ES540079A0 - Procedimiento para preparar 1,4-bis-3-(3,4,5-trimetoxi-ben- zoiloxi)-propil-diazepan - Google Patents

Procedimiento para preparar 1,4-bis-3-(3,4,5-trimetoxi-ben- zoiloxi)-propil-diazepan

Info

Publication number: ES540079A0
Authority: ES; Spain
Prior art keywords: bis; propyl; reacting; zoiloxi; trimetoxi
Prior art date: 1984-02-03
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

ES540079A

Other languages

English (en)

Other versions

ES8607257A1 (es

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Evonik Operations GmbH

Original Assignee

Degussa GmbH

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-02-03

Filing date

1985-02-01

Publication date

1986-05-16

1985-02-01 Application filed by Degussa GmbH filed Critical Degussa GmbH

1986-05-16 Publication of ES8607257A1 publication Critical patent/ES8607257A1/es

1986-05-16 Publication of ES540079A0 publication Critical patent/ES540079A0/es

Status Expired legal-status Critical Current

Links

238000000034 method Methods 0.000 title abstract 2
WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 6
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
239000003513 alkali Substances 0.000 abstract 2
XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 abstract 2
239000007795 chemical reaction product Substances 0.000 abstract 2
LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 abstract 2
SIFCVCJPFLTXKI-UHFFFAOYSA-N 1,4-bis[3-[(3,4,5-trimethoxyphenyl)methoxy]propyl]diazepane Chemical compound COC1=C(OC)C(OC)=CC(COCCCC2CNN(CCCOCC=3C=C(OC)C(OC)=C(OC)C=3)CCC2)=C1 SIFCVCJPFLTXKI-UHFFFAOYSA-N 0.000 abstract 1
-1 3,4,5-trimethoxy-benzoyl groups Chemical group 0.000 abstract 1
NCCYQWDCLLSCCT-UHFFFAOYSA-N 3-(1,4-diazepan-1-yl)propan-1-ol Chemical compound OCCCN1CCCNCC1 NCCYQWDCLLSCCT-UHFFFAOYSA-N 0.000 abstract 1
LYXDZJFQOXMLGP-UHFFFAOYSA-N 3-[cyanomethyl(3-hydroxypropyl)amino]propanenitrile Chemical compound OCCCN(CC#N)CCC#N LYXDZJFQOXMLGP-UHFFFAOYSA-N 0.000 abstract 1
NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 abstract 1
LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 abstract 1
XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 1
WUGQZFFCHPXWKQ-UHFFFAOYSA-N Propanolamine Chemical compound NCCCO WUGQZFFCHPXWKQ-UHFFFAOYSA-N 0.000 abstract 1
229910021529 ammonia Inorganic materials 0.000 abstract 1
239000007864 aqueous solution Substances 0.000 abstract 1
239000003054 catalyst Substances 0.000 abstract 1
150000001875 compounds Chemical class 0.000 abstract 1
230000032050 esterification Effects 0.000 abstract 1
238000005886 esterification reaction Methods 0.000 abstract 1
229910052736 halogen Inorganic materials 0.000 abstract 1
229940079826 hydrogen sulfite Drugs 0.000 abstract 1
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 abstract 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D243/00—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
- C07D243/06—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D243/00—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
- C07D243/06—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4
- C07D243/08—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4 not condensed with other rings

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Plural Heterocyclic Compounds (AREA)
Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

ES540079A 1984-02-03 1985-02-01 Procedimiento para preparar 1,4-bis-3-(3,4,5-trimetoxi-ben- zoiloxi)-propil-diazepan Expired ES8607257A1 (es)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE19843403778 DE3403778A1 (de)	1984-02-03	1984-02-03	Cyanomethyl-(2-cyano-ethyl)-(3-hydroxy-propyl)-amin seine verwendung zur herstellung von 1-(3-hydroxy-propyl)-1,4-diazepan und 1,4-bis(3-(3,4,5-trimethoxybenzoyloxy)-propyl)-diazepan

Publications (2)

Publication Number	Publication Date
ES8607257A1 ES8607257A1 (es)	1986-05-16
ES540079A0 true ES540079A0 (es)	1986-05-16

Family

ID=6226691

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
ES540079A Expired ES8607257A1 (es)	1984-02-03	1985-02-01	Procedimiento para preparar 1,4-bis-3-(3,4,5-trimetoxi-ben- zoiloxi)-propil-diazepan

Country Status (7)

Country	Link
US (1)	US4751298A (es)
EP (1)	EP0152598B1 (es)
JP (1)	JPS60181058A (es)
KR (1)	KR850005832A (es)
AT (1)	ATE33645T1 (es)
DE (2)	DE3403778A1 (es)
ES (1)	ES8607257A1 (es)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE3403778A1 (de) *	1984-02-03	1985-08-08	Degussa Ag, 6000 Frankfurt	Cyanomethyl-(2-cyano-ethyl)-(3-hydroxy-propyl)-amin seine verwendung zur herstellung von 1-(3-hydroxy-propyl)-1,4-diazepan und 1,4-bis(3-(3,4,5-trimethoxybenzoyloxy)-propyl)-diazepan
JP2722250B2 (ja) *	1989-05-30	1998-03-04	興和株式会社	新規なジアミン化合物及びこれを含有する脳機能障害改善剤
US5190946A (en) *	1990-02-23	1993-03-02	Hoffmann-La Roche Inc.	Methods and compounds
AU2056397A (en) *	1997-02-21	1998-09-09	Scripps Research Institute, The	Hydroxyazepanes as inhibitors of glycosidase and hiv protease
US6600075B1 (en) *	2001-11-13	2003-07-29	E. I. Du Pont De Nemours And Company	Process for the preparation of tertiaŕy amines from primary amines and nitriles

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US3040029A (en) *		1962-06-19		Preparation of homopiperazine and al-
US1972465A (en) *	1931-02-16	1934-09-04	Ig Farbenindustrie Ag	Production of nitriles
DE1545575C2 (de) *	1965-12-16	1970-09-10	Asta-Werke Ag, Chemische Fabrik, 4812 Brackwede	N, N'-Bis- eckige Klammer auf 3"(3', 4', 5'-trimethoxybenzoyloxy)-propyl eckige Klammer zu -homopiperazin
JPS5210877B2 (es) *	1972-11-08	1977-03-26
US3980643A (en) *	1974-01-04	1976-09-14	Hokuriku Pharmaceutical Co., Ltd.	Novel piperazine- and homopiperazine-monoalkanol esters and a process of production thereof
JPS53144591A (en) *	1977-05-20	1978-12-15	Asutaabueruke Ag Chem Fuaburii	Process for preparing homopirerazine
JPS56113771A (en) *	1980-02-14	1981-09-07	Hokuriku Seiyaku Co Ltd	N,n'-disubstituted diazacycloalkane derivative
JPS56161377A (en) *	1980-05-16	1981-12-11	Grelan Pharmaceut Co Ltd	Preparation of 1,4-bis 3-hydroxypropyl hexahydro-1h-1,4- diazepine
JPS5731671A (en) *	1980-07-30	1982-02-20	Iwaki Seiyaku Kk	Preparation of homopiperazine derivative
JPS57106668A (en) *	1980-12-23	1982-07-02	Toho Iyaku Kenkyusho:Kk	Preparation of n,n'-bis-(3-(3',4',5'-trimethoxybenzoyloxy)- propyl)homopiperazine
JPS57110668A (en) *	1980-12-29	1982-07-09	Pilot Pen Co Ltd:The	Method for etching and patterning of extruded profile of aluminum or its alloy
DE3403778A1 (de) *	1984-02-03	1985-08-08	Degussa Ag, 6000 Frankfurt	Cyanomethyl-(2-cyano-ethyl)-(3-hydroxy-propyl)-amin seine verwendung zur herstellung von 1-(3-hydroxy-propyl)-1,4-diazepan und 1,4-bis(3-(3,4,5-trimethoxybenzoyloxy)-propyl)-diazepan

1984
- 1984-02-03 DE DE19843403778 patent/DE3403778A1/de not_active Withdrawn
- 1984-12-14 EP EP84115471A patent/EP0152598B1/de not_active Expired
- 1984-12-14 DE DE8484115471T patent/DE3470539D1/de not_active Expired
- 1984-12-14 AT AT84115471T patent/ATE33645T1/de not_active IP Right Cessation
1985
- 1985-01-22 US US06/693,344 patent/US4751298A/en not_active Expired - Fee Related
- 1985-01-31 KR KR1019850000606A patent/KR850005832A/ko not_active Withdrawn
- 1985-02-01 ES ES540079A patent/ES8607257A1/es not_active Expired
- 1985-02-01 JP JP60016727A patent/JPS60181058A/ja active Pending

Also Published As

Publication number	Publication date
ES8607257A1 (es)	1986-05-16
US4751298A (en)	1988-06-14
DE3470539D1 (en)	1988-05-26
ATE33645T1 (de)	1988-05-15
DE3403778A1 (de)	1985-08-08
EP0152598A1 (de)	1985-08-28
JPS60181058A (ja)	1985-09-14
KR850005832A (ko)	1985-09-26
EP0152598B1 (de)	1988-04-20

Legal Events

Date	Code	Title	Description
2001-01-01	FD1A	Patent lapsed	Effective date: 20001102

Publication	Publication Date	Title
ES540079A0 (es)	1986-05-16	Procedimiento para preparar 1,4-bis-3-(3,4,5-trimetoxi-ben- zoiloxi)-propil-diazepan
ATE1526T1 (de)	1982-09-15	Verfahren zur kontinuierlichen herstellung von trioxan.
KR870008835A (ko)	1987-10-21	이미노디아세토니트릴의 제조방법
JPS5799596A (en)	1982-06-21	Phosphonohydroxy acetonitrile and manufacture
DE2961018D1 (en)	1981-12-24	Method for the simultaneous production of trioxane and cyclic formals
EP0248586A3 (en)	1989-07-26	Process for producing amidine sulfonic acid intermediates for guanidines
ATE2895T1 (de)	1983-04-15	Verfahren zur herstellung von 4-hydroxy-carbazol.
MX166488B (es)	1993-01-12	Metodo para la produccion de hidantoinas metiloladas
DE3586232D1 (de)	1992-07-23	Verfahren zur herstellung von n,n',n"-tris(2-hydroxypropyl)melamin.
ATE40343T1 (de)	1989-02-15	Verfahren zur herstellung von cyanamid.
KR840004408A (ko)	1984-10-15	스피로-(모노 및 디)-플루오로플루오렌 화합물을 제조하는 방법
ES468377A1 (es)	1978-12-16	Un procedimiento para la preparacion de nuevas iminas.
GB1121038A (en)	1968-07-24	Process for the manufacture of aminonitriles
KR890006659A (ko)	1989-06-15	디메틸아미노메틸 구리 프탈로시아닌의 제조방법
KR900016084A (ko)	1990-11-12	광학활성 3,4-디히드록시 부티르산 유도체의 제조방법
MX161725A (es)	1990-12-20	Proceso para la preparacion de n-metilantranilato de metilo
JPS54109943A (en)	1979-08-29	Preparation of phenylglycine derivative
ES8104196A1 (es)	1981-04-01	Un procedimiento para preparar b-cloroalanina
DE3768350D1 (de)	1991-04-11	Verfahren zur herstellung von anthracyclin-derivat r2ox2.
EP0310527A3 (en)	1989-10-04	Process for manufacturing amines from olefines
ES543529A0 (es)	1986-06-01	Mejoras en los procedimientos para la produccion de aldehi- dos
SU1128549A1 (ru)	2000-02-20	Способ получения моноэфиров диолов
KR910001160A (ko)	1991-01-30	마류(麻類)를 원료로한 의혁지의 제조
HUT57195A (en)	1991-11-28	New process for producing an isoxazole derivative
SU1596699A1 (ru)	1996-03-10	Способ получения n,n-диметил-(3,5-ди-трет-бутил-4-оксибензил)амина