FR3138658B1 - Procédé d’extraction sélective d’un sel à extraire à partir d’une saumure - Google Patents

Procédé d’extraction sélective d’un sel à extraire à partir d’une saumure

Info

Publication number
FR3138658B1
FR3138658B1 FR2208067A FR2208067A FR3138658B1 FR 3138658 B1 FR3138658 B1 FR 3138658B1 FR 2208067 A FR2208067 A FR 2208067A FR 2208067 A FR2208067 A FR 2208067A FR 3138658 B1 FR3138658 B1 FR 3138658B1
Authority
FR
France
Prior art keywords
salt
brine
organic phase
extracted
sent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2208067A
Other languages
English (en)
Other versions
FR3138658A1 (fr
Inventor
Souza Guillaume De
Florent Bouquet
Jim Vicens
Andrea Trujillo
Lucas Verbrugghe
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Adionics SAS
Original Assignee
Adionics SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR2208067A priority Critical patent/FR3138658B1/fr
Application filed by Adionics SAS filed Critical Adionics SAS
Priority to PCT/IB2023/057828 priority patent/WO2024028786A1/fr
Priority to US19/100,829 priority patent/US20260042036A1/en
Priority to EP23767966.7A priority patent/EP4565723A1/fr
Priority to ARP230102032A priority patent/AR130097A1/es
Priority to KR1020257006640A priority patent/KR20250097792A/ko
Priority to CN202380057353.2A priority patent/CN119768543A/zh
Priority to CA3263957A priority patent/CA3263957A1/fr
Priority to JP2025505979A priority patent/JP2025527275A/ja
Publication of FR3138658A1 publication Critical patent/FR3138658A1/fr
Priority to CL2025000288A priority patent/CL2025000288A1/es
Priority to MX2025001348A priority patent/MX2025001348A/es
Application granted granted Critical
Publication of FR3138658B1 publication Critical patent/FR3138658B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B01D11/043—Counter-current multistage extraction towers in a vertical or sloping position with stationary contacting elements, sieve plates or loose contacting elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B01D11/0434—Counter-current multistage extraction towers in a vertical or sloping position comprising rotating mechanisms, e.g. mixers, rotational oscillating motion, mixing pumps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B01D11/0438—Counter-current multistage extraction towers in a vertical or sloping position comprising vibrating mechanisms, electromagnetic radiations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0446—Juxtaposition of mixers-settlers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0488—Flow sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/26—Treatment of water, waste water, or sewage by extraction
    • C02F1/265—Desalination
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10—Obtaining alkali metals
    • C22B26/12—Obtaining lithium
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
    • C22B3/32—Carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/441—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/44—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/447—Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by membrane distillation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • C02F1/683—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water by addition of complex-forming compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Water Supply & Treatment (AREA)
  • Hydrology & Water Resources (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Toxicology (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)

Abstract

Procédé d’extraction sélective d’un sel à extraire à partir d’une saumure La présente invention porte sur un procédé d’extraction sélective d’un sel à extraire à partir d’une saumure à traiter contenant ledit sel à extraire, caractérisé par le fait que : on adresse la saumure à traiter (S1) à un agitateur-mélangeur (1a) d’extraction dans lequel on introduit également une phase organique hydrophobe liquide, on mélange ladite saumure et ladite phase organique hydrophobe liquide dans ledit agitateur mélangeur (1a) d’extraction, et on adresse le mélange à un décanteur-séparateur (1d), pour obtenir : une saumure de laquelle du sel à extraire a été retiré ; et une phase organique chargée en sel à extraire ; on récupère la saumure de laquelle le sel à extraire a été retiré ; on adresse la phase organique chargée en sel à extraire à un échangeur de chaleur dit « organique » (1e) dans lequel elle est réchauffée avant d’être adressée à une colonne (1c ; 2c) dite de régénération dans laquelle on réalise un échange à contre-courant avec de l’eau chaude, se trouvant à une température supérieure à celle de la saumure de départ, pour obtenir : une eau contenant le sel à extraire ; et une phase organique régénérée, ayant perdu le sel à extraire ; on recycle la phase organique régénérée dans l’agitateur-mélangeur (1a) d’extraction.
FR2208067A 2022-08-03 2022-08-03 Procédé d’extraction sélective d’un sel à extraire à partir d’une saumure Active FR3138658B1 (fr)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FR2208067A FR3138658B1 (fr) 2022-08-03 2022-08-03 Procédé d’extraction sélective d’un sel à extraire à partir d’une saumure
JP2025505979A JP2025527275A (ja) 2022-08-03 2023-08-02 塩水またはブラインから抽出すべき塩を選択的に抽出する方法
EP23767966.7A EP4565723A1 (fr) 2022-08-03 2023-08-02 Procédé d'extraction sélective d'un sel à extraire à partir d'une eau salée ou saumure
ARP230102032A AR130097A1 (es) 2022-08-03 2023-08-02 Proceso para la extracción selectiva de una sal a extraer de un agua salada o salmuera
KR1020257006640A KR20250097792A (ko) 2022-08-03 2023-08-02 염수 또는 염물로부터 추출될 염을 선택적으로 추출하기 위한 방법
CN202380057353.2A CN119768543A (zh) 2022-08-03 2023-08-02 从盐水或咸水中选择性提取盐的方法
PCT/IB2023/057828 WO2024028786A1 (fr) 2022-08-03 2023-08-02 Procédé d'extraction sélective d'un sel à extraire à partir d'une eau salée ou saumure
US19/100,829 US20260042036A1 (en) 2022-08-03 2023-08-02 Method for selectively extracting a salt to be extracted from saltwater or brine
CA3263957A CA3263957A1 (fr) 2022-08-03 2023-08-02 Method for selectively extracting a salt to be extracted from saltwater or brine
CL2025000288A CL2025000288A1 (es) 2022-08-03 2025-01-30 Proceso para extracción selectiva de una sal a extraer de un agua salada o salmuera
MX2025001348A MX2025001348A (es) 2022-08-03 2025-01-31 Proceso para la extracción selectiva de una sal a extraer de un agua salada o salmuera

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2208067 2022-08-03
FR2208067A FR3138658B1 (fr) 2022-08-03 2022-08-03 Procédé d’extraction sélective d’un sel à extraire à partir d’une saumure

Publications (2)

Publication Number Publication Date
FR3138658A1 FR3138658A1 (fr) 2024-02-09
FR3138658B1 true FR3138658B1 (fr) 2025-11-07

Family

ID=84053285

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2208067A Active FR3138658B1 (fr) 2022-08-03 2022-08-03 Procédé d’extraction sélective d’un sel à extraire à partir d’une saumure

Country Status (1)

Country Link
FR (1) FR3138658B1 (fr)

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3433584A (en) * 1966-03-07 1969-03-18 St Paul Ammonia Products Inc Production of potassium nitrate from calcium nitrate
US5336297A (en) * 1993-02-16 1994-08-09 Terra Gaia Environmental Group Inc. Process for the treatment of electric arc furnace dust
FR3031738B1 (fr) * 2015-01-19 2018-10-05 Adionics Dispositif et methode de dessalement d'eau par deionisation thermique et liquide d'extraction ionique liquide applicable audit dispositif
FR3054140B1 (fr) * 2016-07-22 2018-08-31 Adionics Methode d’extraction de sels et composition extractante regeneree en temperature

Also Published As

Publication number Publication date
FR3138658A1 (fr) 2024-02-09

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