ES2981402R1 - Fosfato de hierro similar a una hoja nanométrica, método de preparación y uso del mismo - Google Patents

Fosfato de hierro similar a una hoja nanométrica, método de preparación y uso del mismo Download PDF

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Publication number
ES2981402R1
ES2981402R1 ES202390226A ES202390226A ES2981402R1 ES 2981402 R1 ES2981402 R1 ES 2981402R1 ES 202390226 A ES202390226 A ES 202390226A ES 202390226 A ES202390226 A ES 202390226A ES 2981402 R1 ES2981402 R1 ES 2981402R1
Authority
ES
Spain
Prior art keywords
nanosheet
preparation
iron phosphate
phosphate
iron
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
ES202390226A
Other languages
English (en)
Other versions
ES2981402A2 (es
ES2981402B2 (es
Inventor
Jinliang Duan
Changdong Li
Yang Xia
Dingshan Ruan
Ruokui Chen
Yanchao Qiao
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hunan Brunp Recycling Technology Co Ltd
Guangdong Brunp Recycling Technology Co Ltd
Hunan Bangpu Automobile Circulation Co Ltd
Original Assignee
Hunan Brunp Recycling Technology Co Ltd
Guangdong Brunp Recycling Technology Co Ltd
Hunan Bangpu Automobile Circulation Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hunan Brunp Recycling Technology Co Ltd, Guangdong Brunp Recycling Technology Co Ltd, Hunan Bangpu Automobile Circulation Co Ltd filed Critical Hunan Brunp Recycling Technology Co Ltd
Publication of ES2981402A2 publication Critical patent/ES2981402A2/es
Publication of ES2981402R1 publication Critical patent/ES2981402R1/es
Application granted granted Critical
Publication of ES2981402B2 publication Critical patent/ES2981402B2/es
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/37Phosphates of heavy metals
    • C01B25/375Phosphates of heavy metals of iron
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/45Phosphates containing plural metal, or metal and ammonium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/20Particle morphology extending in two dimensions, e.g. plate-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/10Solid density
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028Positive electrodes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Compounds Of Iron (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Soft Magnetic Materials (AREA)
ES202390226A 2021-07-23 2022-06-06 Fosfato de hierro similar a una hoja nanométrica, método de preparación y uso del mismo Active ES2981402B2 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
CN202110834587.6A CN113603071B (zh) 2021-07-23 2021-07-23 一种纳米片状磷酸铁及其制备方法和应用
PCT/CN2022/097182 WO2023000846A1 (zh) 2021-07-23 2022-06-06 一种纳米片状磷酸铁及其制备方法和应用

Publications (3)

Publication Number Publication Date
ES2981402A2 ES2981402A2 (es) 2024-10-08
ES2981402R1 true ES2981402R1 (es) 2025-02-14
ES2981402B2 ES2981402B2 (es) 2025-10-17

Family

ID=78305214

Family Applications (1)

Application Number Title Priority Date Filing Date
ES202390226A Active ES2981402B2 (es) 2021-07-23 2022-06-06 Fosfato de hierro similar a una hoja nanométrica, método de preparación y uso del mismo

Country Status (8)

Country Link
US (1) US20240317583A1 (es)
CN (1) CN113603071B (es)
DE (1) DE112022002564B4 (es)
ES (1) ES2981402B2 (es)
GB (1) GB2621302A (es)
HU (1) HUP2400061A1 (es)
MA (1) MA63873A1 (es)
WO (1) WO2023000846A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113603071B (zh) * 2021-07-23 2023-11-03 广东邦普循环科技有限公司 一种纳米片状磷酸铁及其制备方法和应用
CN115231539B (zh) * 2022-07-12 2023-10-10 国环电池科技(苏州)有限公司 一种高纯度磷酸铁的制备方法
CN114988383B (zh) * 2022-07-12 2023-12-15 华辰环保能源(广州)有限责任公司 一种电池级的磷酸铁高效制备方法
CN116374978A (zh) * 2023-04-26 2023-07-04 四川大学 制备磷酸铁的方法
CN116534821A (zh) * 2023-05-10 2023-08-04 东华理工大学 一种以硫酸亚铁为原料联产纳米磷酸铁和硫酸钙晶须的方法
MA61717B1 (fr) * 2023-07-24 2025-08-29 Universite Mohammed VI Polytechnique Procede de preparation de lithium fer phosphate micrometrique
CN116946998B (zh) * 2023-08-11 2024-01-26 湖北洋丰美新能源科技有限公司 一种磷酸铁的合成工艺及其合成的磷酸铁
CN117658089A (zh) * 2023-10-12 2024-03-08 浙江友山新材料科技有限公司 一种高性能球形磷酸铁制备方法
CN117602603A (zh) * 2023-11-24 2024-02-27 佛山市德方纳米科技有限公司 纳米磷酸铁及其制备方法、纳米磷酸铁锂正极材料及其制备方法和应用

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110068295A1 (en) * 2009-09-18 2011-03-24 A123 Systems, Inc. Ferric phosphate and methods of preparation thereof
US20120039783A1 (en) * 2009-02-26 2012-02-16 Chemische Fabrik Budenheim Kg Production of iron orthophosphate
US20120058039A1 (en) * 2010-03-02 2012-03-08 Guiqing Huang HIGH PERFORMANCE CATHODE MATERIAL LiFePO4, ITS PRECURSORS AND METHODS OF MAKING THEREOF
US20150203354A1 (en) * 2012-08-10 2015-07-23 Samsung Fine Chemicals Co., Ltd Method for preparing nano-sized iron phosphate particles
CN110294466A (zh) * 2019-08-19 2019-10-01 四川轻化工大学 一种纳米片状磷酸铁的制备方法
WO2019200557A1 (zh) * 2018-04-18 2019-10-24 南通百川新材料有限公司 一种磷酸铁的制备方法
CN110482512A (zh) * 2019-07-12 2019-11-22 乳源东阳光磁性材料有限公司 一种电池级磷酸铁的制备方法
CN112645299A (zh) * 2020-12-03 2021-04-13 广东邦普循环科技有限公司 一种磷酸铁的制备方法和应用

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102009968B (zh) 2011-01-14 2012-08-08 武汉大学 一种纳米片状FePO4·2H2O的制备方法
TWI448420B (zh) * 2011-06-17 2014-08-11 Nat Univ Tsing Hua 鋰離子電池之磷酸亞鐵前驅物、使用其製備之磷酸鋰鐵粉末、及其製作方法
CN104129770B (zh) * 2014-07-14 2016-01-20 湖北高博科技有限公司 一种纳米级磷酸铁及其制备方法
CN104817059B (zh) 2015-04-29 2017-07-18 江西东华科技园有限责任公司 一种由铁粉和磷酸反应制备电池级磷酸铁的方法
CN106876700B (zh) * 2016-11-02 2019-10-01 杨晓钢 两步共沉淀制备微-纳多孔结构磷酸铁前驱体与磷酸铁锂正极材料的方法
CN110615418A (zh) * 2019-06-28 2019-12-27 湖北虹润高科新材料有限公司 一种铁粉制备电池级磷酸铁的制备方法
CN113044823B (zh) * 2021-02-24 2022-05-06 湖南雅城新材料有限公司 一种磷酸铁材料及其制备方法与应用
CN113603071B (zh) * 2021-07-23 2023-11-03 广东邦普循环科技有限公司 一种纳米片状磷酸铁及其制备方法和应用

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20120039783A1 (en) * 2009-02-26 2012-02-16 Chemische Fabrik Budenheim Kg Production of iron orthophosphate
US20110068295A1 (en) * 2009-09-18 2011-03-24 A123 Systems, Inc. Ferric phosphate and methods of preparation thereof
US20120058039A1 (en) * 2010-03-02 2012-03-08 Guiqing Huang HIGH PERFORMANCE CATHODE MATERIAL LiFePO4, ITS PRECURSORS AND METHODS OF MAKING THEREOF
US20150203354A1 (en) * 2012-08-10 2015-07-23 Samsung Fine Chemicals Co., Ltd Method for preparing nano-sized iron phosphate particles
WO2019200557A1 (zh) * 2018-04-18 2019-10-24 南通百川新材料有限公司 一种磷酸铁的制备方法
CN110482512A (zh) * 2019-07-12 2019-11-22 乳源东阳光磁性材料有限公司 一种电池级磷酸铁的制备方法
CN110294466A (zh) * 2019-08-19 2019-10-01 四川轻化工大学 一种纳米片状磷酸铁的制备方法
CN112645299A (zh) * 2020-12-03 2021-04-13 广东邦普循环科技有限公司 一种磷酸铁的制备方法和应用

Also Published As

Publication number Publication date
US20240317583A1 (en) 2024-09-26
DE112022002564T5 (de) 2024-03-07
CN113603071A (zh) 2021-11-05
GB202318497D0 (en) 2024-01-17
ES2981402A2 (es) 2024-10-08
HUP2400061A1 (hu) 2024-04-28
CN113603071B (zh) 2023-11-03
WO2023000846A1 (zh) 2023-01-26
DE112022002564B4 (de) 2025-03-13
MA63873A1 (fr) 2024-12-31
ES2981402B2 (es) 2025-10-17
GB2621302A (en) 2024-02-07

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