IL117281A - Process for the preparation of 3-chloropropionic acid - Google Patents

Process for the preparation of 3-chloropropionic acid

Info

Publication number: IL117281A
Authority: IL; Israel
Prior art keywords: acid; acrylic acid; hydrochloric acid; gas; chloropropionic
Prior art date: 1995-03-03

Application number

IL11728196A

Other languages

English (en)

Hebrew (he)

Other versions

IL117281A0 (en

Inventor

Drivon Gilles

Ruppin Christophe

Original Assignee

Atochem Elf Sa

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1995-03-03

Filing date

1996-02-27

Publication date

1998-10-30

1996-02-27 Application filed by Atochem Elf Sa filed Critical Atochem Elf Sa

1996-06-18 Publication of IL117281A0 publication Critical patent/IL117281A0/xx

1998-10-30 Publication of IL117281A publication Critical patent/IL117281A/en

Links

QEYMMOKECZBKAC-UHFFFAOYSA-N 3-chloropropanoic acid Chemical compound OC(=O)CCCl QEYMMOKECZBKAC-UHFFFAOYSA-N 0.000 title claims abstract description 37
238000000034 method Methods 0.000 title claims description 29
238000002360 preparation method Methods 0.000 title claims description 7
NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 51
SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims abstract description 44
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 78
239000013049 sediment Substances 0.000 claims description 19
239000007864 aqueous solution Substances 0.000 claims description 8
239000000243 solution Substances 0.000 claims description 6
238000007038 hydrochlorination reaction Methods 0.000 claims description 4
239000012429 reaction media Substances 0.000 description 14
239000007789 gas Substances 0.000 description 12
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 7
229910000041 hydrogen chloride Inorganic materials 0.000 description 7
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
238000006243 chemical reaction Methods 0.000 description 6
QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 4
239000007788 liquid Substances 0.000 description 4
238000003756 stirring Methods 0.000 description 4
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
238000004519 manufacturing process Methods 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
238000004458 analytical method Methods 0.000 description 2
238000003556 assay Methods 0.000 description 2
230000005587 bubbling Effects 0.000 description 2
239000003153 chemical reaction reagent Substances 0.000 description 2
XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
238000004821 distillation Methods 0.000 description 2
239000011521 glass Substances 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
239000000825 pharmaceutical preparation Substances 0.000 description 2
229940127557 pharmaceutical product Drugs 0.000 description 2
239000000047 product Substances 0.000 description 2
150000003242 quaternary ammonium salts Chemical class 0.000 description 2
238000005481 NMR spectroscopy Methods 0.000 description 1
229910000831 Steel Inorganic materials 0.000 description 1
239000002253 acid Substances 0.000 description 1
239000000654 additive Substances 0.000 description 1
125000005907 alkyl ester group Chemical group 0.000 description 1
239000003139 biocide Substances 0.000 description 1
230000015572 biosynthetic process Effects 0.000 description 1
239000003086 colorant Substances 0.000 description 1
239000002537 cosmetic Substances 0.000 description 1
230000002089 crippling effect Effects 0.000 description 1
239000012043 crude product Substances 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
238000007872 degassing Methods 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
238000001035 drying Methods 0.000 description 1
238000004817 gas chromatography Methods 0.000 description 1
210000002816 gill Anatomy 0.000 description 1
239000012535 impurity Substances 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
150000004702 methyl esters Chemical class 0.000 description 1
239000000203 mixture Substances 0.000 description 1
239000004033 plastic Substances 0.000 description 1
229920003023 plastic Polymers 0.000 description 1
235000019260 propionic acid Nutrition 0.000 description 1
IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
238000000926 separation method Methods 0.000 description 1
239000010959 steel Substances 0.000 description 1
238000003786 synthesis reaction Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
- C07C51/363—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of halogen; by substitution of halogen atoms by other halogen atoms
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/62—Halogen-containing esters

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Engineering & Computer Science (AREA)
Oil, Petroleum & Natural Gas (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

IL11728196A 1995-03-03 1996-02-27 Process for the preparation of 3-chloropropionic acid IL117281A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FR9502484A FR2731218B1 (fr)	1995-03-03	1995-03-03	Procede de preparation de l'acide 3-chloropropionique

Publications (2)

Publication Number	Publication Date
IL117281A0 IL117281A0 (en)	1996-06-18
IL117281A true IL117281A (en)	1998-10-30

Family

ID=9476703

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
IL11728196A IL117281A (en)	1995-03-03	1996-02-27	Process for the preparation of 3-chloropropionic acid

Country Status (16)

Country	Link
US (1)	US5731469A (2)
EP (1)	EP0729935B1 (2)
JP (1)	JP2701229B2 (2)
KR (1)	KR100191484B1 (2)
CN (1)	CN1119311C (2)
AT (1)	ATE181051T1 (2)
BR (1)	BR9600849A (2)
CA (1)	CA2170846C (2)
DE (1)	DE69602780T2 (2)
FR (1)	FR2731218B1 (2)
IL (1)	IL117281A (2)
IN (1)	IN185461B (2)
MX (1)	MX9600831A (2)
NO (1)	NO304514B1 (2)
TW (1)	TW332199B (2)
ZA (1)	ZA961690B (2)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US7642395B2 (en) *	2004-12-28	2010-01-05	Kimberly-Clark Worldwide, Inc.	Composition and wipe for reducing viscosity of viscoelastic bodily fluids
US20120190879A1 (en) *	2011-01-24	2012-07-26	Michael Todd Coleman	Hydrochlorination of electron-deficient alkenes
CN107573231B (zh) *	2017-09-27	2021-01-29	荆楚理工学院	一种3-氯丙酸的生产方法
CN113292413A (zh) *	2021-06-08	2021-08-24	安徽星宇化工有限公司	一种3-氯丙酸的制备方法
CN116271904B (zh) *	2023-02-09	2025-08-19	淮安洪阳化工有限公司	一种3-氯丙酰氯合成方法及连续化反应装置

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2571901A (en) *	1945-12-12	1951-10-16	Niagara Alkali Company	Chlorinating process
DE1768536B1 (de) *	1968-05-24	1971-05-19	Basf Ag	Verfahren zur Herstellung von alpha-Chlorpropionsaeure

1995
- 1995-03-03 FR FR9502484A patent/FR2731218B1/fr not_active Expired - Fee Related
1996
- 1996-02-26 NO NO960773A patent/NO304514B1/no not_active IP Right Cessation
- 1996-02-27 IL IL11728196A patent/IL117281A/en not_active IP Right Cessation
- 1996-02-29 BR BR9600849A patent/BR9600849A/pt active Search and Examination
- 1996-03-01 DE DE69602780T patent/DE69602780T2/de not_active Expired - Fee Related
- 1996-03-01 AT AT96400442T patent/ATE181051T1/de not_active IP Right Cessation
- 1996-03-01 MX MX9600831A patent/MX9600831A/es unknown
- 1996-03-01 EP EP96400442A patent/EP0729935B1/fr not_active Expired - Lifetime
- 1996-03-01 CA CA002170846A patent/CA2170846C/fr not_active Expired - Fee Related
- 1996-03-01 ZA ZA961690A patent/ZA961690B/xx unknown
- 1996-03-01 IN IN321MA1996 patent/IN185461B/en unknown
- 1996-03-01 JP JP8071361A patent/JP2701229B2/ja not_active Expired - Fee Related
- 1996-03-02 CN CN96105538A patent/CN1119311C/zh not_active Expired - Fee Related
- 1996-03-02 KR KR1019960005479A patent/KR100191484B1/ko not_active Expired - Fee Related
- 1996-03-04 US US08/610,616 patent/US5731469A/en not_active Expired - Fee Related
- 1996-04-27 TW TW085102420A patent/TW332199B/zh active

Also Published As

Publication number	Publication date
BR9600849A (pt)	1997-12-30
KR100191484B1 (ko)	1999-06-15
CA2170846A1 (fr)	1996-09-04
NO960773D0 (no)	1996-02-26
MX9600831A (es)	1997-02-28
TW332199B (en)	1998-05-21
KR960034160A (ko)	1996-10-22
FR2731218B1 (fr)	1997-04-30
JP2701229B2 (ja)	1998-01-21
ATE181051T1 (de)	1999-06-15
EP0729935A1 (fr)	1996-09-04
DE69602780D1 (de)	1999-07-15
JPH08283194A (ja)	1996-10-29
CN1119311C (zh)	2003-08-27
US5731469A (en)	1998-03-24
NO304514B1 (no)	1999-01-04
FR2731218A1 (fr)	1996-09-06
ZA961690B (en)	1996-07-23
IL117281A0 (en)	1996-06-18
NO960773L (no)	1996-09-04
IN185461B (2)	2001-01-27
CA2170846C (fr)	1999-02-16
EP0729935B1 (fr)	1999-06-09
DE69602780T2 (de)	2000-03-09
CN1138569A (zh)	1996-12-25

Legal Events

Date	Code	Title
1999-03-12	FF	Patent granted
1999-09-22	KB	Patent renewed
2006-10-30	MM9K	Patent not in force due to non-payment of renewal fees

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