ES441141A1 - Un procedimiento para la obtencion de la 1, 4, 5-trimetil-2-(3, 4, 5-trimetoxibencil)-1, 2, 3, 6-tetrahidropiridina. - Google Patents

Un procedimiento para la obtencion de la 1, 4, 5-trimetil-2-(3, 4, 5-trimetoxibencil)-1, 2, 3, 6-tetrahidropiridina.

Info

Publication number: ES441141A1
Authority: ES; Spain
Prior art keywords: formula; trimethyl; trimethoxybenzyl; see formula; translation
Prior art date: 1975-09-20
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

ES441141A

Other languages

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Laboratorios Made SA

Original Assignee

Laboratorios Made SA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1975-09-20

Filing date

1975-09-20

Publication date

1977-03-16

1975-09-20 Application filed by Laboratorios Made SA filed Critical Laboratorios Made SA

1975-09-20 Priority to ES441141A priority Critical patent/ES441141A1/es

1977-03-16 Publication of ES441141A1 publication Critical patent/ES441141A1/es

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title abstract 2
239000002253 acid Substances 0.000 abstract 4
150000007513 acids Chemical class 0.000 abstract 3
125000005806 3,4,5-trimethoxybenzyl group Chemical group [H]C1=C(OC([H])([H])[H])C(OC([H])([H])[H])=C(OC([H])([H])[H])C([H])=C1C([H])([H])* 0.000 abstract 2
NURQLCJSMXZBPC-UHFFFAOYSA-N 3,4-dimethylpyridine Chemical compound CC1=CC=NC=C1C NURQLCJSMXZBPC-UHFFFAOYSA-N 0.000 abstract 2
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 2
230000015572 biosynthetic process Effects 0.000 abstract 2
239000000203 mixture Substances 0.000 abstract 2
150000003839 salts Chemical class 0.000 abstract 2
LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 abstract 2
238000003786 synthesis reaction Methods 0.000 abstract 2
FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 abstract 2
UMGQVIOGHDLFBI-UHFFFAOYSA-N (3,4-dimethylpyridin-2-yl)-(3,4,5-trimethoxyphenyl)methanol Chemical compound COC1=C(OC)C(OC)=CC(C(O)C=2C(=C(C)C=CN=2)C)=C1 UMGQVIOGHDLFBI-UHFFFAOYSA-N 0.000 abstract 1
MUTMUJVXPZWDPY-UHFFFAOYSA-N 2-bromo-3,4-dimethylpyridine Chemical compound CC1=CC=NC(Br)=C1C MUTMUJVXPZWDPY-UHFFFAOYSA-N 0.000 abstract 1
BMYNFMYTOJXKLE-UHFFFAOYSA-N 3-azaniumyl-2-hydroxypropanoate Chemical compound NCC(O)C(O)=O BMYNFMYTOJXKLE-UHFFFAOYSA-N 0.000 abstract 1
WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical compound [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 abstract 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
ZLUAOXKTEGETHI-UHFFFAOYSA-N [I-].COC=1C=C(CC2=[NH+]C=C(C(=C2)C)C)C=C(C=1OC)OC Chemical compound [I-].COC=1C=C(CC2=[NH+]C=C(C(=C2)C)C)C=C(C=1OC)OC ZLUAOXKTEGETHI-UHFFFAOYSA-N 0.000 abstract 1
-1 boron tetrahydride Chemical compound 0.000 abstract 1
GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Substances BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 abstract 1
229910052794 bromium Inorganic materials 0.000 abstract 1
238000004440 column chromatography Methods 0.000 abstract 1
INQOMBQAUSQDDS-UHFFFAOYSA-N iodomethane Chemical compound IC INQOMBQAUSQDDS-UHFFFAOYSA-N 0.000 abstract 1
238000002360 preparation method Methods 0.000 abstract 1
229910052708 sodium Inorganic materials 0.000 abstract 1
239000011734 sodium Substances 0.000 abstract 1
ODZPKZBBUMBTMG-UHFFFAOYSA-N sodium amide Chemical compound [NH2-].[Na+] ODZPKZBBUMBTMG-UHFFFAOYSA-N 0.000 abstract 1
235000010288 sodium nitrite Nutrition 0.000 abstract 1

Landscapes

Pyridine Compounds (AREA)

ES441141A 1975-09-20 1975-09-20 Un procedimiento para la obtencion de la 1, 4, 5-trimetil-2-(3, 4, 5-trimetoxibencil)-1, 2, 3, 6-tetrahidropiridina. Expired ES441141A1 (es)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
ES441141A ES441141A1 (es)	1975-09-20	1975-09-20	Un procedimiento para la obtencion de la 1, 4, 5-trimetil-2-(3, 4, 5-trimetoxibencil)-1, 2, 3, 6-tetrahidropiridina.

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
ES441141A ES441141A1 (es)	1975-09-20	1975-09-20	Un procedimiento para la obtencion de la 1, 4, 5-trimetil-2-(3, 4, 5-trimetoxibencil)-1, 2, 3, 6-tetrahidropiridina.

Publications (1)

Publication Number	Publication Date
ES441141A1 true ES441141A1 (es)	1977-03-16

Family

ID=8470019

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
ES441141A Expired ES441141A1 (es)	1975-09-20	1975-09-20	Un procedimiento para la obtencion de la 1, 4, 5-trimetil-2-(3, 4, 5-trimetoxibencil)-1, 2, 3, 6-tetrahidropiridina.

Country Status (1)

Country	Link
ES (1)	ES441141A1 (es)

1975
- 1975-09-20 ES ES441141A patent/ES441141A1/es not_active Expired

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