ES2637347T3 - Procedimiento para la reducción del contenido de 3-MCPD en aceites vegetales refinados - Google Patents
Procedimiento para la reducción del contenido de 3-MCPD en aceites vegetales refinados Download PDFInfo
- Publication number
- ES2637347T3 ES2637347T3 ES09771302.8T ES09771302T ES2637347T3 ES 2637347 T3 ES2637347 T3 ES 2637347T3 ES 09771302 T ES09771302 T ES 09771302T ES 2637347 T3 ES2637347 T3 ES 2637347T3
- Authority
- ES
- Spain
- Prior art keywords
- oil
- mcpd
- bleaching
- h3po4
- degumming
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- SSZWWUDQMAHNAQ-UHFFFAOYSA-N 3-chloropropane-1,2-diol Chemical compound OCC(O)CCl SSZWWUDQMAHNAQ-UHFFFAOYSA-N 0.000 title abstract description 13
- 238000000034 method Methods 0.000 title abstract 2
- 235000015112 vegetable and seed oil Nutrition 0.000 title abstract 2
- 239000008158 vegetable oil Substances 0.000 title abstract 2
- 238000004061 bleaching Methods 0.000 abstract description 12
- 239000003921 oil Substances 0.000 abstract description 9
- 235000019198 oils Nutrition 0.000 abstract description 9
- 239000002253 acid Substances 0.000 abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- 239000002689 soil Substances 0.000 abstract description 2
- 239000010779 crude oil Substances 0.000 abstract 2
- 238000001914 filtration Methods 0.000 abstract 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 22
- 235000011007 phosphoric acid Nutrition 0.000 description 21
- 230000003247 decreasing effect Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 235000019482 Palm oil Nutrition 0.000 description 2
- FAJFGLZHUIUNSS-NSHDSACASA-N benzyl (2s)-2-amino-5-[[amino(nitramido)methylidene]amino]pentanoate Chemical compound [O-][N+](=O)NC(N)=NCCC[C@H](N)C(=O)OCC1=CC=CC=C1 FAJFGLZHUIUNSS-NSHDSACASA-N 0.000 description 2
- 239000012496 blank sample Substances 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000002540 palm oil Substances 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/006—Refining fats or fatty oils by extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
- C11B3/14—Refining fats or fatty oils by distillation with the use of indifferent gases or vapours, e.g. steam
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Paper (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008060059A DE102008060059A1 (de) | 2008-12-02 | 2008-12-02 | Verfahren zur Reduzierung des 3-MCPD-Gehalts in raffinierten Pflanzenölen |
| DE102008060059 | 2008-12-02 | ||
| PCT/EP2009/008557 WO2010063450A1 (de) | 2008-12-02 | 2009-12-01 | Verfahren zur reduzierung des 3-mcpd-gehalts in raffinierten pflanzenöllen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2637347T3 true ES2637347T3 (es) | 2017-10-11 |
Family
ID=41728488
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES09771302.8T Active ES2637347T3 (es) | 2008-12-02 | 2009-12-01 | Procedimiento para la reducción del contenido de 3-MCPD en aceites vegetales refinados |
Country Status (8)
| Country | Link |
|---|---|
| EP (1) | EP2361298B1 (pl) |
| DE (1) | DE102008060059A1 (pl) |
| DK (1) | DK2361298T3 (pl) |
| ES (1) | ES2637347T3 (pl) |
| HU (1) | HUE035623T2 (pl) |
| PL (1) | PL2361298T3 (pl) |
| PT (1) | PT2361298T (pl) |
| WO (1) | WO2010063450A1 (pl) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MY155702A (en) | 2009-06-30 | 2015-11-13 | Sime Darby Malaysia Berhad | Process for manufacturing palm oil fractions containing virtually no 3-monochloropropanediol fatty acid esters |
| WO2011040539A1 (ja) * | 2009-09-30 | 2011-04-07 | 不二製油株式会社 | グリセリド油脂中のクロロプロパノール類及びその形成物質、グリシドール脂肪酸エステルを低減する方法 |
| CN102334563B (zh) | 2010-07-16 | 2015-03-25 | 丰益(上海)生物技术研发中心有限公司 | 控制油脂中3-氯-1,2-丙二醇或其酯含量的方法 |
| CZ303281B6 (cs) * | 2010-10-27 | 2012-07-11 | Vysoká škola chemicko-technologická v Praze | Zpusob zabránení vzniku acylderivátu monochlorpropandiolu pri vysokoteplotních úpravách oleju a tuku |
| GB201019639D0 (en) | 2010-11-19 | 2010-12-29 | Loders Croklaan Bv | Method |
| DK3388502T3 (da) * | 2011-02-10 | 2021-05-31 | Cargill Inc | Fremgangsmåde til reduktion af indholdet af 3-mcpd-glycidylester i olier |
| EP2502500B1 (en) * | 2011-03-25 | 2013-08-21 | Nestec S.A. | Producing refined plant oils from washed crude plant oil |
| JP2011174091A (ja) * | 2011-06-01 | 2011-09-08 | Showa Sangyo Co Ltd | 遊離塩素を除去する工程を設けたパーム油の製造方法 |
| EP2738243B1 (en) | 2011-07-29 | 2016-10-05 | The Nisshin Oillio Group, Ltd. | Purified glyceride composition and method for producing purified glyceride composition |
| US9217120B2 (en) | 2011-12-23 | 2015-12-22 | Loders Croklann B.V. | Method of treating a vegetable oil |
| WO2014012548A1 (en) | 2012-07-18 | 2014-01-23 | Aarhuskarlshamn Ab | Reduction of mcpd-compounds in refined plant oil for food |
| WO2014081279A1 (en) | 2012-11-21 | 2014-05-30 | Universiti Putra Malaysia | An improved palm oil refining process |
| CN103525548B (zh) * | 2013-11-06 | 2014-10-01 | 江南大学 | 一种用于降低植物油中氯源及3-氯-1,2-丙二醇酯前体物质含量的脱胶方法 |
| PL3154374T3 (pl) | 2014-05-16 | 2018-12-31 | Sime Darby Malaysia Berhad | Sposób rafinacji surowego oleju z owoców palmowych |
| GB2538758A (en) | 2015-05-27 | 2016-11-30 | Green Lizard Tech Ltd | Process for removing chloropropanols and/or glycidol |
| EP3098292A1 (en) | 2015-05-27 | 2016-11-30 | Evonik Degussa GmbH | A process for refining glyceride oil comprising a basic quaternary ammonium salt treatment |
| EP3098293A1 (en) | 2015-05-27 | 2016-11-30 | Evonik Degussa GmbH | A process for removing metal from a metal-containing glyceride oil comprising a basic quaternary ammonium salt treatment |
| MY204082A (en) | 2015-08-25 | 2024-08-06 | Dsm Ip Assets Bv | Refined oil compositions and methods for making |
| WO2018156013A1 (en) | 2017-02-21 | 2018-08-30 | Sime Darby Plantation Berhad | Process for producing refined palm fruit oil |
| EP3321348B1 (en) | 2017-08-23 | 2019-12-18 | Bunge Loders Croklaan B.V. | Process for refining vegetable oil with suppression of unwanted impurities |
| EP3483237A1 (de) | 2017-11-10 | 2019-05-15 | Evonik Degussa GmbH | Verfahren zur extraktion von fettsäuren aus triglyceridölen |
| CA3089369A1 (en) * | 2018-02-07 | 2019-08-15 | Cargill, Incorporated | Palm oil without unwanted contaminants |
| US12152218B2 (en) | 2018-02-07 | 2024-11-26 | Cargill, Incorporated | Liquid oils without unwanted contaminants |
| US11634657B2 (en) | 2018-05-07 | 2023-04-25 | Arisdyne Systems, Inc. | Method for refined palm oil production with reduced 3-MCPD formation |
| PL238351B1 (pl) | 2018-08-27 | 2021-08-09 | Komagra Spolka Z Ograniczona Odpowiedzialnoscia | Sposób wytwarzania rafinowanego oleju jadalnego o niskiej zawartości niepożądanych 3-MPCD, 2-MPCD oraz glicydów |
| EP3739027A1 (de) | 2019-05-14 | 2020-11-18 | Clariant International Ltd | Verfahren zur reduzierung des 3-mcpd-gehalts in raffinierten pflanzenölen |
| US12384984B2 (en) | 2019-11-15 | 2025-08-12 | Societe Des Produits Nestle S.A. | Prevention of MCPD formation by auxiliary degumming |
| US20230242838A1 (en) * | 2020-05-28 | 2023-08-03 | Societe Des Produits Nestle S.A. | Prevention of mcpd formation by high temperature washing |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4939115A (en) * | 1986-01-28 | 1990-07-03 | W. R. Grace & Co.-Conn. | Organic acid-treated amorphous silicas for refining glyceride oils |
| DE3643848A1 (de) * | 1986-12-22 | 1988-09-01 | Natec Inst Naturwiss | Verfahren zur herstellung hochraffinierter essbarer glyceridoele mit einem anteil an ungesaettigten fettsaeuren im triglyceridverband und ihre verwendung |
| US5151211A (en) | 1988-12-05 | 1992-09-29 | Oil-Dri Corporation Of America | Oil bleaching method and composition for same |
| US5004570A (en) | 1988-12-05 | 1991-04-02 | Oil-Dri Corporation Of America | Oil bleaching method and composition for same |
| US6346286B1 (en) | 1995-04-26 | 2002-02-12 | Oil-Dri Corporation Of America | Sorptive purification for edible oils |
| CA2260397A1 (en) * | 1999-01-29 | 2000-07-29 | Atlantis Marine Inc. | Method of converting rendered triglyceride oil from marine sources into bland, stable food oil |
| US6638551B1 (en) * | 2002-03-05 | 2003-10-28 | Selecto Scientific, Inc. | Methods and compositions for purifying edible oil |
| JP2005527237A (ja) * | 2002-05-30 | 2005-09-15 | カウンシル・オブ・サイエンティフィック・アンド・インダストリアル・リサーチ | 植物油の物理的精製を行うための前処理方法 |
| DE602005021675D1 (de) * | 2004-11-04 | 2010-07-15 | Monsanto Technology Llc | Verfahren zur herstellung von ölzusammensetzungen |
| SI1893329T1 (sl) * | 2005-06-08 | 2012-02-29 | Sued Chemie Ag | Proizvodnja belilne zemlje z aktivacijo povrĺ insko bogatih glin |
| DE102006035064A1 (de) | 2006-07-28 | 2008-01-31 | Süd-Chemie AG | Vereinfachtes Verfahren zur Raffination von Fetten und Ölen |
-
2008
- 2008-12-02 DE DE102008060059A patent/DE102008060059A1/de not_active Withdrawn
-
2009
- 2009-12-01 ES ES09771302.8T patent/ES2637347T3/es active Active
- 2009-12-01 WO PCT/EP2009/008557 patent/WO2010063450A1/de not_active Ceased
- 2009-12-01 HU HUE09771302A patent/HUE035623T2/en unknown
- 2009-12-01 EP EP09771302.8A patent/EP2361298B1/de not_active Not-in-force
- 2009-12-01 PL PL09771302T patent/PL2361298T3/pl unknown
- 2009-12-01 DK DK09771302.8T patent/DK2361298T3/en active
- 2009-12-01 PT PT97713028T patent/PT2361298T/pt unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DK2361298T3 (en) | 2017-07-24 |
| PL2361298T3 (pl) | 2017-10-31 |
| PT2361298T (pt) | 2017-08-25 |
| WO2010063450A1 (de) | 2010-06-10 |
| EP2361298A1 (de) | 2011-08-31 |
| HUE035623T2 (en) | 2018-05-28 |
| EP2361298B1 (de) | 2017-05-17 |
| DE102008060059A1 (de) | 2010-06-10 |
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