IE32415L - Preparation of 6-aminopenicillanic acid - Google Patents
Preparation of 6-aminopenicillanic acidInfo
- Publication number
- IE32415L IE32415L IE681213A IE121368A IE32415L IE 32415 L IE32415 L IE 32415L IE 681213 A IE681213 A IE 681213A IE 121368 A IE121368 A IE 121368A IE 32415 L IE32415 L IE 32415L
- Authority
- IE
- Ireland
- Prior art keywords
- aminopenicillanic acid
- preparation
- acid
- reacted
- alcohol
- Prior art date
Links
- NGHVIOIJCVXTGV-ALEPSDHESA-N 6-aminopenicillanic acid Chemical compound [O-]C(=O)[C@H]1C(C)(C)S[C@@H]2[C@H]([NH3+])C(=O)N21 NGHVIOIJCVXTGV-ALEPSDHESA-N 0.000 title abstract 3
- NGHVIOIJCVXTGV-UHFFFAOYSA-N 6beta-amino-penicillanic acid Natural products OC(=O)C1C(C)(C)SC2C(N)C(=O)N21 NGHVIOIJCVXTGV-UHFFFAOYSA-N 0.000 title abstract 3
- -1 silyl ester Chemical class 0.000 abstract 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- ODUCDPQEXGNKDN-UHFFFAOYSA-N nitroxyl Chemical compound O=N ODUCDPQEXGNKDN-UHFFFAOYSA-N 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D499/00—Heterocyclic compounds containing 4-thia-1-azabicyclo [3.2.0] heptane ring systems, i.e. compounds containing a ring system of the formula:, e.g. penicillins, penems; Such ring systems being further condensed, e.g. 2,3-condensed with an oxygen-, nitrogen- or sulfur-containing hetero ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Grinding Of Cylindrical And Plane Surfaces (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1,224,017. 6 - Aminopenicillanic acid. KONINKLIJKE NEDERLANDSCHE GISTEN SPIRITUSFABRIEK N.V. 19 Sept., 1968 [11 Oct., 1967], No. 44655/68. Addition to 1,189,022. Heading C2A. A process for the preparation of 6-aminopenicillanic acid or a salt thereof as claimed in claim 2 of Specification 1,189,022, in which the silyl ester of the 6-acylaminopenicillanic acid is reacted with a substance capable of forming an imino halide on the 6-amido nitrogen atom and in which the imino halide is reacted with an alcohol to form the imino ether at a temperature not exceeding - 20‹ C. Preferably the reaction with the alcohol is carried out at temperatures of - 40‹ to - 60‹ C.
[GB1224017A]
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL676713809A NL145861B (en) | 1967-10-11 | 1967-10-11 | IMPROVEMENT OF THE METHOD FOR THE CHEMICAL PREPARATION OF 6-AMINOPENICILLAN ACID OR SALTS THEREOF. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| IE32415L true IE32415L (en) | 1969-04-11 |
| IE32415B1 IE32415B1 (en) | 1973-07-25 |
Family
ID=19801429
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IE1213/68A IE32415B1 (en) | 1967-10-11 | 1968-10-10 | Process for the preparation of 6-aminopenicillanic acid |
Country Status (17)
| Country | Link |
|---|---|
| JP (1) | JPS516152B1 (en) |
| BE (1) | BE722052A (en) |
| BR (1) | BR6803037D0 (en) |
| CH (1) | CH546257A (en) |
| CS (1) | CS159750B2 (en) |
| DK (1) | DK130347B (en) |
| ES (1) | ES358992A2 (en) |
| FI (1) | FI50423C (en) |
| FR (1) | FR95946E (en) |
| GB (1) | GB1224017A (en) |
| IE (1) | IE32415B1 (en) |
| IL (1) | IL30758A0 (en) |
| IT (1) | IT1064102B (en) |
| NL (1) | NL145861B (en) |
| NO (1) | NO136097C (en) |
| SE (1) | SE356301B (en) |
| YU (1) | YU33005B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1388265A (en) * | 1971-03-12 | 1975-03-26 | Glaxo Lab Ltd | Preparation of antibiotic compounds |
| NL7908867A (en) * | 1979-12-10 | 1981-07-01 | Gist Brocades Nv | PROCESS FOR PREPARING 6-AMINOPENICILLANIC ACID -1-1-DIOXIDE AND ITS SALTS. |
| JPS5976997U (en) * | 1982-11-17 | 1984-05-24 | 中濃窯業株式会社 | Baking jig |
| JPS61145299U (en) * | 1985-02-28 | 1986-09-08 | ||
| JPS61159792U (en) * | 1985-03-22 | 1986-10-03 |
-
0
- FR FR169510A patent/FR95946E/en not_active Expired
-
1967
- 1967-10-11 NL NL676713809A patent/NL145861B/en unknown
-
1968
- 1968-09-19 GB GB44655/68A patent/GB1224017A/en not_active Expired
- 1968-09-20 SE SE12723/68A patent/SE356301B/xx unknown
- 1968-09-22 IL IL30758A patent/IL30758A0/en unknown
- 1968-09-30 NO NO3862/68A patent/NO136097C/en unknown
- 1968-10-04 YU YU2323/68A patent/YU33005B/en unknown
- 1968-10-08 FI FI682844A patent/FI50423C/en active
- 1968-10-09 ES ES358992A patent/ES358992A2/en not_active Expired
- 1968-10-09 BE BE722052D patent/BE722052A/xx unknown
- 1968-10-10 DK DK488368AA patent/DK130347B/en not_active IP Right Cessation
- 1968-10-10 IT IT40365/68A patent/IT1064102B/en active
- 1968-10-10 IE IE1213/68A patent/IE32415B1/en unknown
- 1968-10-11 CH CH1522768A patent/CH546257A/en not_active IP Right Cessation
- 1968-10-11 BR BR203037/68A patent/BR6803037D0/en unknown
- 1968-10-11 JP JP43073566A patent/JPS516152B1/ja active Pending
- 1968-10-11 CS CS7020A patent/CS159750B2/cs unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NO136097C (en) | 1977-07-20 |
| GB1224017A (en) | 1971-03-03 |
| BE722052A (en) | 1969-04-09 |
| FR95946E (en) | 1972-03-10 |
| ES358992A2 (en) | 1970-05-16 |
| DE1795436B2 (en) | 1975-06-26 |
| DK130347C (en) | 1975-07-07 |
| DE1795436A1 (en) | 1973-01-04 |
| YU232368A (en) | 1975-08-31 |
| FI50423B (en) | 1975-12-01 |
| DK130347B (en) | 1975-02-10 |
| BR6803037D0 (en) | 1973-02-22 |
| NL6713809A (en) | 1969-04-15 |
| IT1064102B (en) | 1985-02-18 |
| SE356301B (en) | 1973-05-21 |
| NO136097B (en) | 1977-04-12 |
| NL145861B (en) | 1975-05-15 |
| IL30758A0 (en) | 1968-11-27 |
| IE32415B1 (en) | 1973-07-25 |
| YU33005B (en) | 1976-03-31 |
| CS159750B2 (en) | 1975-01-31 |
| JPS516152B1 (en) | 1976-02-25 |
| FI50423C (en) | 1976-03-10 |
| CH546257A (en) | 1974-02-28 |
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