FR3143379B1 - Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d’une filtration - Google Patents

Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d’une filtration Download PDF

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Publication number
FR3143379B1
FR3143379B1 FR2213367A FR2213367A FR3143379B1 FR 3143379 B1 FR3143379 B1 FR 3143379B1 FR 2213367 A FR2213367 A FR 2213367A FR 2213367 A FR2213367 A FR 2213367A FR 3143379 B1 FR3143379 B1 FR 3143379B1
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France
Prior art keywords
liquid
solvent
aqueous
hmf
aqueous solution
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FR2213367A
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English (en)
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FR3143379A1 (fr
Inventor
Meriem Bouras
Olivier Cotte
Thi Bich Ngoc Dang
Espada Pastor Maria Fernandez
Kim Larmier
Hélène Lorcet
Alexandre Pagot
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
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Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to FR2213367A priority Critical patent/FR3143379B1/fr
Priority to EP23809628.3A priority patent/EP4634164A1/fr
Priority to JP2025534312A priority patent/JP2025539563A/ja
Priority to CN202380084677.5A priority patent/CN120282954A/zh
Priority to PCT/EP2023/082709 priority patent/WO2024125991A1/fr
Publication of FR3143379A1 publication Critical patent/FR3143379A1/fr
Application granted granted Critical
Publication of FR3143379B1 publication Critical patent/FR3143379B1/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B01D11/043—Counter-current multistage extraction towers in a vertical or sloping position with stationary contacting elements, sieve plates or loose contacting elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B01D11/0434—Counter-current multistage extraction towers in a vertical or sloping position comprising rotating mechanisms, e.g. mixers, rotational oscillating motion, mixing pumps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
    • B01D11/0438—Counter-current multistage extraction towers in a vertical or sloping position comprising vibrating mechanisms, electromagnetic radiations
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0446—Juxtaposition of mixers-settlers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0488—Flow sheets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/04—Solvent extraction of solutions which are liquid
    • B01D11/0492—Applications, solvents used

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

L’invention concerne un procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural (5-HMF), comprenant successivement a) une mise en contact de d’une charge (1) contenant du 5-HMF et un solvant de synthèse polaire aprotique avec un flux aqueux, b) une extraction liquide-liquide avec un solvant d’extraction organique suivie d’une étape de contre-lavage c) par un solvant aqueux pour obtenir un raffinat organique riche en 5-HMF et en solvant. Le raffinat organique, éventuellement concentré, est ensuite soumis à une étape d’hydrodistillation e) pour obtenir une solution aqueuse de 5-HMF. Une étape f) de séparation liquide-solide d’une fraction de particules solides formée par des humines précipitées et présente au sein du raffinat aqueux (5) issu de l’étape b) et/ou d’un flux liquide intermédiaire (19) issu de l’étape b) est réalisée. Le raffinat aqueux issu de l’étape b) d’extraction liquide-liquide, débarrassé des humines précipitées, est traité dans une étape g) de traitement de mélanges eau-solvant de synthèse polaire aprotique. Figure 1 à publier
FR2213367A 2022-12-14 2022-12-14 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d’une filtration Active FR3143379B1 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
FR2213367A FR3143379B1 (fr) 2022-12-14 2022-12-14 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d’une filtration
EP23809628.3A EP4634164A1 (fr) 2022-12-14 2023-11-22 Procédé de production d'une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d'une filtration
JP2025534312A JP2025539563A (ja) 2022-12-14 2023-11-22 濾過に組み込まれるまたは濾過前の液液抽出工程を含む５－ヒドロキシメチルフルフラールの水溶液を製造するための方法
CN202380084677.5A CN120282954A (zh) 2022-12-14 2023-11-22 包括结合了过滤或随后进行过滤的液-液萃取步骤的生产5-羟甲基糠醛水溶液的方法
PCT/EP2023/082709 WO2024125991A1 (fr) 2022-12-14 2023-11-22 Procédé de production d'une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d'une filtration

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2213367 2022-12-14
FR2213367A FR3143379B1 (fr) 2022-12-14 2022-12-14 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d’une filtration

Publications (2)

Publication Number Publication Date
FR3143379A1 FR3143379A1 (fr) 2024-06-21
FR3143379B1 true FR3143379B1 (fr) 2024-11-22

Family

ID=85278112

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2213367A Active FR3143379B1 (fr) 2022-12-14 2022-12-14 Procédé de production d’une solution aqueuse de 5-hydroxyméthylfurfural comportant une extraction liquide-liquide intégrant ou suivie d’une filtration

Country Status (5)

Country Link
EP (1) EP4634164A1 (fr)
JP (1) JP2025539563A (fr)
CN (1) CN120282954A (fr)
FR (1) FR3143379B1 (fr)
WO (1) WO2024125991A1 (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN119118965A (zh) * 2024-09-09 2024-12-13 厦门大学 一种原生木质生物质制备5-羟甲基糠醛及纯化的方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1342349A (en) 1970-11-11 1974-01-03 Southalls Birmingham Ltd Support devices
FR2669635B1 (fr) 1990-11-22 1994-06-10 Furchim Procede de fabrication d'hydroxymethylfurfural (hmf) du purete elevee.
EP1834950A1 (fr) 2006-03-10 2007-09-19 Avantium International B.V. Procédé de fabrication d'alkoxyméthylfurfurales et leur utilisation
FR3071172B1 (fr) * 2017-09-18 2019-10-04 IFP Energies Nouvelles Procede de separation des composes furaniques, en particulier le 5- hydroxymethylfurfural, du dimethoxysulfoxyde par des extractions liquide-liquide

Also Published As

Publication number Publication date
EP4634164A1 (fr) 2025-10-22
WO2024125991A1 (fr) 2024-06-20
FR3143379A1 (fr) 2024-06-21
JP2025539563A (ja) 2025-12-05
CN120282954A (zh) 2025-07-08

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