FR2393784A1 - Procede pour l'obtention en continu d'alcoolates alcalins - Google Patents
Procede pour l'obtention en continu d'alcoolates alcalinsInfo
- Publication number
- FR2393784A1 FR2393784A1 FR787817335A FR7817335A FR2393784A1 FR 2393784 A1 FR2393784 A1 FR 2393784A1 FR 787817335 A FR787817335 A FR 787817335A FR 7817335 A FR7817335 A FR 7817335A FR 2393784 A1 FR2393784 A1 FR 2393784A1
- Authority
- FR
- France
- Prior art keywords
- alcoholates
- alkaline alcoholates
- alcoholysis
- alkaline
- continuous obtaining
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 title abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 abstract 3
- 150000001298 alcohols Chemical class 0.000 abstract 2
- 238000006136 alcoholysis reaction Methods 0.000 abstract 2
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
- 238000004821 distillation Methods 0.000 abstract 1
- 230000008030 elimination Effects 0.000 abstract 1
- 238000003379 elimination reaction Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/68—Preparation of metal alcoholates
- C07C29/70—Preparation of metal alcoholates by converting hydroxy groups to O-metal groups
- C07C29/705—Preparation of metal alcoholates by converting hydroxy groups to O-metal groups by transalcoholysis
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procédé pour l'obtention en continu d'alcoolates alcalin par alcoolyse d'alcoolates alcalins d'alcools inférieurs, en particulier de méthanol ou d'éthanol, avec des alcools supérieurs introduits en excès, notamment des monoalcools aliphatiques ou cycloaliphatiques,et élimination de l'alcool à bas point d'ébullition. L'alcoolyse et la purification par distillation de l'alcool inférieur sont réalisées simultanément dans un dispositif comportant une section réactionnelle et une section de rectification directement couplée à celle-ci. Fabrication industrielle d'alcoolates alcalins.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2726491A DE2726491C3 (de) | 1977-06-11 | 1977-06-11 | Verfahren zur kontinuierlichen Herstellung von Alkalialkoholaten |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| FR2393784A1 true FR2393784A1 (fr) | 1979-01-05 |
Family
ID=6011363
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR787817335A Withdrawn FR2393784A1 (fr) | 1977-06-11 | 1978-06-09 | Procede pour l'obtention en continu d'alcoolates alcalins |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US4327230A (fr) |
| JP (1) | JPS545904A (fr) |
| AT (1) | AT362767B (fr) |
| BE (1) | BE867972A (fr) |
| DE (1) | DE2726491C3 (fr) |
| DK (1) | DK258178A (fr) |
| ES (2) | ES470652A1 (fr) |
| FR (1) | FR2393784A1 (fr) |
| GB (1) | GB1600446A (fr) |
| IT (1) | IT1156814B (fr) |
| NL (1) | NL7806308A (fr) |
| SE (1) | SE7805653L (fr) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3413212C1 (de) * | 1984-04-07 | 1985-09-12 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von wasserfreiem Kalium-tert.-butoxid |
| US4536188A (en) * | 1984-07-31 | 1985-08-20 | Witt Clinton J De | Alcohol compositions having luminous flames |
| US4748283A (en) * | 1987-02-17 | 1988-05-31 | Lithium Corporation Of America | Hydrocarbon and chlorinated hydrocarbon-soluble magnesium dialkoxides |
| US4774363A (en) * | 1987-10-16 | 1988-09-27 | Gaf Corporation | Metal derivatives of butenediol |
| JP2556353B2 (ja) * | 1988-06-30 | 1996-11-20 | 昭栄化学工業株式会社 | 金属酸化物の製造方法 |
| DE10358412A1 (de) * | 2003-12-13 | 2005-07-07 | Degussa Ag | Verfahren zur Herstellung alkoxyreiner Erdalkalialkoxide |
| DE10358411A1 (de) * | 2003-12-13 | 2005-07-07 | Degussa Ag | Verfahren zur Herstellung alkoxyreiner Erdalkalialkoxide |
| US20090134369A1 (en) * | 2007-11-26 | 2009-05-28 | Applied Nanoworks, Inc. | Metal alkoxides, apparatus for manufacturing metal alkoxides, related methods and uses thereof |
| CN103204763A (zh) * | 2013-04-28 | 2013-07-17 | 江苏双乐化工颜料有限公司 | 一种有机醇钠的合成方法 |
| WO2021122702A1 (fr) | 2019-12-18 | 2021-06-24 | Basf Se | Procédé de production d'alcoolates métalliques |
| US20240002319A1 (en) | 2020-12-04 | 2024-01-04 | Basf Se | Process for preparing metal alkoxides by transalcoholisation |
| US20240018078A1 (en) | 2020-12-04 | 2024-01-18 | Basf Se | Method for controlling a reactive distillation column |
| US20240279145A1 (en) | 2021-06-16 | 2024-08-22 | Evonik Operations Gmbh | Process for workup of a methanol/water mixture in the production of alkali metal methoxides in a reaction column |
| JP2025511294A (ja) | 2022-04-04 | 2025-04-15 | エボニック オペレーションズ ゲーエムベーハー | ポリエチレンテレフタレートの改良された解重合法 |
| US20240052107A1 (en) | 2022-08-12 | 2024-02-15 | Evonik Operations Gmbh | Production of alkoxysiloxanes |
| CA3208899A1 (fr) | 2022-08-12 | 2024-02-12 | Evonik Operations Gmbh | Production d~alkoxysiloxanes |
| CA3208911A1 (fr) | 2022-08-12 | 2024-02-12 | Evonik Operations Gmbh | Procede de production d~alkoxysiloxanes a partir de silicone recycle |
| KR20250092186A (ko) | 2022-10-19 | 2025-06-23 | 에보닉 오퍼레이션스 게엠베하 | 폴리에틸렌 테레프탈레이트의 개선된 탈중합 방법 |
| WO2024083336A1 (fr) | 2022-10-20 | 2024-04-25 | Evonik Operations Gmbh | Procédé amélioré pour produire des méthoxydes de métaux alcalins |
| KR20250114030A (ko) | 2022-11-30 | 2025-07-28 | 에보닉 오퍼레이션스 게엠베하 | 알칼리 금속 메톡사이드를 제조하기 위한 개선된 프로세스 |
| WO2024120883A1 (fr) | 2022-12-07 | 2024-06-13 | Evonik Operations Gmbh | Procédé amélioré pour préparer des composés d'alcoxyde métallique |
| WO2024125775A1 (fr) | 2022-12-14 | 2024-06-20 | Evonik Operations Gmbh | Procédé amélioré pour préparer des composés d'alcoolates métalliques |
| JP2026502013A (ja) | 2023-01-23 | 2026-01-20 | エボニック オペレーションズ ゲーエムベーハー | 押出機におけるポリアルキレンテレフタレートの解重合のためのプロセス |
| WO2024156567A1 (fr) | 2023-01-23 | 2024-08-02 | Evonik Operations Gmbh | Processus de dépolymérisation de téréphtalates de polyalkylène dans une extrudeuse |
| WO2024156563A1 (fr) | 2023-01-23 | 2024-08-02 | Evonik Operations Gmbh | Processus de dépolymérisation de téréphtalates de polyalkylène dans des mélanges avec des polyoléfines à point de fusion inférieur |
| EP4424760B1 (fr) | 2023-03-02 | 2025-07-09 | Evonik Operations GmbH | Récupération de cycles siloxane |
| CA3248863A1 (fr) | 2023-07-27 | 2025-06-05 | Evonik Operations Gmbh | Réutilisation physique de papiers siliconés |
| CN119371285A (zh) * | 2024-10-18 | 2025-01-28 | 安徽金邦医药化工有限公司 | 一种高纯度颗粒状叔丁醇钠的制备方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1555094A (fr) * | 1967-02-17 | 1969-01-24 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL31269C (fr) * | 1930-10-08 | |||
| GB490388A (en) * | 1936-08-26 | 1938-08-15 | Mathieson Alkali Works | Improvements in production of alcoholates of higher alcohols |
| US3028221A (en) * | 1958-12-15 | 1962-04-03 | Callery Chemical Co | Continuous process for the production of boranes |
| DE1254612C2 (de) | 1965-11-10 | 1973-05-17 | Dynamit Nobel Ag | Verfahren zur kontinuierlichen Herstellung von Alkalialkoholaten |
-
1977
- 1977-06-11 DE DE2726491A patent/DE2726491C3/de not_active Expired
-
1978
- 1978-05-17 SE SE7805653A patent/SE7805653L/xx unknown
- 1978-05-25 GB GB22851/78A patent/GB1600446A/en not_active Expired
- 1978-06-07 JP JP6874678A patent/JPS545904A/ja active Pending
- 1978-06-09 ES ES470652A patent/ES470652A1/es not_active Expired
- 1978-06-09 BE BE188447A patent/BE867972A/fr unknown
- 1978-06-09 FR FR787817335A patent/FR2393784A1/fr not_active Withdrawn
- 1978-06-09 AT AT0419878A patent/AT362767B/de not_active IP Right Cessation
- 1978-06-09 NL NL7806308A patent/NL7806308A/xx not_active Application Discontinuation
- 1978-06-09 DK DK258178A patent/DK258178A/da not_active Application Discontinuation
- 1978-06-09 IT IT49799/78A patent/IT1156814B/it active
- 1978-07-18 ES ES471832A patent/ES471832A1/es not_active Expired
-
1980
- 1980-03-10 US US06/128,421 patent/US4327230A/en not_active Expired - Lifetime
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1555094A (fr) * | 1967-02-17 | 1969-01-24 |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2726491A1 (de) | 1978-12-14 |
| DK258178A (da) | 1978-12-12 |
| ES470652A1 (es) | 1979-02-01 |
| IT7849799A0 (it) | 1978-06-09 |
| AT362767B (de) | 1981-06-10 |
| DE2726491C3 (de) | 1981-02-12 |
| IT1156814B (it) | 1987-02-04 |
| BE867972A (fr) | 1978-10-02 |
| SE7805653L (sv) | 1978-12-12 |
| GB1600446A (en) | 1981-10-14 |
| ES471832A1 (es) | 1979-11-16 |
| NL7806308A (nl) | 1978-12-13 |
| DE2726491B2 (de) | 1980-05-29 |
| US4327230A (en) | 1982-04-27 |
| JPS545904A (en) | 1979-01-17 |
| ATA419878A (de) | 1980-11-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RE | Withdrawal of published application |