ES471832A1 - Instalacion para la preparacion continua de alcoholatos de metales alcalinos - Google Patents
Instalacion para la preparacion continua de alcoholatos de metales alcalinosInfo
- Publication number
- ES471832A1 ES471832A1 ES471832A ES471832A ES471832A1 ES 471832 A1 ES471832 A1 ES 471832A1 ES 471832 A ES471832 A ES 471832A ES 471832 A ES471832 A ES 471832A ES 471832 A1 ES471832 A1 ES 471832A1
- Authority
- ES
- Spain
- Prior art keywords
- alcoholates
- reaction vessel
- continuous preparation
- alkali metal
- metal alcoholate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 4
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 150000001340 alkali metals Chemical class 0.000 abstract 2
- 238000010924 continuous production Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/68—Preparation of metal alcoholates
- C07C29/70—Preparation of metal alcoholates by converting hydroxy groups to O-metal groups
- C07C29/705—Preparation of metal alcoholates by converting hydroxy groups to O-metal groups by transalcoholysis
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Instalación para la preparación continua de alcoholatos de metales alcalinos por transalcohilación de alcoholatos de metales alcalinos de alcoholes inferiores, especialmente de metanol o etanol, con alcoholes superiores introducidos en exceso, especialmente alcoholes monovalentes alifáticos o ciclo alifáticos, y separación del alcohol de más bajo punto de ebullición, caracterizada porque comprende una columna provista de platos, en donde están dispuestas una zona de reacción inferior para la fase líquida y una zona de concentración superior pudiendo ser calentada la zona de reacción inferior de la columna a fin de conseguir de este modo la relación de reflujo apropiada del alcohol inferior en la zona de concentración superior
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2726491A DE2726491C3 (de) | 1977-06-11 | 1977-06-11 | Verfahren zur kontinuierlichen Herstellung von Alkalialkoholaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES471832A1 true ES471832A1 (es) | 1979-11-16 |
Family
ID=6011363
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES470652A Expired ES470652A1 (es) | 1977-06-11 | 1978-06-09 | Procedimiento para la preparacion continua de alcoholatos de metales alcalinos |
| ES471832A Expired ES471832A1 (es) | 1977-06-11 | 1978-07-18 | Instalacion para la preparacion continua de alcoholatos de metales alcalinos |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES470652A Expired ES470652A1 (es) | 1977-06-11 | 1978-06-09 | Procedimiento para la preparacion continua de alcoholatos de metales alcalinos |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4327230A (es) |
| JP (1) | JPS545904A (es) |
| AT (1) | AT362767B (es) |
| BE (1) | BE867972A (es) |
| DE (1) | DE2726491C3 (es) |
| DK (1) | DK258178A (es) |
| ES (2) | ES470652A1 (es) |
| FR (1) | FR2393784A1 (es) |
| GB (1) | GB1600446A (es) |
| IT (1) | IT1156814B (es) |
| NL (1) | NL7806308A (es) |
| SE (1) | SE7805653L (es) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3413212C1 (de) * | 1984-04-07 | 1985-09-12 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von wasserfreiem Kalium-tert.-butoxid |
| US4536188A (en) * | 1984-07-31 | 1985-08-20 | Witt Clinton J De | Alcohol compositions having luminous flames |
| US4748283A (en) * | 1987-02-17 | 1988-05-31 | Lithium Corporation Of America | Hydrocarbon and chlorinated hydrocarbon-soluble magnesium dialkoxides |
| US4774363A (en) * | 1987-10-16 | 1988-09-27 | Gaf Corporation | Metal derivatives of butenediol |
| JP2556353B2 (ja) * | 1988-06-30 | 1996-11-20 | 昭栄化学工業株式会社 | 金属酸化物の製造方法 |
| DE10358412A1 (de) * | 2003-12-13 | 2005-07-07 | Degussa Ag | Verfahren zur Herstellung alkoxyreiner Erdalkalialkoxide |
| DE10358411A1 (de) * | 2003-12-13 | 2005-07-07 | Degussa Ag | Verfahren zur Herstellung alkoxyreiner Erdalkalialkoxide |
| US20090134369A1 (en) * | 2007-11-26 | 2009-05-28 | Applied Nanoworks, Inc. | Metal alkoxides, apparatus for manufacturing metal alkoxides, related methods and uses thereof |
| CN103204763A (zh) * | 2013-04-28 | 2013-07-17 | 江苏双乐化工颜料有限公司 | 一种有机醇钠的合成方法 |
| WO2021122702A1 (de) | 2019-12-18 | 2021-06-24 | Basf Se | Verfahren zur herstellung von metallalkoholaten |
| US20240002319A1 (en) | 2020-12-04 | 2024-01-04 | Basf Se | Process for preparing metal alkoxides by transalcoholisation |
| US20240018078A1 (en) | 2020-12-04 | 2024-01-18 | Basf Se | Method for controlling a reactive distillation column |
| US20240279145A1 (en) | 2021-06-16 | 2024-08-22 | Evonik Operations Gmbh | Process for workup of a methanol/water mixture in the production of alkali metal methoxides in a reaction column |
| JP2025511294A (ja) | 2022-04-04 | 2025-04-15 | エボニック オペレーションズ ゲーエムベーハー | ポリエチレンテレフタレートの改良された解重合法 |
| US20240052107A1 (en) | 2022-08-12 | 2024-02-15 | Evonik Operations Gmbh | Production of alkoxysiloxanes |
| CA3208899A1 (en) | 2022-08-12 | 2024-02-12 | Evonik Operations Gmbh | Production of alkoxysiloxanes |
| CA3208911A1 (en) | 2022-08-12 | 2024-02-12 | Evonik Operations Gmbh | Process for producing alkoxysiloxanes from waste silicone |
| KR20250092186A (ko) | 2022-10-19 | 2025-06-23 | 에보닉 오퍼레이션스 게엠베하 | 폴리에틸렌 테레프탈레이트의 개선된 탈중합 방법 |
| WO2024083336A1 (de) | 2022-10-20 | 2024-04-25 | Evonik Operations Gmbh | Verbessertes verfahren zur herstellung von alkalimetallmethanolaten |
| KR20250114030A (ko) | 2022-11-30 | 2025-07-28 | 에보닉 오퍼레이션스 게엠베하 | 알칼리 금속 메톡사이드를 제조하기 위한 개선된 프로세스 |
| WO2024120883A1 (en) | 2022-12-07 | 2024-06-13 | Evonik Operations Gmbh | Improved process for preparing metal alkoxide compounds |
| WO2024125775A1 (de) | 2022-12-14 | 2024-06-20 | Evonik Operations Gmbh | Verbessertes verfahren zur herstellung von metallalkoholatverbindungen |
| JP2026502013A (ja) | 2023-01-23 | 2026-01-20 | エボニック オペレーションズ ゲーエムベーハー | 押出機におけるポリアルキレンテレフタレートの解重合のためのプロセス |
| WO2024156567A1 (en) | 2023-01-23 | 2024-08-02 | Evonik Operations Gmbh | Process for depolymerization of polyalkylene terephthalates in an extruder |
| WO2024156563A1 (en) | 2023-01-23 | 2024-08-02 | Evonik Operations Gmbh | Process for depolymerizing polyalkylene terephthalates in mixtures with lower-melting polyolefins |
| EP4424760B1 (de) | 2023-03-02 | 2025-07-09 | Evonik Operations GmbH | Gewinnung von siloxanzyklen |
| CA3248863A1 (en) | 2023-07-27 | 2025-06-05 | Evonik Operations Gmbh | PHYSICAL REUSE OF SILICONED PAPER |
| CN119371285A (zh) * | 2024-10-18 | 2025-01-28 | 安徽金邦医药化工有限公司 | 一种高纯度颗粒状叔丁醇钠的制备方法 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL31269C (es) * | 1930-10-08 | |||
| GB490388A (en) * | 1936-08-26 | 1938-08-15 | Mathieson Alkali Works | Improvements in production of alcoholates of higher alcohols |
| US3028221A (en) * | 1958-12-15 | 1962-04-03 | Callery Chemical Co | Continuous process for the production of boranes |
| DE1254612C2 (de) | 1965-11-10 | 1973-05-17 | Dynamit Nobel Ag | Verfahren zur kontinuierlichen Herstellung von Alkalialkoholaten |
| GB1143897A (en) * | 1967-02-17 | 1969-02-26 | Metallgesellschaft Ag | A process for preparing alkali metal alcoholates and phenolates |
-
1977
- 1977-06-11 DE DE2726491A patent/DE2726491C3/de not_active Expired
-
1978
- 1978-05-17 SE SE7805653A patent/SE7805653L/xx unknown
- 1978-05-25 GB GB22851/78A patent/GB1600446A/en not_active Expired
- 1978-06-07 JP JP6874678A patent/JPS545904A/ja active Pending
- 1978-06-09 ES ES470652A patent/ES470652A1/es not_active Expired
- 1978-06-09 BE BE188447A patent/BE867972A/xx unknown
- 1978-06-09 FR FR787817335A patent/FR2393784A1/fr not_active Withdrawn
- 1978-06-09 AT AT0419878A patent/AT362767B/de not_active IP Right Cessation
- 1978-06-09 NL NL7806308A patent/NL7806308A/xx not_active Application Discontinuation
- 1978-06-09 DK DK258178A patent/DK258178A/da not_active Application Discontinuation
- 1978-06-09 IT IT49799/78A patent/IT1156814B/it active
- 1978-07-18 ES ES471832A patent/ES471832A1/es not_active Expired
-
1980
- 1980-03-10 US US06/128,421 patent/US4327230A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE2726491A1 (de) | 1978-12-14 |
| DK258178A (da) | 1978-12-12 |
| ES470652A1 (es) | 1979-02-01 |
| IT7849799A0 (it) | 1978-06-09 |
| AT362767B (de) | 1981-06-10 |
| DE2726491C3 (de) | 1981-02-12 |
| IT1156814B (it) | 1987-02-04 |
| BE867972A (fr) | 1978-10-02 |
| SE7805653L (sv) | 1978-12-12 |
| GB1600446A (en) | 1981-10-14 |
| NL7806308A (nl) | 1978-12-13 |
| DE2726491B2 (de) | 1980-05-29 |
| US4327230A (en) | 1982-04-27 |
| FR2393784A1 (fr) | 1979-01-05 |
| JPS545904A (en) | 1979-01-17 |
| ATA419878A (de) | 1980-11-15 |
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