ES2646616T3 - Óxidos cerámicos esféricos nanocristalinos, proceso para la síntesis y uso de los mismos - Google Patents

Óxidos cerámicos esféricos nanocristalinos, proceso para la síntesis y uso de los mismos Download PDF

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Publication number
ES2646616T3
ES2646616T3 ES08807822.5T ES08807822T ES2646616T3 ES 2646616 T3 ES2646616 T3 ES 2646616T3 ES 08807822 T ES08807822 T ES 08807822T ES 2646616 T3 ES2646616 T3 ES 2646616T3
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Prior art keywords
synthesis
spherical ceramic
detonation
phase based
temperature
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ES08807822.5T
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English (en)
Inventor
João Manuel CALADO DA SILVA
Elsa Marisa Dos Santos Antunes
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Innovnano- Materiais Avancados Sa
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Innovnano- Materiais Avancados Sa
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/32—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of elements or compounds in the liquid or solid state or in non-aqueous solution, e.g. sol-gel process
    • C01B13/328—Methods for preparing oxides or hydroxides in general by oxidation or hydrolysis of elements or compounds in the liquid or solid state or in non-aqueous solution, e.g. sol-gel process by processes making use of emulsions, e.g. the kerosine process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/06—Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
    • B01J3/08—Application of shock waves for chemical reactions or for modifying the crystal structure of substances
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/18—Methods for preparing oxides or hydroxides in general by thermal decomposition of compounds, e.g. of salts or hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general
    • C01B13/14—Methods for preparing oxides or hydroxides in general
    • C01B13/18—Methods for preparing oxides or hydroxides in general by thermal decomposition of compounds, e.g. of salts or hydroxides
    • C01B13/185—Preparing mixtures of oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/02—Magnesia
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/02—Magnesia
    • C01F5/04—Magnesia by oxidation of metallic magnesium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F7/00—Compounds of aluminium
    • C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
    • C01F7/42—Preparation of aluminium oxide or hydroxide from metallic aluminium, e.g. by oxidation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G23/00—Compounds of titanium
    • C01G23/04—Oxides; Hydroxides
    • C01G23/047—Titanium dioxide
    • C01G23/053—Producing by wet processes, e.g. hydrolysing titanium salts
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G25/00—Compounds of zirconium
    • C01G25/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G3/00—Compounds of copper
    • C01G3/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G45/00—Compounds of manganese
    • C01G45/02—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G53/00—Compounds of nickel
    • C01G53/04—Oxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G9/00—Compounds of zinc
    • C01G9/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/60—Compounds characterised by their crystallite size
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C01P2004/53—Particles with a specific particle size distribution bimodal size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/32—Thermal properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Compositions Of Oxide Ceramics (AREA)
  • Cosmetics (AREA)

Abstract

Proceso para la síntesis de polvo de óxidos cerámicos esféricos nanocristalinos caracterizado por que se lleva a cabo por detonación de una emulsión de agua en aceite (W/O) que comprende metales, una fase oxidante interna basada en una solución acuosa de nitrato de amonio que comprende sales metálicas de los metales correspondientes disueltos en ella para ajustar la temperatura de detonación y una fase externa de combustible basada en compuestos orgánicos, las dos fases íntimamente unidas por un tensioactivo, a una temperatura en la zona de reacción (punto C,J (Chapman, Jouguet)) que es mayor que el punto de fusión del óxido.

Description

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Claims (1)

  1. imagen1
ES08807822.5T 2007-09-28 2008-09-26 Óxidos cerámicos esféricos nanocristalinos, proceso para la síntesis y uso de los mismos Active ES2646616T3 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
PT10383807 2007-09-28
PT103838A PT103838B (pt) 2007-09-28 2007-09-28 Óxidos cerâmicos esféricos nanocristalinos, processo para a sua síntese e respectivas utilizações
PCT/IB2008/053932 WO2009040770A2 (en) 2007-09-28 2008-09-26 Nanocrystaline spherical ceramic oxides, process for the synthesis and use thereof

Publications (1)

Publication Number Publication Date
ES2646616T3 true ES2646616T3 (es) 2017-12-14

Family

ID=40511985

Family Applications (1)

Application Number Title Priority Date Filing Date
ES08807822.5T Active ES2646616T3 (es) 2007-09-28 2008-09-26 Óxidos cerámicos esféricos nanocristalinos, proceso para la síntesis y uso de los mismos

Country Status (13)

Country Link
US (2) US9249020B2 (es)
EP (1) EP2205526B1 (es)
JP (1) JP5721434B2 (es)
KR (1) KR20100097090A (es)
CN (2) CN101855166A (es)
BR (1) BRPI0817504A2 (es)
CA (1) CA2700984C (es)
EA (1) EA018086B1 (es)
EG (1) EG26634A (es)
ES (1) ES2646616T3 (es)
PT (2) PT103838B (es)
WO (1) WO2009040770A2 (es)
ZA (1) ZA201002083B (es)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PT104085B (pt) * 2008-05-27 2009-08-07 Cuf Companhia Uniao Fabril Sgp Materiais cerâmicos de dimensão nanométrica, processo para a sua síntese e respectivas utilizações
WO2010059070A1 (en) * 2008-10-13 2010-05-27 Cuf-Companhia União Fabril, Sgps, S.A. Ceramic powders coated with a nanoparticle layer and process for obtaining thereof
PT105339A (pt) * 2010-10-15 2012-04-16 Innovnano Materiais Avancados S A Processo de síntese de nanomateriais a partir da preparação e detonação de uma emulsão, respectivos produtos e emulsões utilizadas
PT105340A (pt) * 2010-10-18 2012-04-18 Innovnano Materiais Avancados S A Processo contínuo de síntese de nanomateriais a partir da emulsificação e detonação em simultâneo de uma emulsão
TW201333284A (zh) * 2012-01-31 2013-08-16 Anf Technology Ltd 從鋁熔體合成氧化鋁奈米纖維的方法與系統
CA2972974C (en) 2014-05-13 2021-07-13 University Of Utah Research Foundation Production of substantially spherical metal powders
WO2016090052A1 (en) 2014-12-02 2016-06-09 University Of Utah Research Foundation Molten salt de-oxygenation of metal powders
CN106045526A (zh) * 2016-08-22 2016-10-26 中国科学院力学研究所 一种液态co2制备陶瓷粉体的方法

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JP3019375B2 (ja) * 1989-08-23 2000-03-13 日本油脂株式会社 油中水型エマルション爆薬組成物
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JP3749391B2 (ja) * 1998-03-04 2006-02-22 トヨタ自動車株式会社 排ガス浄化用触媒及びその製造方法
JP3984383B2 (ja) * 1998-12-16 2007-10-03 日本工機株式会社 油中水滴型エマルション爆薬組成物の製造方法
IL151794A0 (en) * 2000-03-31 2003-04-10 Bayer Ag Polishing agent and method for producing planar layers
JP4032652B2 (ja) * 2001-02-23 2008-01-16 株式会社豊田中央研究所 複合酸化物粉末及びその製造方法
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Also Published As

Publication number Publication date
JP5721434B2 (ja) 2015-05-20
AU2008303156A1 (en) 2009-04-02
US20110039103A1 (en) 2011-02-17
US9249020B2 (en) 2016-02-02
JP2010540384A (ja) 2010-12-24
WO2009040770A3 (en) 2009-06-18
CN106006568B (zh) 2019-01-11
EA201000380A1 (ru) 2010-10-29
PT2205526T (pt) 2017-11-15
CA2700984C (en) 2016-02-23
CN101855166A (zh) 2010-10-06
WO2009040770A4 (en) 2009-08-20
ZA201002083B (en) 2011-05-25
CN106006568A (zh) 2016-10-12
PT103838B (pt) 2008-11-03
BRPI0817504A2 (pt) 2015-03-24
EG26634A (en) 2014-04-14
EP2205526B1 (en) 2017-08-16
PT103838A (pt) 2008-02-19
EA018086B1 (ru) 2013-05-30
KR20100097090A (ko) 2010-09-02
CA2700984A1 (en) 2009-04-02
WO2009040770A2 (en) 2009-04-02
EP2205526A2 (en) 2010-07-14
US20160145117A1 (en) 2016-05-26

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