FR2496128A1 - Bains de revetement electrolytique pour obtenir des depots blancs de palladium metallique, renfermant une source de palladium, un sel d'ammonium, un agent organique de brillance et de l'ammoniaque - Google Patents
Bains de revetement electrolytique pour obtenir des depots blancs de palladium metallique, renfermant une source de palladium, un sel d'ammonium, un agent organique de brillance et de l'ammoniaque Download PDFInfo
- Publication number
- FR2496128A1 FR2496128A1 FR8122681A FR8122681A FR2496128A1 FR 2496128 A1 FR2496128 A1 FR 2496128A1 FR 8122681 A FR8122681 A FR 8122681A FR 8122681 A FR8122681 A FR 8122681A FR 2496128 A1 FR2496128 A1 FR 2496128A1
- Authority
- FR
- France
- Prior art keywords
- palladium
- bath
- bath according
- ammonium
- ammonium salt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 title claims abstract description 95
- 229910052763 palladium Inorganic materials 0.000 title claims abstract description 38
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 238000000576 coating method Methods 0.000 title claims abstract description 23
- 239000011248 coating agent Substances 0.000 title claims abstract description 21
- 229910021529 ammonia Inorganic materials 0.000 title claims abstract description 16
- 150000003863 ammonium salts Chemical class 0.000 title claims description 10
- 239000003795 chemical substances by application Substances 0.000 title description 6
- 238000000151 deposition Methods 0.000 claims description 7
- HOGKWLXRMABQDU-UHFFFAOYSA-N OB(O)OB(O)O.N.N.N.N Chemical group OB(O)OB(O)O.N.N.N.N HOGKWLXRMABQDU-UHFFFAOYSA-N 0.000 claims description 5
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims description 5
- 230000008021 deposition Effects 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- 239000006172 buffering agent Substances 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 3
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 3
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 3
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 239000000758 substrate Substances 0.000 claims description 3
- DLDJFQGPPSQZKI-UHFFFAOYSA-N but-2-yne-1,4-diol Chemical compound OCC#CCO DLDJFQGPPSQZKI-UHFFFAOYSA-N 0.000 claims description 2
- 239000004020 conductor Substances 0.000 claims description 2
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical group [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 229940081974 saccharin Drugs 0.000 claims description 2
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 claims description 2
- 235000019204 saccharin Nutrition 0.000 claims description 2
- 239000000901 saccharin and its Na,K and Ca salt Substances 0.000 claims description 2
- 239000001166 ammonium sulphate Substances 0.000 claims 1
- 239000000126 substance Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 abstract description 7
- 229910052751 metal Inorganic materials 0.000 abstract description 3
- 239000002184 metal Substances 0.000 abstract description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 16
- 229910052759 nickel Inorganic materials 0.000 description 8
- 229910052703 rhodium Inorganic materials 0.000 description 7
- 239000010948 rhodium Substances 0.000 description 7
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 7
- 239000000872 buffer Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000005282 brightening Methods 0.000 description 3
- 238000002310 reflectometry Methods 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000009713 electroplating Methods 0.000 description 2
- FTLYMKDSHNWQKD-UHFFFAOYSA-N (2,4,5-trichlorophenyl)boronic acid Chemical compound OB(O)C1=CC(Cl)=C(Cl)C=C1Cl FTLYMKDSHNWQKD-UHFFFAOYSA-N 0.000 description 1
- WHOZNOZYMBRCBL-OUKQBFOZSA-N (2E)-2-Tetradecenal Chemical compound CCCCCCCCCCC\C=C\C=O WHOZNOZYMBRCBL-OUKQBFOZSA-N 0.000 description 1
- ORTVZLZNOYNASJ-UPHRSURJSA-N (z)-but-2-ene-1,4-diol Chemical compound OC\C=C/CO ORTVZLZNOYNASJ-UPHRSURJSA-N 0.000 description 1
- ZMESHQOXZMOOQQ-UHFFFAOYSA-N 1-(naphthalen-1-ylmethyl)naphthalene Chemical compound C1=CC=C2C(CC=3C4=CC=CC=C4C=CC=3)=CC=CC2=C1 ZMESHQOXZMOOQQ-UHFFFAOYSA-N 0.000 description 1
- -1 Allyl sulfonate Chemical compound 0.000 description 1
- 239000004254 Ammonium phosphate Substances 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 206010026749 Mania Diseases 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical class OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- 235000011941 Tilia x europaea Nutrition 0.000 description 1
- XMXZJUHGOGNHMO-UHFFFAOYSA-N [Na].C(C#CCO)O Chemical compound [Na].C(C#CCO)O XMXZJUHGOGNHMO-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 1
- 235000019289 ammonium phosphates Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 229940077388 benzenesulfonate Drugs 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 150000001642 boronic acid derivatives Chemical class 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004070 electrodeposition Methods 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229940020445 flector Drugs 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000004571 lime Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000002815 nickel Chemical class 0.000 description 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 description 1
- PIBWKRNGBLPSSY-UHFFFAOYSA-L palladium(II) chloride Chemical compound Cl[Pd]Cl PIBWKRNGBLPSSY-UHFFFAOYSA-L 0.000 description 1
- 229940044654 phenolsulfonic acid Drugs 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 229940085605 saccharin sodium Drugs 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000004071 soot Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/50—Electroplating: Baths therefor from solutions of platinum group metals
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US21731680A | 1980-12-17 | 1980-12-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| FR2496128A1 true FR2496128A1 (fr) | 1982-06-18 |
Family
ID=22810545
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR8122681A Withdrawn FR2496128A1 (fr) | 1980-12-17 | 1981-12-03 | Bains de revetement electrolytique pour obtenir des depots blancs de palladium metallique, renfermant une source de palladium, un sel d'ammonium, un agent organique de brillance et de l'ammoniaque |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS57123993A (de) |
| AT (1) | AT375965B (de) |
| AU (1) | AU530024B2 (de) |
| BR (1) | BR8108191A (de) |
| CH (1) | CH647010A5 (de) |
| DE (1) | DE3147251A1 (de) |
| ES (1) | ES508036A0 (de) |
| FR (1) | FR2496128A1 (de) |
| GB (1) | GB2090867B (de) |
| HK (1) | HK67286A (de) |
| IT (1) | IT8149860A0 (de) |
| SE (1) | SE8106693L (de) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0415631A1 (de) * | 1989-08-29 | 1991-03-06 | AT&T Corp. | Elektroabscheidung einer Palladiumschicht |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU323467A1 (de) * | Киевский ордена Ленина политехнический институт имени лети | |||
| GB1171734A (en) * | 1967-09-08 | 1969-11-26 | Sel Rex Corp | Improvements in and relating to the electro-deposition of palladium. |
| US3530050A (en) * | 1964-06-12 | 1970-09-22 | Johnson Matthey Co Ltd | Electrodeposition of palladium |
| US3972787A (en) * | 1974-06-14 | 1976-08-03 | Lea-Ronal, Inc. | Palladium electrolyte baths utilizing quaternized pyridine compounds as brighteners |
| SU572539A1 (ru) * | 1976-04-29 | 1977-09-15 | Минский радиотехнический институт | Электролит дл осаждени паллади |
| US4066517A (en) * | 1976-03-11 | 1978-01-03 | Oxy Metal Industries Corporation | Electrodeposition of palladium |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4098656A (en) * | 1976-03-11 | 1978-07-04 | Oxy Metal Industries Corporation | Bright palladium electroplating baths |
| DE2839360C2 (de) * | 1978-09-09 | 1982-11-04 | Oxy Metal Industries Corp., Detroit, Mich. | Wäßriges Bad zur galvanischen Abscheidung von glänzenden Überzügen aus Palladium oder seinen Legierungen |
| CH649581A5 (de) * | 1979-08-20 | 1985-05-31 | Oxy Metal Industries Corp | Mittel zur elektrolytischen ablagerung von metallischem palladium auf einem substrat. |
-
1981
- 1981-11-11 SE SE8106693A patent/SE8106693L/ not_active Application Discontinuation
- 1981-11-16 AU AU77532/81A patent/AU530024B2/en not_active Ceased
- 1981-11-28 DE DE19813147251 patent/DE3147251A1/de not_active Ceased
- 1981-12-03 FR FR8122681A patent/FR2496128A1/fr not_active Withdrawn
- 1981-12-09 IT IT8149860A patent/IT8149860A0/it unknown
- 1981-12-09 AT AT0527381A patent/AT375965B/de not_active IP Right Cessation
- 1981-12-15 JP JP56202350A patent/JPS57123993A/ja active Pending
- 1981-12-16 ES ES508036A patent/ES508036A0/es active Granted
- 1981-12-16 CH CH803381A patent/CH647010A5/de not_active IP Right Cessation
- 1981-12-16 GB GB8137925A patent/GB2090867B/en not_active Expired
- 1981-12-16 BR BR8108191A patent/BR8108191A/pt unknown
-
1986
- 1986-09-11 HK HK672/86A patent/HK67286A/xx unknown
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU323467A1 (de) * | Киевский ордена Ленина политехнический институт имени лети | |||
| US3530050A (en) * | 1964-06-12 | 1970-09-22 | Johnson Matthey Co Ltd | Electrodeposition of palladium |
| GB1171734A (en) * | 1967-09-08 | 1969-11-26 | Sel Rex Corp | Improvements in and relating to the electro-deposition of palladium. |
| US3972787A (en) * | 1974-06-14 | 1976-08-03 | Lea-Ronal, Inc. | Palladium electrolyte baths utilizing quaternized pyridine compounds as brighteners |
| US4066517A (en) * | 1976-03-11 | 1978-01-03 | Oxy Metal Industries Corporation | Electrodeposition of palladium |
| SU572539A1 (ru) * | 1976-04-29 | 1977-09-15 | Минский радиотехнический институт | Электролит дл осаждени паллади |
Non-Patent Citations (2)
| Title |
|---|
| CHEMICAL ABSTRACTS, vol.76, no.14, 3 avril 1972, page 574, résumé no. 80307n, COLUMBUS, Ohio (US) & SU-A1-323 467 (KIEV POLYTECHNIC INSTITURE) (10 décembre 1971) * |
| GALVANOTECHNIK, vol.68, no.12, décembre 1977, SAULGAU (DE) & SU-A1-572 539, page 1133 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0415631A1 (de) * | 1989-08-29 | 1991-03-06 | AT&T Corp. | Elektroabscheidung einer Palladiumschicht |
Also Published As
| Publication number | Publication date |
|---|---|
| GB2090867B (en) | 1984-08-01 |
| ES8304221A1 (es) | 1983-02-16 |
| HK67286A (en) | 1986-09-18 |
| DE3147251A1 (de) | 1982-09-09 |
| ES508036A0 (es) | 1983-02-16 |
| BR8108191A (pt) | 1982-09-28 |
| ATA527381A (de) | 1984-02-15 |
| AT375965B (de) | 1984-09-25 |
| JPS57123993A (en) | 1982-08-02 |
| AU530024B2 (en) | 1983-06-30 |
| AU7753281A (en) | 1982-06-24 |
| GB2090867A (en) | 1982-07-21 |
| SE8106693L (sv) | 1982-06-18 |
| IT8149860A0 (it) | 1981-12-09 |
| CH647010A5 (de) | 1984-12-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| CD | Change of name or company name | ||
| TP | Transmission of property | ||
| ST | Notification of lapse |