HUE028073T2 - Eljárás tiszta nanorészecskék elõállítására folyamatos áramlási rendszer alkalmazásával - Google Patents
Eljárás tiszta nanorészecskék elõállítására folyamatos áramlási rendszer alkalmazásával Download PDFInfo
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- B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
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Claims (7)
- Szabadalmi igénypontok1. Elf Ms tiszta, smbâlyozotî toéretö mmtësæxMk ifélyamatos áÉSt»íásÉ :r«rofc$erbên. tbïtéao AI· sêfït, amely oanerészeeskék; leiszfbÉt ífeliiéíakbv :8a$»gpR vagy egyél ®&cm: nroféknlák jgteeöek adszorbé-á$S8*: «tel a fidysmsdos áramlást purster olyan esôwsjæstéket larSidíház, a reagensek Is termékek |mma feiyamatoaan. ttstad, és; aarely eljárás legalább egy olyan lépést tartalmaz, amelyben egy pteknrzor anyag otóatöt reánkeios rssakesfeák' vebtnk alá agy jmdekálowzer oldat áilsirnszasávar, és banofészeeskék# «Iteœk elé, aszal jellemezve, hogy a réti-akciós reakciót az «toké lépés alán: egy, a redukálc-szen semiegeslîô anyag hozzáadásával leállítjuk, és nmíofészeeske kolloidot állítunk elé.
- 2. As I. Igénypont szerinti eljárás, amely eljárás tartalmaz egy olyan lépést, »élyfcen a prekarzor arsysg; oklatot redukciós reakciónak vetjük alá tedukiiAszer oldat aikalíoazáeával, és homogén nanorészeeskéket állt-tank elő.
- 3. .Az I. Igénypont szerinti eljárás, amely eljárás legalább két olyan lépést tartalmaz, amelyben a psístezdr anyag oldatta íedekxáés reakciónak vétjük alá rédtMlószér old® alkalmazásával és magdal íipasb félepS; danoídszecskékét állítunk elő.
- 4. Az leli. IgénypösttAk bármelyike smMl «ljéá% sbö! a jfékorzor anyag egy prektirzór vagy fém; prekurzorok keveréke. 5. Λ 4. igénypert szerinti eljárás, ahol a fém prekurzor egy fémso vagy különböző fémsók keveréke. 6. A 4. vagy 5. igénypont szerűn! eljárás, ahol a fém palladium. eziM, arany, platina, raténktm, oztnlten, rddsum, tédism, nikkel,,kitolt, féz és vas csoportjából van kiválasztva. '% Az Idi, igénypontok, bárjpélylke sástártí: eljárás, ahol » preknrzoí anyag égy Só ,%ΝΟ*, AgOOs, AgHSd* Ag:;SOs, AgWy ÄgPF*, Agl%, C%€ÓQAg, AgF:Fv$Ö3, €oC%: €^mh CiS<h, C«pSd$& Cu{CÍO,);í, CuF::, (CH€00}:Cn. B;.PtCiö. Η,,αΑΑΡι, P:Ck FtBr3, l^jPtCy, NadPtCb], LlfPCill. ijPtCOkii:, Fl(MO;d>, WÄfCtv [Pt(NH.s}4(HCO.O> jPiíNHO-dtOAefe, pM,j:iP;Br„ KjPtCW PlSCb, FdjHSOÁ, PitCKAfe, ftÄ% Μ2Ν?Μ Pb€k FdBrj, Κ,ΙΡοΟί,]. Ntnj'PdCy, iXpklCUl, H#d(ÖHj<;, m^L· (Μ(μη&¥3* I«»jíHcci*, (p#«^ô% cNea^dBó,, mm* BdpSÖ^, Mpiöp »Ä, Au€%. AttO,: An% (CMpSAußi Auf, AöCICSCÄk AaBr, AaBig, Na:,AuíSA>;. HAuBr,. ül AntjCN hl CoF> Co<NO:;}>, CoCb, CoS04, CoCHStXh, CoíCÍOp (CHCOOfeCo, ékfe, |Co{KHP)o<. rco(,KKH-iss<'í;. ;Α<χϋ€Α)ίΜΗρ]θ,, ms, mmOm WSO* B%m®éh \tvC.n>, ,C ICOO j Mi, VBr<, N-vOH>AxV N ,'JHK'k Fc, . i'cAO FeC% FeSO* FepSÖP, FepiCA),, tCMCOOhFe, feiB% FeF?: Fepöp, FeCk, FegFO.n, Fe(iíSO,;b:,:Fei€l04}x (CHCOÖjsFe, FeBr?, Rpai ijOlijiSöto BbClj, KnOIOsjj, iRnBri,: R«% Bup<â3)x ÇN* Ä.·^ mi, 08¾ ®m\ Os% IrFs, lifO;;,: Mir Ms, \%cm^ -^líCg, SsjféCgj, Najli^y, ^zï^l. ^P'Klÿ, yj{lí€y:, ííríNHjjXya, RhF,. RóF,. Ráa:í, jSh(NH?}?CI)í'b, RIClpftNsItlr KjRl5(G0)jG:ij| yp^wii tzéíumm m bídrátelt kévéréke! esopos^Äl kiiválesztva. I, àâ :l-|, 3ges?ypOítok bármelyike saerMl eljárás, ahol a redskálószer hkteí«s sszfcorbmsav, náírmm--bórhiárid, aáödmís-lápofoszií* hÎmm-tetraetnbôrhsdrjd, metanol, lJ“hex;jÄindiesk hidroxilsmi« és: dtmediildraza« DMAS dSO|>sfiäb^ va® kiválasztva,
- 9. Az SS.. la^sypoetisk bármelyike saééíati elfarás, aboi: a redykálbszeA semlegesítő anysg; Itidmgéíi--laerossd, Ózon* 01¾ ës egy sate pj-f&r esopotdáMI van kMasZiva, If* Ak $*#< sgáíívfontok Memelyfe szcd&tl eptás:, sthol g áramlási readtar csoszaldtszfe, somlj-ed a: főhessek,.« reakeíóteverék és: a termékek áraim áibáls4 ktSJ§8fe&§ hőmérsékleteken tanjak. H, As 1::,,. 2.,. 4-1:0. igénypontok bármelyike: szerinti eljárás,: aböl: a prekorzor agyag a tstkíkáldsKSr feldrssis «s a redekálászert semlegesM aítpgjlldrygéd'péíöx.iii I. 2:. As k* 2.,: 4-i:Í.: igénypontok bármelyike szerinti eljárás, alsói a. prekarzor anyag CoP^jj, a t«(káálósz®r %xámM és » téddkálészert semlegesítő anyag: hidrogémperokid:, ahol a redakák>s2prt semlegesítő anyag oldata KsÖH-t is taftaknaz. :13:. As ί ,, Ρΐδ.. ͧéi0&m0k W$0· ahol az első lépésben a ÇiP#a)s $8#toæar ssnvag: oldatát redukciós reakciónak vss^lk- sM iiidí&zilt: óidat alkalmazásáét ami rézmag képzbdésët #redt$&· κνορ,: és a másoátk lépésbe« a redkeMkeyeröknss: a PdPPií prekarzor agpsg oldatát adjuk, amelynek redtds-ciöja az első lépésiből képződött rés aas^BÉseesKéktm palládium héják képződését mdmáayezi.,--ls a redukciós ssesiksiÉ hidrogélo-gerozib oldat és egy bázis bözzáadáMvá!:: leállójuk. alsóba Mais koncentrációja: a iessuékákita sendeges pH-j ástak biztosításához elegendő,
- 14, Az ].J,S 4-:10:, ígéoypomok hánnelyike szerinti eljárás, ahol: a psttkuszor geyag Pdpp}2 ésP^NCkjp keverék«, amelyek reakciója Pd/'Pt ötydgöí Isöíítstgé« «agssnlsseeiifeémëk: képződését eredmeoyezl.
- 15. As 1-1¾.. igénypontok bánuelyifes szerinti: eprás,, ahol a redukálészert semlegesítő anyag egy redos ptíifer,.amelynek potenciálja a fémre-ap® íeyő külső fésnréteg potenciál tdsííi reddkálisira alkalmas* !b. As I -15 igpyponiok bármelyike szerinti eljárás, amely eljárás isttalmaz egy, 8 kolloid n&oörészecske eenoifugál&sára és/vagy szárítására vonatkozó további lépést, amelynek során oattorészecske pod.állbahk elő.
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| Application Number | Priority Date | Filing Date | Title |
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| PL399505A PL399505A1 (pl) | 2012-06-13 | 2012-06-13 | Sposób wytwarzania zasadniczo czystych nanoczastek w ukladzie przeplywowym, nanoczastki otrzymane tym sposobem oraz ich zastosowanie |
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| US (1) | US9221044B2 (hu) |
| EP (1) | EP2785483B1 (hu) |
| JP (1) | JP5807129B2 (hu) |
| DK (1) | DK2785483T3 (hu) |
| HR (1) | HRP20151121T1 (hu) |
| HU (1) | HUE028073T2 (hu) |
| PL (2) | PL399505A1 (hu) |
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Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL240163B1 (pl) * | 2014-02-14 | 2022-02-28 | Univ Warszawski | Sposób wytwarzania czystych nanocząstek metali szlachetnych o ścianach (100) oraz zastosowanie nanocząstek otrzymanych tym sposobem |
| JP6020506B2 (ja) | 2014-04-11 | 2016-11-02 | トヨタ自動車株式会社 | 触媒微粒子及びカーボン担持触媒の各製造方法 |
| EP3169465A1 (en) * | 2014-07-17 | 2017-05-24 | King Abdullah University Of Science And Technology | Scalable shape- and size-controlled synthesis of metal nano-alloys |
| CN106794448A (zh) | 2014-10-07 | 2017-05-31 | 巴斯夫公司 | 具有受控尺寸和形态的胶体贵金属纳米粒子的合成 |
| JP6096816B2 (ja) * | 2015-01-22 | 2017-03-15 | トヨタ自動車株式会社 | 触媒の製造方法及び製造装置 |
| DE112016003311T5 (de) | 2015-07-23 | 2018-05-24 | National Institute Of Advanced Industrial Science And Technology | Vorrichtung und Verfahren zum Herstellen einer Metall-Nanopartikel-Dispersion, Verfahren zum Herstellen eines Metall-Nanopartikel-Trägers, Metall-Nanopartikel, Metall-Nanopartikel-Dispersion und Metall-Nanopartikel-Träger |
| CN105214655B (zh) * | 2015-09-25 | 2017-07-28 | 北京化工大学 | 一种无负载纳米金属催化剂的制备及应用 |
| JP6821696B2 (ja) * | 2015-12-23 | 2021-01-27 | ウニヘルシテット・ワルシャフスキUniwersytet Warszawski | 準単原子層精度で無電解金属析出を行うための手段 |
| CN106914255B (zh) * | 2017-03-29 | 2020-03-03 | 国家纳米科学中心 | 一种非合金金属复合物及其制备方法和应用 |
| EP3635154A1 (en) * | 2017-06-06 | 2020-04-15 | Uniwersytet Warszawski | A method of electroless deposition of platinum group metals and their alloys and a plating bath used therein |
| CN107511479A (zh) * | 2017-09-08 | 2017-12-26 | 厦门大学 | 一种超薄壳层隔绝大粒径金纳米粒子的合成方法 |
| CN107648263A (zh) * | 2017-11-15 | 2018-02-02 | 福州大学 | 一种金铂双金属纳米粒子在制备细胞免疫治疗促进剂上的应用 |
| CL2017003489A1 (es) * | 2017-12-29 | 2018-05-25 | Univ Chile | Método secuencial para la construcción de nanopartículas de cobre metálico y su posterior decoración o revestimiento con nanopartículas más pequeñas del metal secundario |
| JP6847994B2 (ja) * | 2018-03-20 | 2021-03-24 | 旭化成株式会社 | 分散体の製造方法 |
| US20190308157A1 (en) * | 2018-04-09 | 2019-10-10 | COMSATS University Islamabad | One-step Dual Heater Based Flow Synthesis Setup for Synthesis of Inorganic Particles in Near Ambient Conditions |
| CN108588740B (zh) * | 2018-04-12 | 2019-08-30 | 商洛学院 | 一种用于水裂解产氧的Au-Ir纳米链电催化剂的制备方法 |
| CN108672718B (zh) * | 2018-06-07 | 2019-10-11 | 武汉船用电力推进装置研究所(中国船舶重工集团公司第七一二研究所) | 一种类球形银粉的制备方法 |
| EP3962531A4 (en) * | 2019-04-29 | 2023-05-17 | The Johns Hopkins University | PLASMID DNA NANOPARTICLES/POLYCATIONS OF DEFINED CONSTITUTION AND METHODS OF PREPARING THEM |
| CN110405200B (zh) * | 2019-06-18 | 2021-10-19 | 华南农业大学 | 一种蛋黄-蛋壳结构贵金属@空心碳纳米球复合材料及其制备方法和应用 |
| CN112387980A (zh) * | 2019-08-19 | 2021-02-23 | 近镒生技股份有限公司 | 纳米金粒子、包含其的药物载体、其制备方法及其用途 |
| CN115945204B (zh) * | 2022-04-01 | 2024-04-26 | 四川晨光博达新材料有限公司 | 一种多孔负载定型二氟化钴催化剂及其制备方法 |
| CN117102477A (zh) * | 2023-08-01 | 2023-11-24 | 淮安中顺环保科技有限公司 | 一种铜钯合金纳米颗粒及其制备方法和应用 |
| CN118417577B (zh) * | 2024-04-15 | 2025-03-04 | 重庆材料研究院有限公司 | 一种高均匀性微米级铂粉的制备方法 |
| CN119346119B (zh) * | 2024-12-24 | 2025-03-14 | 成都大学 | 一种具有核壳结构的气凝胶催化剂及其制备方法和应用 |
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| US8497131B2 (en) * | 1999-10-06 | 2013-07-30 | Becton, Dickinson And Company | Surface enhanced spectroscopy-active composite nanoparticles comprising Raman-active reporter molecules |
| KR100438408B1 (ko) * | 2001-08-16 | 2004-07-02 | 한국과학기술원 | 금속간의 치환 반응을 이용한 코어-쉘 구조 및 혼합된합금 구조의 금속 나노 입자의 제조 방법과 그 응용 |
| WO2004076056A2 (en) | 2003-02-26 | 2004-09-10 | Lake Shore Cryotronics Inc. | Microfluidic chemical reactor for the manufacture of chemically-produced nanoparticles |
| US8361553B2 (en) * | 2004-07-30 | 2013-01-29 | Kimberly-Clark Worldwide, Inc. | Methods and compositions for metal nanoparticle treated surfaces |
| JP4553356B2 (ja) * | 2004-10-29 | 2010-09-29 | キヤノン株式会社 | 顔料分散物の製造方法及び顔料分散物製造装置 |
| US20070116773A1 (en) * | 2005-07-05 | 2007-05-24 | Interuniversitair Microelektronica Centrum (Imec) | Metal nanostructures and pharmaceutical compositions |
| US7601668B2 (en) | 2006-09-29 | 2009-10-13 | Headwaters Technology Innovation, Llc | Methods for manufacturing bi-metallic catalysts having a controlled crystal face exposure |
| JP2008297614A (ja) * | 2007-06-01 | 2008-12-11 | Fuji Xerox Co Ltd | 金属粒子混合体の作製装置 |
| HU230862B1 (hu) | 2008-04-28 | 2018-10-29 | DARHOLDING Vagyonkezelő Kft | Berendezés és eljárás nanorészecskék folyamatos üzemű előállítására |
| WO2010108837A1 (en) * | 2009-03-24 | 2010-09-30 | Basf Se | Preparation of shaped metal particles and their uses |
| KR20110019603A (ko) | 2009-08-20 | 2011-02-28 | 한국지질자원연구원 | 슬러리환원법에 의해 염화은으로부터 나노 은 입자를 제조하는 방법 및 그 나노 은입자 |
| JP2011195852A (ja) * | 2010-03-17 | 2011-10-06 | Daihatsu Motor Co Ltd | ナノ粒子の製造方法 |
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| DK2785483T3 (en) | 2015-11-16 |
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