FI56490C - Foerfarande foer avlaegsnande av gasformiga foeroreningar ur svavelsyrakontaktanordningars avgaser - Google Patents

Foerfarande foer avlaegsnande av gasformiga foeroreningar ur svavelsyrakontaktanordningars avgaser Download PDF

Info

Publication number: FI56490C
Authority: FI; Finland
Prior art keywords: acid; sulfuric acid; venturin; sump; tower
Prior art date: 1973-05-08

Application number

FI1370/74A

Other languages

English (en)

Finnish (fi)

Swedish (sv)

Other versions

FI56490B (fi

Inventor

Karl-Heinz Doerr

Hugo Grimm

Ulrich Sander

Robert Peichl

Michael Tacke

Original Assignee

Metallgesellschaft Ag

Sued Chemie Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1973-05-08

Filing date

1974-05-06

Publication date

1980-02-11

1974-05-06 Application filed by Metallgesellschaft Ag, Sued Chemie Ag filed Critical Metallgesellschaft Ag

1979-10-31 Application granted granted Critical

1979-10-31 Publication of FI56490B publication Critical patent/FI56490B/fi

1980-02-11 Publication of FI56490C publication Critical patent/FI56490C/fi

Links

QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 115
239000002253 acid Substances 0.000 claims description 87
239000007789 gas Substances 0.000 claims description 46
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 33
239000001301 oxygen Substances 0.000 claims description 32
229910052760 oxygen Inorganic materials 0.000 claims description 32
238000005406 washing Methods 0.000 claims description 32
230000003647 oxidation Effects 0.000 claims description 27
238000007254 oxidation reaction Methods 0.000 claims description 27
238000000034 method Methods 0.000 claims description 23
230000007062 hydrolysis Effects 0.000 claims description 14
238000006460 hydrolysis reaction Methods 0.000 claims description 14
150000002978 peroxides Chemical class 0.000 claims description 11
239000000945 filler Substances 0.000 claims description 9
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
239000000203 mixture Substances 0.000 claims description 6
238000012432 intermediate storage Methods 0.000 claims description 4
238000002156 mixing Methods 0.000 claims description 4
150000003464 sulfur compounds Chemical class 0.000 claims description 3
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
239000006096 absorbing agent Substances 0.000 claims description 2
229910017604 nitric acid Inorganic materials 0.000 claims description 2
LDVVMCZRFWMZSG-UHFFFAOYSA-N captan Chemical compound C1C=CCC2C(=O)N(SC(Cl)(Cl)Cl)C(=O)C21 LDVVMCZRFWMZSG-UHFFFAOYSA-N 0.000 claims 22
JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims 3
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
238000002347 injection Methods 0.000 claims 2
239000007924 injection Substances 0.000 claims 2
238000009795 derivation Methods 0.000 claims 1
239000004310 lactic acid Substances 0.000 claims 1
235000014655 lactic acid Nutrition 0.000 claims 1
238000005201 scrubbing Methods 0.000 description 13
239000000047 product Substances 0.000 description 11
230000001413 cellular effect Effects 0.000 description 9
238000010521 absorption reaction Methods 0.000 description 6
239000000243 solution Substances 0.000 description 6
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 5
239000007788 liquid Substances 0.000 description 5
235000011149 sulphuric acid Nutrition 0.000 description 5
238000005868 electrolysis reaction Methods 0.000 description 4
238000001704 evaporation Methods 0.000 description 3
230000008020 evaporation Effects 0.000 description 3
239000012535 impurity Substances 0.000 description 3
239000002002 slurry Substances 0.000 description 3
238000003860 storage Methods 0.000 description 3
QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
150000001875 compounds Chemical class 0.000 description 2
239000000470 constituent Substances 0.000 description 2
238000000354 decomposition reaction Methods 0.000 description 2
239000003546 flue gas Substances 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
229910000372 mercury(II) sulfate Inorganic materials 0.000 description 2
FHHJDRFHHWUPDG-UHFFFAOYSA-N peroxysulfuric acid Chemical compound OOS(O)(=O)=O FHHJDRFHHWUPDG-UHFFFAOYSA-N 0.000 description 2
238000001556 precipitation Methods 0.000 description 2
238000000746 purification Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
229910052717 sulfur Inorganic materials 0.000 description 2
239000011593 sulfur Substances 0.000 description 2
238000011144 upstream manufacturing Methods 0.000 description 2
235000008733 Citrus aurantifolia Nutrition 0.000 description 1
235000011941 Tilia x europaea Nutrition 0.000 description 1
239000003463 adsorbent Substances 0.000 description 1
229910021529 ammonia Inorganic materials 0.000 description 1
230000005587 bubbling Effects 0.000 description 1
238000001354 calcination Methods 0.000 description 1
239000001506 calcium phosphate Substances 0.000 description 1
239000003610 charcoal Substances 0.000 description 1
238000003889 chemical engineering Methods 0.000 description 1
239000003795 chemical substances by application Substances 0.000 description 1
230000003749 cleanliness Effects 0.000 description 1
238000010276 construction Methods 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
230000000694 effects Effects 0.000 description 1
230000005518 electrochemistry Effects 0.000 description 1
230000008030 elimination Effects 0.000 description 1
238000003379 elimination reaction Methods 0.000 description 1
239000003344 environmental pollutant Substances 0.000 description 1
238000011049 filling Methods 0.000 description 1
230000010354 integration Effects 0.000 description 1
239000004571 lime Substances 0.000 description 1
239000000463 material Substances 0.000 description 1
229910021645 metal ion Inorganic materials 0.000 description 1
RVMFLWODSKUVCY-UHFFFAOYSA-N methylazanium;sulfite Chemical compound NC.NC.OS(O)=O RVMFLWODSKUVCY-UHFFFAOYSA-N 0.000 description 1
239000003595 mist Substances 0.000 description 1
238000006386 neutralization reaction Methods 0.000 description 1
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
150000002894 organic compounds Chemical class 0.000 description 1
230000001590 oxidative effect Effects 0.000 description 1
238000012856 packing Methods 0.000 description 1
238000005192 partition Methods 0.000 description 1
150000004965 peroxy acids Chemical class 0.000 description 1
231100000719 pollutant Toxicity 0.000 description 1
238000010926 purge Methods 0.000 description 1
238000011084 recovery Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000012265 solid product Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 1
229940078499 tricalcium phosphate Drugs 0.000 description 1
229910000391 tricalcium phosphate Inorganic materials 0.000 description 1
235000019731 tricalcium phosphate Nutrition 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Classifications

- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D47/00—Separating dispersed particles from gases, air or vapours by liquid as separating agent
- B01D47/10—Venturi scrubbers
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/74—Preparation
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/10—Greenhouse gas [GHG] capture, material saving, heat recovery or other energy efficient measures, e.g. motor control, characterised by manufacturing processes, e.g. for rolling metal or metal working

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Inorganic Chemistry (AREA)
Health & Medical Sciences (AREA)
Biomedical Technology (AREA)
Environmental & Geological Engineering (AREA)
Analytical Chemistry (AREA)
General Chemical & Material Sciences (AREA)
Oil, Petroleum & Natural Gas (AREA)
Treating Waste Gases (AREA)

FI1370/74A 1973-05-08 1974-05-06 Foerfarande foer avlaegsnande av gasformiga foeroreningar ur svavelsyrakontaktanordningars avgaser FI56490C (fi)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE2322982		1973-05-08
DE2322982A DE2322982C3 (de)	1973-05-08	1973-05-08	Verfahren zur Entfernung von gasförmigen Verunreinigungen aus Abgasen von Schwefelsäurekontaktanlagen

Publications (2)

Publication Number	Publication Date
FI56490B FI56490B (fi)	1979-10-31
FI56490C true FI56490C (fi)	1980-02-11

Family

ID=5880207

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
FI1370/74A FI56490C (fi)	1973-05-08	1974-05-06	Foerfarande foer avlaegsnande av gasformiga foeroreningar ur svavelsyrakontaktanordningars avgaser

Country Status (15)

Country	Link
US (1)	US3944401A (de)
JP (2)	JPS5018384A (de)
AT (1)	AT333784B (de)
BE (1)	BE814693R (de)
CA (1)	CA1019540A (de)
CH (1)	CH576803A5 (de)
DE (1)	DE2322982C3 (de)
ES (1)	ES424676A2 (de)
FI (1)	FI56490C (de)
FR (1)	FR2228528B2 (de)
GB (1)	GB1465371A (de)
IT (1)	IT1046117B (de)
NL (1)	NL182213C (de)
SE (1)	SE412994B (de)
ZA (1)	ZA742211B (de)

Families Citing this family (44)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2505828C3 (de) *	1975-02-12	1980-06-12	Sued-Chemie Ag, 8000 Muenchen	Verfahren und Vorrichtung zur Erzeugung von konzentrierter Schwefelsäure und/oder Oleum
DE2519928C3 (de) *	1975-05-05	1981-04-02	Metallgesellschaft Ag, 6000 Frankfurt	Verfahren zur Herstellung von Schwefelsäure
CA1059943A (en) *	1976-07-20	1979-08-07	Noranda Mines Limited	Electrolytically forming peroxosulfuric acid to oxidize organic material in sulfuric acid
US4256468A (en) *	1977-12-28	1981-03-17	Bethlehem Steel Corporation	Method for cleaning sinter plant gas emissions
US4409064A (en) *	1978-10-16	1983-10-11	Air Products And Chemicals, Inc.	Process for concentrating sulfuric acid in an evaporator
DE2945021A1 (de) *	1979-11-08	1981-05-21	Metallgesellschaft Ag, 6000 Frankfurt	Verfahren zur herstellung von konzentrierter schwefelsaeure
DE3008718C2 (de) *	1980-03-07	1987-01-22	Hölter, Heinz, Dipl.-Ing., 4390 Gladbeck	Vorrichtung zur Gaswäsche für Chemisorptionsanlagen
WO1981003034A1 (en) *	1980-04-25	1981-10-29	Pacific Eng & Prod Co Nevada	Matched stage odor control system
US4310502A (en) *	1980-05-29	1982-01-12	Rockwell International Corporation	Singlet delta oxygen generator and process
US4996038A (en) *	1983-07-05	1991-02-26	Monsanto Company	Heat recovery from concentrated sulfuric acid
AT383049B (de) *	1985-01-28	1987-05-11	Elin Union Ag	Verfahren zur reduzierung der emissionswerte von industriellen abgasen und industrieller abluft
DE3507718A1 (de) *	1985-03-05	1986-09-11	Nukem Gmbh, 6450 Hanau	Verfahren zur reinigung von rauchgasen
US4668498A (en) *	1985-09-27	1987-05-26	Davis James A	Supersonic singlet delta oxygen aerosol generator
US4830718A (en) *	1985-10-21	1989-05-16	John Stauffer	Removal of sulfur dioxide (SO2) from waste gases and recovery as sulfuric acid
US4654205A (en) *	1986-01-15	1987-03-31	C-I-L Inc.	Sulphur trioxide absorption apparatus and process
DE3629766A1 (de) *	1986-09-02	1988-03-17	Bayer Ag	Verfahren zur reinigung und wiederaufheizung von abgasen
US5009869A (en) *	1987-12-28	1991-04-23	Electrocinerator Technologies, Inc.	Methods for purification of air
AU622372B2 (en) *	1988-12-30	1992-04-02	John E. Stauffer	Removal of sulfur dioxide from waste gases and recovery as sulfuric acid
US5505767A (en) *	1994-06-08	1996-04-09	Minor; Cheryl	System and process for collecting sulfuric acid fumes
US5593652A (en) *	1995-06-28	1997-01-14	Vulcan Materials Company	Method for increasing the production capacity of sulfuric acid plants and processes
US5683670A (en) *	1995-06-28	1997-11-04	Vulcan Materials Company	Method for increasing the production capacity of sulfuric acid plants and processes
AT402264B (de)	1995-09-07	1997-03-25	Austrian Energy & Environment	Verfahren und einrichtung zur nassen abscheidung saurer gase
US6019818A (en) *	1996-09-27	2000-02-01	G.F.K. Consulting, Ltd.	Combination quenching and scrubbing process and apparatus therefor
US6174510B1 (en) *	1999-08-27	2001-01-16	Marcos D. Riano	Multi-pass cocurrent flow sulfuric acid tower process
US6312503B1 (en) *	1999-10-13	2001-11-06	Arteva North America S.A.R.L.	System to quench gasses and remove condensables
TW527221B (en) *	2000-08-21	2003-04-11	Sumitomo Chemical Co	Method for removing sulfuric acid mist and apparatus for removing the same
KR20020080032A (ko) *	2001-04-10	2002-10-23	송용철	탈취시스템 및 이를 이용한 탈취방법
DE10118961B4 (de) *	2001-04-10	2006-08-31	Thermoselect Ag	Wäscher und Verfahren zum Reinigen von Gasen
US6726748B2 (en) *	2002-07-16	2004-04-27	The Babcock & Wilcox Company	Method of converting a downflow/upflow wet flue gas desulfurization (WFGD) system to an upflow single-loop WFGD system
US20040188356A1 (en) *	2003-03-24	2004-09-30	Haydock Intellectual Properties, L.L.C.	System for producing large particle precipitates
JP2007534601A (ja) *	2004-04-27	2007-11-29	アルベマール・コーポレーシヨン	二酸化イオウの併流酸化法およびテトラブロモフタル酸無水物の製造におけるその使用
EP1912723A4 (de) *	2006-05-03	2011-08-03	Snc Lavalin Europ N V Sa	Gasquench- und wäscherabzugssystem
JP4891705B2 (ja) *	2006-08-28	2012-03-07	ヤンマー株式会社	コンバイン
WO2009023186A2 (en) *	2007-08-10	2009-02-19	Freije Treatment Systems, Inc.	Method and apparatus for treating a fluid
US20110192179A1 (en) *	2010-02-05	2011-08-11	Freije Iii William F	Evaporative heat transfer system and method
EP2578293A4 (de) *	2010-05-31	2015-01-28	Mitsubishi Heavy Ind Ltd	Abgasverarbeitungssystem und -verfahren
JPWO2011152548A1 (ja)	2010-05-31	2013-08-01	三菱重工業株式会社	排ガス処理システム及び方法
CA2800997C (en)	2010-05-31	2015-12-22	Mitsubishi Heavy Industries, Ltd.	Air pollution control system and method
CN102500126B (zh) *	2011-12-11	2014-06-04	浙江大学	净化处理含持久性有机污染物高温烟气的方法及装置
CN102657991B (zh) *	2012-05-24	2014-04-16	深圳市泓耀环保有限公司	一体化文丘里空气洗涤装置
TW201432204A (zh) *	2013-02-08	2014-08-16	Wholetech System Hitech Ltd	燃燒式有害氣體處理裝置
CN104353306B (zh) *	2014-10-27	2016-05-04	瓮福（集团）有限责任公司	一种硫酸炉气净化工艺装置
JP7085818B2 (ja) *	2017-10-31	2022-06-17	三菱重工エンジニアリング株式会社	ガス処理装置及びガス処理方法、ｃｏ２回収装置及びｃｏ２回収方法
EP4077212B1 (de)	2019-12-19	2024-02-07	Metso Metals Oy	Venturi-absorberrohr zum absorbieren von schwefeltrioxid in schwefelsäure

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE670966C (de) *	1937-05-09	1939-01-28	I G Farbenindustrie Akt Ges	Verfahren zur Gewinnung von Schwefelsaeure aus gasfoermigen Schwefelverbindungen niederer Oxydationsstufe
DE1234912B (de) *	1961-12-02	1967-02-23	Otto & Co Gmbh Dr C	Verfahren zur Entfernung der Schwefeloxyde aus Rauchgasen
US3523880A (en) *	1967-12-27	1970-08-11	Ionics	Electrolytic cell for removal and recovery of so2 from waste gases
US3524801A (en) *	1968-02-09	1970-08-18	Ionics	Process for producing sulfuric acid from so2 containing waste gas
CH547231A (de) *	1970-10-15	1974-03-29	Metallgesellschaft Ag	Zwischenabsorber fuer die absorption von so3 und verfahren zum betreiben des zwischenabsorbers.
DE2050580C3 (de) *	1970-10-15	1979-09-06	Metallgesellschaft Ag, 6000 Frankfurt	Vorrichtung zur Absorption von gasförmigen Bestandteilen
US3760061A (en) *	1971-03-02	1973-09-18	Du Pont	High-strength acid containing h2o2 to scrub so2

1973
- 1973-05-08 DE DE2322982A patent/DE2322982C3/de not_active Expired
1974
- 1974-03-14 NL NLAANVRAGE7403424,A patent/NL182213C/xx not_active IP Right Cessation
- 1974-03-27 ES ES424676A patent/ES424676A2/es not_active Expired
- 1974-03-29 AT AT264474A patent/AT333784B/de active
- 1974-04-05 ZA ZA00742211A patent/ZA742211B/xx unknown
- 1974-04-12 FR FR7413071A patent/FR2228528B2/fr not_active Expired
- 1974-05-02 JP JP49049639A patent/JPS5018384A/ja active Pending
- 1974-05-03 IT IT22250/74A patent/IT1046117B/it active
- 1974-05-03 CH CH605474A patent/CH576803A5/xx not_active IP Right Cessation
- 1974-05-06 FI FI1370/74A patent/FI56490C/fi active
- 1974-05-06 US US05/467,387 patent/US3944401A/en not_active Expired - Lifetime
- 1974-05-07 GB GB2017474A patent/GB1465371A/en not_active Expired
- 1974-05-07 BE BE6044569A patent/BE814693R/xx not_active IP Right Cessation
- 1974-05-08 CA CA199,328A patent/CA1019540A/en not_active Expired
- 1974-05-08 SE SE7406163A patent/SE412994B/xx not_active IP Right Cessation
1981
- 1981-11-18 JP JP56185141A patent/JPS57174124A/ja active Pending

Also Published As

Publication number	Publication date
JPS57174124A (en)	1982-10-26
ZA742211B (en)	1975-11-26
FR2228528B2 (de)	1977-01-07
AT333784B (de)	1976-12-10
ATA264474A (de)	1976-04-15
GB1465371A (en)	1977-02-23
NL182213B (nl)	1987-09-01
FI56490B (fi)	1979-10-31
IT1046117B (it)	1980-06-30
DE2322982C3 (de)	1979-09-13
JPS5018384A (de)	1975-02-26
AU6830974A (en)	1975-10-30
US3944401A (en)	1976-03-16
SE412994B (sv)	1980-03-31
CA1019540A (en)	1977-10-25
DE2322982B2 (de)	1979-01-18
NL7403424A (de)	1974-11-12
BE814693R (fr)	1974-11-07
NL182213C (nl)	1988-02-01
CH576803A5 (de)	1976-06-30
FR2228528A2 (de)	1974-12-06
ES424676A2 (es)	1976-01-16
DE2322982A1 (de)	1974-11-28

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