent/MX2011012689A/es active IP Right Grant
- 2010-05-27 DK DK10724031.9T patent/DK2438012T3/da active
- 2010-05-27 EA EA201171467A patent/EA020264B1/ru not_active IP Right Cessation
- 2010-05-27 MY MYPI2011005723A patent/MY158515A/en unknown
- 2010-05-27 PL PL10724031T patent/PL2438012T3/pl unknown
- 2010-05-27 ES ES10724031.9T patent/ES2483115T3/es active Active
- 2010-05-27 AU AU2010255850A patent/AU2010255850B2/en active Active
- 2010-05-27 WO PCT/EP2010/057287 patent/WO2010139588A1/en not_active Ceased
- 2010-05-27 KR KR1020117028023A patent/KR101809145B1/ko not_active Expired - Fee Related
- 2010-05-27 UA UAA201115311A patent/UA106758C2/uk unknown
- 2010-05-27 CA CA2763612A patent/CA2763612C/en active Active
- 2010-05-27 US US13/322,319 patent/US8759574B2/en active Active
- 2010-05-27 EP EP10724031.9A patent/EP2438012B1/en active Active
- 2010-05-27 PT PT107240319T patent/PT2438012E/pt unknown
- 2010-05-27 BR BRPI1008276-0A patent/BRPI1008276B1/pt not_active IP Right Cessation
- 2010-05-27 SI SI201030680T patent/SI2438012T1/sl unknown
- 2010-05-27 PE PE2011002007A patent/PE20121053A1/es active IP Right Grant
- 2010-05-27 JP JP2012513547A patent/JP5437484B2/ja not_active Expired - Fee Related
- 2010-05-27 CN CN201080002132.8A patent/CN102099294B/zh active Active
- 2010-05-27 SG SG2011085032A patent/SG176143A1/en unknown
- 2010-06-01 TW TW099117639A patent/TWI480259B/zh not_active IP Right Cessation
-
2011
- 2011-11-03 IL IL216106A patent/IL216106A/en active IP Right Grant
- 2011-11-09 ZA ZA2011/08234A patent/ZA201108234B/en unknown
- 2011-11-25 TN TNP2011000598A patent/TN2011000598A1/en unknown
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