ES8200338A1 - Un procedimiento para la separacion por via de destilacion dehidroperoxidos de ter-alquilo - Google Patents
Un procedimiento para la separacion por via de destilacion dehidroperoxidos de ter-alquiloInfo
- Publication number
- ES8200338A1 ES8200338A1 ES490787A ES490787A ES8200338A1 ES 8200338 A1 ES8200338 A1 ES 8200338A1 ES 490787 A ES490787 A ES 490787A ES 490787 A ES490787 A ES 490787A ES 8200338 A1 ES8200338 A1 ES 8200338A1
- Authority
- ES
- Spain
- Prior art keywords
- tertiary alkyl
- distillative separation
- hydroperoxides
- ditertiary
- peroxides
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- -1 alkyl hydroperoxides Chemical group 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 3
- 238000007700 distillative separation Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 abstract 2
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 238000005292 vacuum distillation Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
- C07C407/003—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PROCEDIMIENTO DE SEPARACION POR DESTILACION DE HIDROPEROXIDOS DE TER-ALQUILO. CONSISTE EN NEUTRALIZAR LA MEZCLA DE REACCION QUE SE PRODUCE EN LA OBTENCION DEL HIDROPEROXIDO DE TER-ALQUILO; A CONTINUACION SE DESTILA EN PRESENCIA DE AGUA A UNA TEMPERATURA INFERIOR A 45. EN LA MEZCLA DE REACCION SE MANTIENE LA CONCENTRACION DEL PEROXIDO DEL CALDERION DE DESTILACION POR DEBAJO DE, APROXIMADAMENTE, 70 POR 100 EN PESO, POR MEDIO DE ADICION DE AGUA. LA PRESION DEL CALDERIN ES, APROXIMADAMENTE, DE 22 A 55 MILIBARES. LA DESTILACION SE PRACTICA DE MANERA CONTINUA, PARA LO QUE SE ALIMENTA EL PRODUCTO BRUTO DE MANERA CONTINUA Y EL DESTILADO SE RETIRA ASIMISMO DE MANERA CONTIN
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19792916572 DE2916572A1 (de) | 1979-04-24 | 1979-04-24 | Verfahren zur destillativen trennung von tert.-alkylhydroperoxiden und di- tert.-alkylperoxiden |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES8200338A1 true ES8200338A1 (es) | 1981-11-01 |
| ES490787A0 ES490787A0 (es) | 1981-11-01 |
Family
ID=6069138
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES490787A Granted ES490787A0 (es) | 1979-04-24 | 1980-04-22 | Un procedimiento para la separacion por via de destilacion dehidroperoxidos de ter-alquilo |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US4381222A (es) |
| JP (1) | JPS55143964A (es) |
| AU (1) | AU538760B2 (es) |
| BE (1) | BE882820A (es) |
| BR (1) | BR8002470A (es) |
| CA (1) | CA1158195A (es) |
| DE (1) | DE2916572A1 (es) |
| ES (1) | ES490787A0 (es) |
| FR (1) | FR2455036A1 (es) |
| GB (1) | GB2048865B (es) |
| IT (1) | IT1129079B (es) |
| NL (1) | NL8002104A (es) |
| RO (1) | RO79823A (es) |
| SE (1) | SE434834B (es) |
| ZA (1) | ZA802466B (es) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4584413A (en) * | 1983-09-14 | 1986-04-22 | Atlantic Richfield Company | Purification of tertiary butyl hydroperoxide containing primary and secondary alkyl hydroperoxide contaminants |
| US4900850A (en) * | 1986-12-23 | 1990-02-13 | Texaco Inc. | Recovery of purified ditertiary butyl peroxide |
| US4891101A (en) * | 1988-11-23 | 1990-01-02 | Arco Chemical Technology, Inc. | Purification of tertiary hydroperoxides containing primary and secondary hydroperoxide contaminants |
| US4935101A (en) * | 1989-10-13 | 1990-06-19 | Arco Chemical Technology, Inc. | Process for the recovery of a water-insoluble epoxy alcohol |
| US5104493B1 (en) * | 1991-01-24 | 1995-08-15 | Arco Chem Tech | Tertiary butyl hydroperoxide concentration |
| US5453548A (en) * | 1994-10-25 | 1995-09-26 | Arco Chemical Technology, L.P. | Purification of ditertiary butyl peroxide |
| JP2001106680A (ja) * | 1999-10-04 | 2001-04-17 | Nof Corp | グリシドールの製造方法 |
| JP6695005B2 (ja) * | 2016-10-12 | 2020-05-20 | ライオンデル ケミカル テクノロジー、エル.ピー. | Tert−ブチルヒドロペルオキシド溶液の製造及びそれから生成物を形成するための方法 |
| FR3091280B1 (fr) | 2018-12-26 | 2021-06-25 | Arkema France | Purification d’hydroperoxyde d’alkyle par distillation extractive |
| FR3091281B1 (fr) | 2018-12-26 | 2021-06-18 | Arkema France | Procédé de purification de l’hydroperoxyde d’alkyle par extraction à l’eau et séparation de la phase aqueuse |
| FR3091283B1 (fr) | 2018-12-26 | 2021-06-25 | Arkema France | Purification d’hydroperoxyde d’alkyle par distillation en presence de methanol et d’eau |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2383919A (en) * | 1944-05-23 | 1945-08-28 | Shell Dev | Recovery of organic peroxides |
| GB1137717A (en) * | 1965-05-20 | 1968-12-27 | Laporte Chemical | Process for the purification of tertiary butyl hydroperoxide |
| US3449217A (en) * | 1968-01-05 | 1969-06-10 | Halcon International Inc | Process of buffering a neutralized t-butyl hydroperoxide during distillation |
| GB1243313A (en) * | 1970-02-20 | 1971-08-18 | Pennwalt Corp | Organic peroxides |
| GB1334459A (en) * | 1970-09-02 | 1973-10-17 | Atlantic Richfield Co | Process for recovering hydroperoxides |
| DE2159764B2 (de) * | 1971-12-02 | 1976-11-18 | Akzo Gmbh, 5600 Wuppertal | Verfahren zur kontinuierlichen herstellung und anreicherung von kohlenwasserstoffhydroperoxiden |
| JPS5653546B2 (es) * | 1973-05-02 | 1981-12-19 |
-
1979
- 1979-04-24 DE DE19792916572 patent/DE2916572A1/de active Granted
-
1980
- 1980-03-27 CA CA000348801A patent/CA1158195A/en not_active Expired
- 1980-04-10 NL NL8002104A patent/NL8002104A/nl not_active Application Discontinuation
- 1980-04-17 BE BE1/9790A patent/BE882820A/fr not_active IP Right Cessation
- 1980-04-17 SE SE8002891A patent/SE434834B/sv unknown
- 1980-04-17 GB GB8012650A patent/GB2048865B/en not_active Expired
- 1980-04-18 FR FR8008848A patent/FR2455036A1/fr active Granted
- 1980-04-21 AU AU57635/80A patent/AU538760B2/en not_active Ceased
- 1980-04-22 JP JP5242780A patent/JPS55143964A/ja active Granted
- 1980-04-22 ES ES490787A patent/ES490787A0/es active Granted
- 1980-04-23 IT IT67647/80A patent/IT1129079B/it active
- 1980-04-23 BR BR8002470A patent/BR8002470A/pt unknown
- 1980-04-24 RO RO80100939A patent/RO79823A/ro unknown
- 1980-04-24 ZA ZA00802466A patent/ZA802466B/xx unknown
-
1981
- 1981-10-27 US US06/315,389 patent/US4381222A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| NL8002104A (nl) | 1980-10-28 |
| AU5763580A (en) | 1980-10-30 |
| FR2455036B1 (es) | 1982-12-03 |
| JPS55143964A (en) | 1980-11-10 |
| DE2916572A1 (de) | 1980-11-13 |
| SE434834B (sv) | 1984-08-20 |
| JPS6212790B2 (es) | 1987-03-20 |
| ZA802466B (en) | 1981-05-27 |
| RO79823A (ro) | 1982-10-26 |
| IT8067647A0 (it) | 1980-04-23 |
| FR2455036A1 (fr) | 1980-11-21 |
| CA1158195A (en) | 1983-12-06 |
| ES490787A0 (es) | 1981-11-01 |
| GB2048865A (en) | 1980-12-17 |
| AU538760B2 (en) | 1984-08-23 |
| DE2916572C2 (es) | 1989-01-12 |
| US4381222A (en) | 1983-04-26 |
| SE8002891L (sv) | 1980-10-25 |
| IT1129079B (it) | 1986-06-04 |
| BR8002470A (pt) | 1980-12-09 |
| GB2048865B (en) | 1983-04-27 |
| BE882820A (fr) | 1980-10-17 |
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