ES471529A1 - Un procedimiento para la preparacion en continuo de cloro- bis-(alquilamino)-s-triacina - Google Patents
Un procedimiento para la preparacion en continuo de cloro- bis-(alquilamino)-s-triacinaInfo
- Publication number
- ES471529A1 ES471529A1 ES471529A ES471529A ES471529A1 ES 471529 A1 ES471529 A1 ES 471529A1 ES 471529 A ES471529 A ES 471529A ES 471529 A ES471529 A ES 471529A ES 471529 A1 ES471529 A1 ES 471529A1
- Authority
- ES
- Spain
- Prior art keywords
- alkylamino
- triazines
- chloro
- alkylamine
- exceeding
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 125000003282 alkyl amino group Chemical group 0.000 title abstract 3
- 150000003973 alkyl amines Chemical class 0.000 abstract 2
- MGNCLNQXLYJVJD-UHFFFAOYSA-N cyanuric chloride Chemical compound ClC1=NC(Cl)=NC(Cl)=N1 MGNCLNQXLYJVJD-UHFFFAOYSA-N 0.000 abstract 2
- 150000007529 inorganic bases Chemical class 0.000 abstract 2
- 230000035484 reaction time Effects 0.000 abstract 2
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/48—Two nitrogen atoms
- C07D251/50—Two nitrogen atoms with a halogen atom attached to the third ring carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
- C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
- C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
- C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
- C07D251/40—Nitrogen atoms
- C07D251/42—One nitrogen atom
- C07D251/44—One nitrogen atom with halogen atoms attached to the two other ring carbon atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Un procedimiento para la preparación en continuo de cloro-bis(alquilamino)-s-triacina, por medio de la sustitución por etapa de dos átomos de cloro de cloruro cianúrico con grupo alquilamínicos, caracterizado por alimentar de forma continua cloruro cianúrico en forma de una solución en un disolvente orgánico por el extremo de entrada de una primera zona de reacción tubular, alimentar de forma continua una base inorgánica, una primera alquilamina y agua a dicha primera zona de reacción tubular, alimentándose dicha base inorgánica y dicha primera alquilamina por lo menos en parte por el extremo de entrada de dicha primera zona de reacción, alimentándose dicho cloruro cianurico, base inorgánica y primera alquilamina en proporciones sustancialmente estequiométricas y relacionando en dicha primera zona de reacción bajo condiciones de turbulencia y a una temperatura no superior a 90ºC para convertir sustancialmente por completo dicho cloruro cianúrico en 2,4-di-cloro-6-alquilamino-6-triacina, y descargar el producto reaccional de (a) por el extremo de salida de dicha primera zona de reacción tubular.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IT25474/77A IT1081516B (it) | 1977-07-07 | 1977-07-07 | Procedimetno per la produzione di cloro-bis(alchilammine)-s-triazine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES471529A1 true ES471529A1 (es) | 1979-01-16 |
Family
ID=11216798
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES471529A Expired ES471529A1 (es) | 1977-07-07 | 1978-07-06 | Un procedimiento para la preparacion en continuo de cloro- bis-(alquilamino)-s-triacina |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4232153A (es) |
| JP (1) | JPS5919543B2 (es) |
| CH (1) | CH633004A5 (es) |
| ES (1) | ES471529A1 (es) |
| FR (1) | FR2396754A1 (es) |
| GB (1) | GB1586849A (es) |
| IL (1) | IL55021A (es) |
| IT (1) | IT1081516B (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS63186650U (es) * | 1987-05-22 | 1988-11-30 | ||
| EP0682019A1 (de) * | 1994-05-06 | 1995-11-15 | Hoechst Aktiengesellschaft | Verfahren zur kontinuierlichen Umsetzung von Cyanurfluorid mit Aminen |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH476746A (de) * | 1965-12-13 | 1969-08-15 | Agripat Sa | Verfahren zur Herstellung von Chlor-diamino-s-triazinen |
| US3436394A (en) * | 1967-03-20 | 1969-04-01 | Geigy Chem Corp | Process for the production of 2,4-alkylamino-6-chloro-s-triazines |
| US3639399A (en) * | 1969-07-10 | 1972-02-01 | Ciba Geigy Corp | Preparation of amino-s-triazines |
| US3883515A (en) * | 1969-12-29 | 1975-05-13 | Ciba Geigy Corp | Adiabatic process for the production of 2,4-dichloro-6-amino-S-triazines |
| IT1027241B (it) * | 1975-01-03 | 1978-11-20 | Rumianca Spa | Procedimento per la produzione di cloro amino s triazine |
| DE2505703C3 (de) * | 1975-02-12 | 1979-03-15 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zur Herstellung von gegebenenfalls substituierten 2-Alkylamino-4,6-dichlor-s-triazinen und 2,4-Bisalkylamino-6-chlor-s-triazinen |
| ES444742A1 (es) * | 1975-02-12 | 1977-08-16 | Degussa | Procedimiento para reemplazar uno o dos atomos de cloro del cloruro cianurico por una amina o por dos aminas iguales o diferentes. |
| ZA776989B (en) * | 1976-12-22 | 1978-09-27 | Ciba Geigy Ag | A caustic-free process for the production of monochloro-diamino-s-triazines |
-
1977
- 1977-07-07 IT IT25474/77A patent/IT1081516B/it active
-
1978
- 1978-05-31 GB GB24731/78A patent/GB1586849A/en not_active Expired
- 1978-06-27 IL IL55021A patent/IL55021A/xx unknown
- 1978-07-06 CH CH737078A patent/CH633004A5/it not_active IP Right Cessation
- 1978-07-06 ES ES471529A patent/ES471529A1/es not_active Expired
- 1978-07-06 FR FR7820169A patent/FR2396754A1/fr active Granted
- 1978-07-07 JP JP53082864A patent/JPS5919543B2/ja not_active Expired
- 1978-07-07 US US05/922,698 patent/US4232153A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5444687A (en) | 1979-04-09 |
| FR2396754B1 (es) | 1982-03-12 |
| CH633004A5 (it) | 1982-11-15 |
| US4232153A (en) | 1980-11-04 |
| GB1586849A (en) | 1981-03-25 |
| JPS5919543B2 (ja) | 1984-05-07 |
| FR2396754A1 (fr) | 1979-02-02 |
| IL55021A0 (en) | 1978-08-31 |
| IL55021A (en) | 1982-05-31 |
| IT1081516B (it) | 1985-05-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB1211497A (en) | Process for the production of cyanogen chloride and/or cyanuric chloride and tetrameric cyanogen chloride | |
| ES8405432A1 (es) | Procedimiento para la preparacion de polifosfato amonico activado | |
| EP0313254A3 (en) | Production of vinylidene fluoride | |
| ES8202530A1 (es) | Procedimiento para la preparacion selectiva de 2-cloro-1,1, 1,2,3,3,3-heptafluoropropano | |
| FR1503872A (fr) | Procédé de synthèse de composés chimiques, en particulier d'ammoniac, à partir de réactifs gazeux | |
| ES466363A1 (es) | Procedimiento para la obtencion de acido n-9,10-dihidro - lisergil-m-amino-benzoico | |
| PH16338A (en) | Process for the production of ures grains with improved properties | |
| ES475471A1 (es) | Procedimiento para la preparacion de 3-yodo- y 3-bromorrifa-micina s. | |
| GB1395861A (en) | Production of 2,6-dichloropyridine | |
| GB1323094A (en) | Production of triazine derivatives | |
| ES466103A1 (es) | Un procedimiento para preparar melamina. | |
| DE3063898D1 (en) | Process for the preparation of substituted anthraquinones | |
| GB1293304A (en) | Vinyl trichlorosilane | |
| DE3160460D1 (en) | Process for the preparation of 2-chloro-acetoacetic acid esters | |
| ES444742A1 (es) | Procedimiento para reemplazar uno o dos atomos de cloro del cloruro cianurico por una amina o por dos aminas iguales o diferentes. | |
| ES465914A1 (es) | Procedimiento para preparar tiazolina-2-tionas. | |
| EP0234503A3 (en) | Process for the preparation of 1,1,3-trichloroacetone | |
| GB1344636A (en) | Manufacture of halogenated pyridine derivatives | |
| FR2396754A1 (fr) | Procede de production en continu de chloro-bis (alkylamino)-s-triazines | |
| IL49014A (en) | Process for the substitution of the chlorine atoms of cyanuric chloride by amines | |
| SE7708204L (sv) | Sett att kontinuerligt framstella rent fosfin | |
| ES466197A1 (es) | Procedimiento para la obtencion de triazinas cloradas y fluoradas en forma mixta. | |
| GB1061555A (en) | Improvements in or relating to the production of potassium monopersulphate | |
| ES8201147A1 (es) | Procedimiento para la fabricacion de 5-amino-1,2,3-tiadiazo-les | |
| GB1209418A (en) | Process for preparing n-alkyl chlorides |