ES458631A1 - Procedimiento para la preparacion de acido tereftalico. - Google Patents
Procedimiento para la preparacion de acido tereftalico.Info
- Publication number
- ES458631A1 ES458631A1 ES458631A ES458631A ES458631A1 ES 458631 A1 ES458631 A1 ES 458631A1 ES 458631 A ES458631 A ES 458631A ES 458631 A ES458631 A ES 458631A ES 458631 A1 ES458631 A1 ES 458631A1
- Authority
- ES
- Spain
- Prior art keywords
- terephthalic acid
- preparation
- stage process
- aids
- prepared
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 title abstract 6
- LRUDDHYVRFQYCN-UHFFFAOYSA-L dipotassium;terephthalate Chemical compound [K+].[K+].[O-]C(=O)C1=CC=C(C([O-])=O)C=C1 LRUDDHYVRFQYCN-UHFFFAOYSA-L 0.000 abstract 1
- 239000000835 fiber Substances 0.000 abstract 1
- 229920000728 polyester Polymers 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/416—Henkel reaction and related reactions, i.e. rearrangement of carboxylate salt groups linked to six-membered aromatic rings, in the absence or in the presence of CO or CO2, (e.g. preparation of terepholates from benzoates); no additional classification for the subsequent hydrolysis of the salt groups has to be given
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyesters Or Polycarbonates (AREA)
- Artificial Filaments (AREA)
Abstract
Procedimiento para la preparación de ácido tereftálico mediante la reacción de tereftalato dipotásico con ácido benzoico, caracterizado porque en su realización se efectúan sucesivamente las siguientes operaciones: a) inicialmente se hace reaccionar poniendo en contacto ambos componente, tereftalato dipotásico con ácido benzoico en un medio acuoso que contiene benzoato potásico a una temperatura superior a 80ºC, encontrándose los diversos componentes introducidos de manera que se tenga, para cada kf de agua, 0,05 a 1,2 moles de benzoato potásico, menos de 0,4 moles de tereftalato dipotásico y la relación molar entre ácido benzoico y tereftalado dipotásico esté comprendida entre 4 y 12. b) Se separa el ácido tereftálico de sus aguas madres por cualquier medio conocido y a una temperatura superior a los 80ºC. c) Se somete el ácido tereftálico a un tratamiento de purificación.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7614867A FR2351081A1 (fr) | 1976-05-11 | 1976-05-11 | Procede de fabrication d'acide terephtalique a partir de terephtalate dipotassique, realisation en un etage |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES458631A1 true ES458631A1 (es) | 1978-02-16 |
Family
ID=9173243
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES458631A Expired ES458631A1 (es) | 1976-05-11 | 1977-05-10 | Procedimiento para la preparacion de acido tereftalico. |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US4212991A (es) |
| JP (1) | JPS537635A (es) |
| AR (1) | AR213522A1 (es) |
| AT (1) | AT350534B (es) |
| AU (1) | AU2501677A (es) |
| BE (1) | BE854469A (es) |
| BR (2) | BR7703021A (es) |
| CH (1) | CH599094A5 (es) |
| CS (1) | CS193574B2 (es) |
| DD (1) | DD129440A5 (es) |
| DE (1) | DE2721255A1 (es) |
| ES (1) | ES458631A1 (es) |
| FR (1) | FR2351081A1 (es) |
| GB (1) | GB1542182A (es) |
| IL (1) | IL52051A0 (es) |
| LU (1) | LU77293A1 (es) |
| NL (1) | NL7705158A (es) |
| PL (1) | PL102649B1 (es) |
| SE (1) | SE7705464L (es) |
| SU (1) | SU710514A3 (es) |
| ZA (1) | ZA772788B (es) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5965702U (ja) * | 1982-10-27 | 1984-05-02 | 住友ベークライト株式会社 | 水流冷却管 |
| US4540493A (en) * | 1983-11-30 | 1985-09-10 | Ecolochem, Inc. | Process for treating wash water from the manufacture of terephthalic acid |
| US4675108A (en) * | 1983-11-30 | 1987-06-23 | Ecolochem, Inc. | Apparatus for treating wash water from the manufacture of terephthalic acid |
| US5074756A (en) * | 1988-05-17 | 1991-12-24 | Patient Solutions, Inc. | Infusion device with disposable elements |
| US6426430B1 (en) * | 1999-08-30 | 2002-07-30 | Mossi & Ghisolfi Oversears, S.A. | Method for reduction of potassium in an integrated process for the production of 2,6—NDA |
| US6649263B2 (en) * | 2001-11-16 | 2003-11-18 | Honeywell International Inc. | Polyester resin and industrial yarn process |
| US7884231B2 (en) * | 2005-05-19 | 2011-02-08 | Eastman Chemical Company | Process to produce an enriched composition |
| US7304178B2 (en) * | 2005-05-19 | 2007-12-04 | Eastman Chemical Company | Enriched isophthalic acid composition |
| US7880031B2 (en) * | 2005-05-19 | 2011-02-01 | Eastman Chemical Company | Process to produce an enrichment feed |
| US20060264664A1 (en) * | 2005-05-19 | 2006-11-23 | Parker Kenny R | Esterification of an exchange solvent enriched composition |
| US7741516B2 (en) | 2005-05-19 | 2010-06-22 | Eastman Chemical Company | Process to enrich a carboxylic acid composition |
| US7557243B2 (en) * | 2005-05-19 | 2009-07-07 | Eastman Chemical Company | Enriched terephthalic acid composition |
| US20060264656A1 (en) * | 2005-05-19 | 2006-11-23 | Fujitsu Limited | Enrichment process using compounds useful in a polyester process |
| US7919652B2 (en) * | 2005-05-19 | 2011-04-05 | Eastman Chemical Company | Process to produce an enriched composition through the use of a catalyst removal zone and an enrichment zone |
| US7897809B2 (en) * | 2005-05-19 | 2011-03-01 | Eastman Chemical Company | Process to produce an enrichment feed |
| US7834208B2 (en) * | 2005-05-19 | 2010-11-16 | Eastman Chemical Company | Process to produce a post catalyst removal composition |
| US20060264662A1 (en) * | 2005-05-19 | 2006-11-23 | Gibson Philip E | Esterification of an enriched composition |
| US7432395B2 (en) * | 2005-05-19 | 2008-10-07 | Eastman Chemical Company | Enriched carboxylic acid composition |
| US7888529B2 (en) * | 2006-03-01 | 2011-02-15 | Eastman Chemical Company | Process to produce a post catalyst removal composition |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2846468A (en) * | 1957-03-08 | 1958-08-05 | Hercules Powder Co Ltd | Recovery of terephthalic acid |
| GB975113A (en) * | 1961-02-01 | 1964-11-11 | Teikoku Jinzo Kenshi Kk | Process for the preparation of terephthalic acid from dialkali metal terephthalates |
| BE788314A (fr) * | 1971-06-01 | 1973-03-01 | Phillips Petroleum Co | Procede de recuperation d'acide terephtalique et nouveau produit ainsi obtenu |
| JPS608623B2 (ja) * | 1975-10-28 | 1985-03-04 | 三菱電機株式会社 | 半導体素子の製造方法 |
-
1976
- 1976-05-11 FR FR7614867A patent/FR2351081A1/fr active Granted
-
1977
- 1977-05-05 US US05/794,134 patent/US4212991A/en not_active Expired - Lifetime
- 1977-05-06 AT AT324377A patent/AT350534B/de not_active IP Right Cessation
- 1977-05-09 LU LU77293A patent/LU77293A1/xx unknown
- 1977-05-09 AU AU25016/77A patent/AU2501677A/en not_active Expired
- 1977-05-10 JP JP5365877A patent/JPS537635A/ja active Granted
- 1977-05-10 DD DD7700198852A patent/DD129440A5/xx unknown
- 1977-05-10 GB GB7719652A patent/GB1542182A/en not_active Expired
- 1977-05-10 NL NL7705158A patent/NL7705158A/xx not_active Application Discontinuation
- 1977-05-10 BR BR7703021A patent/BR7703021A/pt unknown
- 1977-05-10 BR BR7703022A patent/BR7703022A/pt unknown
- 1977-05-10 ES ES458631A patent/ES458631A1/es not_active Expired
- 1977-05-10 PL PL1977198010A patent/PL102649B1/pl unknown
- 1977-05-10 BE BE177450A patent/BE854469A/xx unknown
- 1977-05-10 IL IL52051A patent/IL52051A0/xx unknown
- 1977-05-10 ZA ZA00772788A patent/ZA772788B/xx unknown
- 1977-05-10 CH CH583477A patent/CH599094A5/xx not_active IP Right Cessation
- 1977-05-10 AR AR267555A patent/AR213522A1/es active
- 1977-05-10 SE SE7705464A patent/SE7705464L/xx unknown
- 1977-05-11 CS CS773088A patent/CS193574B2/cs unknown
- 1977-05-11 DE DE19772721255 patent/DE2721255A1/de not_active Withdrawn
- 1977-05-11 SU SU772480075A patent/SU710514A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| CH599094A5 (es) | 1978-05-12 |
| AR213522A1 (es) | 1979-02-15 |
| AU2501677A (en) | 1978-11-16 |
| JPS537635A (en) | 1978-01-24 |
| SU710514A3 (ru) | 1980-01-15 |
| PL102649B1 (pl) | 1979-04-30 |
| BE854469A (fr) | 1977-11-10 |
| NL7705158A (nl) | 1977-11-15 |
| DD129440A5 (de) | 1978-01-18 |
| JPS5610901B2 (es) | 1981-03-11 |
| PL198010A1 (pl) | 1978-01-02 |
| CS193574B2 (en) | 1979-10-31 |
| AT350534B (de) | 1979-06-11 |
| LU77293A1 (es) | 1978-06-26 |
| GB1542182A (en) | 1979-03-14 |
| ZA772788B (en) | 1978-04-26 |
| BR7703021A (pt) | 1977-12-20 |
| BR7703022A (pt) | 1977-12-20 |
| IL52051A0 (en) | 1977-07-31 |
| FR2351081A1 (fr) | 1977-12-09 |
| ATA324377A (de) | 1978-11-15 |
| US4212991A (en) | 1980-07-15 |
| FR2351081B1 (es) | 1980-09-19 |
| SE7705464L (sv) | 1977-11-12 |
| DE2721255A1 (de) | 1977-11-17 |
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