IE40274B1 - Resinous sulphonated polyisocyanates - Google Patents

Resinous sulphonated polyisocyanates

Info

Publication number: IE40274B1
Authority: IE; Ireland
Prior art keywords: sulphur trioxide; isocyanate; sulphonation; mixture; content
Prior art date: 1973-11-30

Application number

IE247074A

Other languages

English (en)

Other versions

IE40274L (en

Original Assignee

Bayer Ag

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1973-11-30

Filing date

1974-11-29

Publication date

1979-04-25

1974-11-29 Application filed by Bayer Ag filed Critical Bayer Ag

1975-05-30 Publication of IE40274L publication Critical patent/IE40274L/en

1979-04-25 Publication of IE40274B1 publication Critical patent/IE40274B1/en

Links

239000005056 polyisocyanate Substances 0.000 title claims description 20
229920001228 polyisocyanate Polymers 0.000 title claims description 20
AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims description 64
238000000034 method Methods 0.000 claims description 30
239000012948 isocyanate Substances 0.000 claims description 21
150000002513 isocyanates Chemical class 0.000 claims description 20
125000003118 aryl group Chemical group 0.000 claims description 11
BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical compound OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 claims description 11
239000003795 chemical substances by application Substances 0.000 claims description 10
239000000203 mixture Substances 0.000 claims description 10
239000007788 liquid Substances 0.000 claims description 9
239000007787 solid Substances 0.000 claims description 9
-1 aromatic isocyanate Chemical class 0.000 claims description 6
IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 claims description 5
125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 claims description 5
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 4
150000007514 bases Chemical class 0.000 claims description 3
238000004519 manufacturing process Methods 0.000 claims description 3
239000007789 gas Substances 0.000 claims description 2
239000012442 inert solvent Substances 0.000 claims description 2
229910052757 nitrogen Inorganic materials 0.000 claims description 2
239000011541 reaction mixture Substances 0.000 claims 3
239000000047 product Substances 0.000 description 32
229920005989 resin Polymers 0.000 description 18
239000011347 resin Substances 0.000 description 18
PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 16
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 14
239000005864 Sulphur Substances 0.000 description 14
238000006243 chemical reaction Methods 0.000 description 11
239000002253 acid Substances 0.000 description 10
238000004821 distillation Methods 0.000 description 9
238000006386 neutralization reaction Methods 0.000 description 9
150000007513 acids Chemical class 0.000 description 6
230000003472 neutralizing effect Effects 0.000 description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
239000002904 solvent Substances 0.000 description 5
239000000470 constituent Substances 0.000 description 4
238000001816 cooling Methods 0.000 description 4
JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 4
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 3
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 3
239000000945 filler Substances 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 3
239000000843 powder Substances 0.000 description 3
238000010298 pulverizing process Methods 0.000 description 3
150000003839 salts Chemical class 0.000 description 3
239000001117 sulphuric acid Substances 0.000 description 3
235000011149 sulphuric acid Nutrition 0.000 description 3
125000005628 tolylene group Chemical group 0.000 description 3
101150018711 AASS gene Proteins 0.000 description 2
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
229920002396 Polyurea Polymers 0.000 description 2
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
229910052799 carbon Inorganic materials 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
239000012262 resinous product Substances 0.000 description 2
239000007921 spray Substances 0.000 description 2
XTHPWXDJESJLNJ-UHFFFAOYSA-N sulfurochloridic acid Chemical compound OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 description 2
WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 1
241000237858 Gastropoda Species 0.000 description 1
241000272168 Laridae Species 0.000 description 1
MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
244000046052 Phaseolus vulgaris Species 0.000 description 1
241000220317 Rosa Species 0.000 description 1
CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical class [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
FMRLDPWIRHBCCC-UHFFFAOYSA-L Zinc carbonate Chemical compound [Zn+2].[O-]C([O-])=O FMRLDPWIRHBCCC-UHFFFAOYSA-L 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
150000008064 anhydrides Chemical group 0.000 description 1
JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 description 1
239000011230 binding agent Substances 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
238000000576 coating method Methods 0.000 description 1
238000007796 conventional method Methods 0.000 description 1
238000004132 cross linking Methods 0.000 description 1
238000006731 degradation reaction Methods 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
150000002500 ions Chemical class 0.000 description 1
235000014413 iron hydroxide Nutrition 0.000 description 1
NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 description 1
239000003595 mist Substances 0.000 description 1
239000004570 mortar (masonry) Substances 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
231100000252 nontoxic Toxicity 0.000 description 1
230000003000 nontoxic effect Effects 0.000 description 1
239000004814 polyurethane Substances 0.000 description 1
229920002635 polyurethane Polymers 0.000 description 1
239000002244 precipitate Substances 0.000 description 1
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
230000009257 reactivity Effects 0.000 description 1
230000000630 rising effect Effects 0.000 description 1
238000007086 side reaction Methods 0.000 description 1
239000012265 solid product Substances 0.000 description 1
238000003860 storage Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000004291 sulphur dioxide Substances 0.000 description 1
235000010269 sulphur dioxide Nutrition 0.000 description 1
229920003002 synthetic resin Polymers 0.000 description 1
239000000057 synthetic resin Substances 0.000 description 1
150000003512 tertiary amines Chemical class 0.000 description 1
239000002562 thickening agent Substances 0.000 description 1
238000004448 titration Methods 0.000 description 1
XSQUKJJJFZCRTK-UHFFFAOYSA-N urea group Chemical group NC(=O)N XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1
239000000080 wetting agent Substances 0.000 description 1
229910000010 zinc carbonate Inorganic materials 0.000 description 1
235000004416 zinc carbonate Nutrition 0.000 description 1
239000011667 zinc carbonate Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/775—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur sulfur

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Health & Medical Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Medicinal Chemistry (AREA)
Polymers & Plastics (AREA)
Polyurethanes Or Polyureas (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

IE247074A 1973-11-30 1974-11-29 Resinous sulphonated polyisocyanates IE40274B1 (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
DE19732359615 DE2359615A1 (de)	1973-11-30	1973-11-30	Harzartige sulfonierte polyisocyanate

Publications (2)

Publication Number	Publication Date
IE40274L IE40274L (en)	1975-05-30
IE40274B1 true IE40274B1 (en)	1979-04-25

Family

ID=5899468

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
IE247074A IE40274B1 (en)	1973-11-30	1974-11-29	Resinous sulphonated polyisocyanates

Country Status (9)

Country	Link
JP (1)	JPS5084548A (fr)
BE (1)	BE822701R (fr)
DE (1)	DE2359615A1 (fr)
DK (1)	DK619774A (fr)
FR (1)	FR2253040B2 (fr)
GB (1)	GB1454144A (fr)
IE (1)	IE40274B1 (fr)
LU (1)	LU71395A1 (fr)
NL (1)	NL7415631A (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE2615876C2 (de) *	1976-04-10	1986-05-15	Bayer Ag, 5090 Leverkusen	Aromatische Isocyanato-polysulfonsäuren und Verfahren zu deren Herstellung
DE2637114A1 (de) *	1976-08-18	1978-02-23	Bayer Ag	Verfahren zur herstellung von isocyanaten
DE2640103C2 (de) *	1976-09-07	1986-05-07	Bayer Ag, 5090 Leverkusen	Lagerstabile Gemische aus aromatischen Isocyanatosulfonsäuren und organischen Flüssigkeiten sowie Verfahren zu deren Herstellung
DE2801130A1 (de)	1978-01-12	1979-07-19	Bayer Ag	Modifizierte, sulfonsaeureestergruppen aufweisende polyisocyanate
DE2801129A1 (de)	1978-01-12	1979-07-19	Bayer Ag	Modifizierte, sulfonsaeureestergruppen aufweisende polyisocyanate
DE2851341A1 (de) *	1978-11-28	1980-06-04	Bayer Ag	Dispersionen aromatischer isocyanatosulfonsaeure-uretdione in organischen polyisocyanaten und ein verfahren zu ihrer herstellung

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JPS5111109A (ja) *	1974-07-18	1976-01-29	Tokyo Shibaura Electric Co	Jiseikusabi
JPS5250777A (en) *	1975-10-22	1977-04-23	Hitachi Ltd	Double beam photospectrometer

1973
- 1973-11-30 DE DE19732359615 patent/DE2359615A1/de active Pending
1974
- 1974-11-28 BE BE150943A patent/BE822701R/fr not_active IP Right Cessation
- 1974-11-28 LU LU71395A patent/LU71395A1/xx unknown
- 1974-11-29 FR FR7439140A patent/FR2253040B2/fr not_active Expired
- 1974-11-29 GB GB5178874A patent/GB1454144A/en not_active Expired
- 1974-11-29 NL NL7415631A patent/NL7415631A/xx not_active Application Discontinuation
- 1974-11-29 DK DK619774A patent/DK619774A/da unknown
- 1974-11-29 JP JP49136336A patent/JPS5084548A/ja active Pending
- 1974-11-29 IE IE247074A patent/IE40274B1/en unknown

Also Published As

Publication number	Publication date
GB1454144A (en)	1976-10-27
FR2253040B2 (fr)	1978-11-24
BE822701R (fr)	1975-05-28
JPS5084548A (fr)	1975-07-08
LU71395A1 (fr)	1975-08-20
FR2253040A2 (fr)	1975-06-27
DK619774A (fr)	1975-07-28
IE40274L (en)	1975-05-30
NL7415631A (nl)	1975-06-03
DE2359615A1 (de)	1975-06-05

Publication	Publication Date	Title
US3959329A (en)	1976-05-25	Polyisocyanates containing sulphonic acid or sulphonate groups
US5919859A (en)	1999-07-06	Aqueous resin dispersions
US4297456A (en)	1981-10-27	Process for working up isocyanate distillation residues
IE40274L (en)	1975-05-30	Resinous sulphonated polyisocyanates
EP0027943A1 (fr)	1981-05-06	Procédé pour le traitement de résidus réticulés contenant des groupements urée, provenant de la distillation d'isocyanates et utilisation des produits ainsi obtenus comme composés de départ dans la fabrication de matières plastiques
DE2452265C2 (de)	1984-05-24	Lagerstabile Preßmassen zur Herstellung von lichtstabilen, kriechstromfesten Kunststoffen
DE2000658A1 (de)	1971-07-15	Neue Polyaether-Verbindungen und Verfahren zur Herstellung dieser Polyaether
EP0066167B1 (fr)	1985-03-27	Procédé de préparation d'oligouréthanes contenant des groupes mercapto, leur utilisation comme liant pour des masses de revêtement ou de calfatage durcissables par oxydation ou comme additif pour des résines époxydes
US4144267A (en)	1979-03-13	Organic polyisocyanates
CA1218910A (fr)	1987-03-10	Composition faisant office d'agent de dispersion
EP0379749B1 (fr)	1994-06-22	Procédé pour la préparation des agents dispersants sulfonés
DE2227111C2 (de)	1984-07-26	Verfahren zur Herstellung von flüssigen, Sulfonsäure- und/oder Sulfonatgruppen aufweisenden, aromatischen Polyisocyanatgemischen und die danach hergestellten Gemische
DE2638986A1 (de)	1977-03-10	Rasch abbindende zusammensetzungen
US3849377A (en)	1974-11-19	Polyester containing sulphonic acid groups
US4401786A (en)	1983-08-30	Use of water soluble electrolytes as additives in aqueous dispersions of synthetic materials and an aqueous dispersion of synthetic materials containing a water soluble electrolyte
US1923392A (en)	1933-08-22	Olefin-polysulphide plastic
US3503930A (en)	1970-03-31	Mercaptan polymers
EP0113048B1 (fr)	1986-06-11	Procédé pour la préparation de polymères en poudre et leurs usages
DE69713338T2 (de)	2003-01-23	Zusammensetzung für die herstellung einer matten oder seidigen beschichtung, verwendung dieser zusammensetzung sowie daraus hergestellte beschichtung
US2683137A (en)	1954-07-06	Production of water-dispersible sulfonates of alkenyl aromatic resins
DE1720142A1 (de)	1971-08-12	Vulkanisierbare Zusammensetzung aus fluessigen Polymeren
EP0033458B1 (fr)	1983-04-27	Procédé de préparation de polyisocyanates modifiés et leur utilisation pour préparer des matières plastiques en polyuréthane
DE4306614A1 (de)	1994-09-08	Verfahren zur Wiederverwertung von Lackabfällen
JPS6021191B2 (ja)	1985-05-25	遊離イソシアネート基含有ポリウレタン組成物の貯蔵安定性増大のための添加剤としてモノイソシアネートを使用する方法
SU1065448A1 (ru)	1984-01-07	Способ получени полиэфирбитумной композиции дл полиуретана