IL124258A - Process for purification of dimethyl sulphoxide (dmso) - Google Patents

Process for purification of dimethyl sulphoxide (dmso)

Info

Publication number: IL124258A
Authority: IL; Israel
Prior art keywords: dmso; purified; content; resin; process according
Prior art date: 1997-05-15

Application number

IL12425898A

Other languages

English (en)

Original Assignee

Elf Aquitaine Exploration Prod

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1997-05-15

Filing date

1998-04-28

Publication date

2002-07-25

1998-04-28 Application filed by Elf Aquitaine Exploration Prod filed Critical Elf Aquitaine Exploration Prod

2002-07-25 Publication of IL124258A publication Critical patent/IL124258A/en

Links

238000000034 method Methods 0.000 title claims abstract description 18
238000000746 purification Methods 0.000 title claims description 7
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 title abstract description 37
229960001760 dimethyl sulfoxide Drugs 0.000 title abstract description 36
239000011347 resin Substances 0.000 claims abstract description 18
229920005989 resin Polymers 0.000 claims abstract description 18
150000001768 cations Chemical class 0.000 claims abstract description 12
229910052751 metal Inorganic materials 0.000 claims abstract description 12
239000002184 metal Substances 0.000 claims abstract description 10
NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims abstract description 7
239000003513 alkali Substances 0.000 claims abstract description 6
239000007787 solid Substances 0.000 claims abstract description 6
239000003456 ion exchange resin Substances 0.000 claims abstract description 5
229920003303 ion-exchange polymer Polymers 0.000 claims abstract description 5
239000007788 liquid Substances 0.000 claims abstract description 4
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
MYRTYDVEIRVNKP-UHFFFAOYSA-N divinylbenzene Substances C=CC1=CC=CC=C1C=C MYRTYDVEIRVNKP-UHFFFAOYSA-N 0.000 claims description 9
229910052784 alkaline earth metal Inorganic materials 0.000 claims description 6
238000004458 analytical method Methods 0.000 claims description 6
150000001342 alkaline earth metals Chemical class 0.000 claims description 5
238000001636 atomic emission spectroscopy Methods 0.000 claims description 4
229920001577 copolymer Polymers 0.000 claims description 3
238000001514 detection method Methods 0.000 claims description 2
ATTZFSUZZUNHBP-UHFFFAOYSA-N Piperonyl sulfoxide Chemical compound CCCCCCCCS(=O)C(C)CC1=CC=C2OCOC2=C1 ATTZFSUZZUNHBP-UHFFFAOYSA-N 0.000 claims 1
125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims 1
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract description 5
JXLHNMVSKXFWAO-UHFFFAOYSA-N azane;7-fluoro-2,1,3-benzoxadiazole-4-sulfonic acid Chemical compound N.OS(=O)(=O)C1=CC=C(F)C2=NON=C12 JXLHNMVSKXFWAO-UHFFFAOYSA-N 0.000 abstract description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 16
239000011734 sodium Substances 0.000 description 9
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 7
229910052742 iron Inorganic materials 0.000 description 7
229910052708 sodium Inorganic materials 0.000 description 7
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 2
150000001450 anions Chemical class 0.000 description 2
239000003729 cation exchange resin Substances 0.000 description 2
238000011109 contamination Methods 0.000 description 2
239000008367 deionised water Substances 0.000 description 2
229910021641 deionized water Inorganic materials 0.000 description 2
239000012535 impurity Substances 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
150000002739 metals Chemical class 0.000 description 2
230000007935 neutral effect Effects 0.000 description 2
239000000243 solution Substances 0.000 description 2
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
241001550224 Apha Species 0.000 description 1
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
QMMFVYPAHWMCMS-UHFFFAOYSA-N Dimethyl sulfide Chemical compound CSC QMMFVYPAHWMCMS-UHFFFAOYSA-N 0.000 description 1
229910017974 NH40H Inorganic materials 0.000 description 1
239000004793 Polystyrene Substances 0.000 description 1
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
-1 ammonium anions Chemical class 0.000 description 1
238000005349 anion exchange Methods 0.000 description 1
239000012736 aqueous medium Substances 0.000 description 1
239000007864 aqueous solution Substances 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
239000011575 calcium Substances 0.000 description 1
238000005341 cation exchange Methods 0.000 description 1
238000004587 chromatography analysis Methods 0.000 description 1
229910052804 chromium Inorganic materials 0.000 description 1
239000011651 chromium Substances 0.000 description 1
239000000356 contaminant Substances 0.000 description 1
229910052802 copper Inorganic materials 0.000 description 1
239000010949 copper Substances 0.000 description 1
238000004132 cross linking Methods 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
239000000428 dust Substances 0.000 description 1
230000000694 effects Effects 0.000 description 1
238000001704 evaporation Methods 0.000 description 1
230000008020 evaporation Effects 0.000 description 1
238000001914 filtration Methods 0.000 description 1
238000004508 fractional distillation Methods 0.000 description 1
238000005342 ion exchange Methods 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000002609 medium Substances 0.000 description 1
230000008018 melting Effects 0.000 description 1
238000002844 melting Methods 0.000 description 1
239000000203 mixture Substances 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
238000005325 percolation Methods 0.000 description 1
229920002223 polystyrene Polymers 0.000 description 1
229920003053 polystyrene-divinylbenzene Polymers 0.000 description 1
239000011148 porous material Substances 0.000 description 1
229910052700 potassium Inorganic materials 0.000 description 1
239000011591 potassium Substances 0.000 description 1
238000004313 potentiometry Methods 0.000 description 1
238000002360 preparation method Methods 0.000 description 1
239000000700 radioactive tracer Substances 0.000 description 1
230000000717 retained effect Effects 0.000 description 1
229910001220 stainless steel Inorganic materials 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
239000000126 substance Substances 0.000 description 1
235000011149 sulphuric acid Nutrition 0.000 description 1
239000001117 sulphuric acid Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
230000000007 visual effect Effects 0.000 description 1
239000011701 zinc Substances 0.000 description 1
229910052725 zinc Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C315/00—Preparation of sulfones; Preparation of sulfoxides
- C07C315/06—Separation; Purification; Stabilisation; Use of additives

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Treatment Of Water By Ion Exchange (AREA)
Treatment Of Liquids With Adsorbents In General (AREA)
Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
Treating Waste Gases (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)
Catalysts (AREA)
Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)

IL12425898A 1997-05-15 1998-04-28 Process for purification of dimethyl sulphoxide (dmso) IL124258A (en)

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
FR9705965A FR2763332B1 (fr)	1997-05-15	1997-05-15	Procede de purification de dimethylsulfoxyde (dmso)

Publications (1)

Publication Number	Publication Date
IL124258A true IL124258A (en)	2002-07-25

Family

ID=9506917

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
IL12425898A IL124258A (en)	1997-05-15	1998-04-28	Process for purification of dimethyl sulphoxide (dmso)

Country Status (16)

Country	Link
US (1)	US6020530A (de)
EP (1)	EP0882708B1 (de)
JP (1)	JPH10330348A (de)
KR (1)	KR100560359B1 (de)
CN (1)	CN1084731C (de)
AT (1)	ATE204565T1 (de)
CA (1)	CA2235770A1 (de)
DE (2)	DE69801395T2 (de)
ES (1)	ES2162696T3 (de)
FR (1)	FR2763332B1 (de)
GB (1)	GB2325228B (de)
IL (1)	IL124258A (de)
MY (1)	MY114591A (de)
PL (1)	PL326289A1 (de)
SG (1)	SG63848A1 (de)
TW (1)	TW455577B (de)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
FR2763333B1 (fr) *	1997-05-15	1999-06-25	Elf Aquitaine	Procede de purification de dimethylsulfoxyde (dmso)
JP3958888B2 (ja) *	1999-03-31	2007-08-15	株式会社神鋼環境ソリューション	ジメチルスルホキシド含有廃水の処理方法
WO2014175187A1 (ja) *	2013-04-24	2014-10-30	東レ・ファインケミカル株式会社	ジメチルスルホキシドの精製方法
FR3021551A1 (fr)	2014-06-03	2015-12-04	Arkema France	Procede d'elimination d'ions metalliques dans une solution organique visqueuse
TWI725162B (zh)	2016-04-08	2021-04-21	日商富士軟片股份有限公司	處理液、其製造方法、圖案形成方法及電子器件的製造方法
ES3056187T3 (en) *	2017-04-12	2026-02-18	Toray Finechemicals Co Ltd	Method for distilling dimethylsulfoxide and multistage distillation column
CN112649489A (zh) *	2020-09-27	2021-04-13	浙江迪谱诊断技术有限公司	一种核酸质谱离子净化方法
CN115784952B (zh) *	2022-10-09	2024-07-05	新疆兴发化工有限公司	一种电子级二甲基亚砜的提纯工艺

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1768779A1 (de) *	1968-06-28	1972-01-13	Glanzstoff Ag	Verfahren zur Gewinnung von reinem Dimethylsulfoxyd

1997
- 1997-05-15 FR FR9705965A patent/FR2763332B1/fr not_active Expired - Fee Related
1998
- 1998-04-28 EP EP98401030A patent/EP0882708B1/de not_active Expired - Lifetime
- 1998-04-28 DE DE69801395T patent/DE69801395T2/de not_active Expired - Fee Related
- 1998-04-28 IL IL12425898A patent/IL124258A/en not_active IP Right Cessation
- 1998-04-28 AT AT98401030T patent/ATE204565T1/de not_active IP Right Cessation
- 1998-04-28 ES ES98401030T patent/ES2162696T3/es not_active Expired - Lifetime
- 1998-05-13 DE DE19821326A patent/DE19821326A1/de not_active Withdrawn
- 1998-05-13 SG SG1998001044A patent/SG63848A1/en unknown
- 1998-05-14 CA CA002235770A patent/CA2235770A1/fr not_active Abandoned
- 1998-05-14 PL PL98326289A patent/PL326289A1/xx unknown
- 1998-05-14 US US09/078,479 patent/US6020530A/en not_active Expired - Fee Related
- 1998-05-14 KR KR1019980017398A patent/KR100560359B1/ko not_active Expired - Fee Related
- 1998-05-14 MY MYPI98002144A patent/MY114591A/en unknown
- 1998-05-15 GB GB9810503A patent/GB2325228B/en not_active Expired - Fee Related
- 1998-05-15 JP JP10133499A patent/JPH10330348A/ja not_active Ceased
- 1998-05-15 CN CN98102500.5A patent/CN1084731C/zh not_active Expired - Fee Related
- 1998-05-15 TW TW087107538A patent/TW455577B/zh active

Also Published As

Publication number	Publication date
CN1084731C (zh)	2002-05-15
FR2763332B1 (fr)	1999-06-25
FR2763332A1 (fr)	1998-11-20
DE19821326A1 (de)	1998-11-19
SG63848A1 (en)	1999-03-30
US6020530A (en)	2000-02-01
EP0882708B1 (de)	2001-08-22
GB9810503D0 (en)	1998-07-15
KR100560359B1 (ko)	2006-05-25
TW455577B (en)	2001-09-21
EP0882708A1 (de)	1998-12-09
DE69801395D1 (de)	2001-09-27
CA2235770A1 (fr)	1998-11-15
ES2162696T3 (es)	2002-01-01
KR19980087051A (ko)	1998-12-05
DE69801395T2 (de)	2002-05-23
ATE204565T1 (de)	2001-09-15
MY114591A (en)	2002-11-30
GB2325228B (en)	2000-11-29
PL326289A1 (en)	1998-11-23
JPH10330348A (ja)	1998-12-15
GB2325228A (en)	1998-11-18
CN1201030A (zh)	1998-12-09

Legal Events

Date	Code	Title
2003-01-12	FF	Patent granted
2003-02-12	KB	Patent renewed
2004-06-01	KB	Patent renewed
2009-07-20	MM9K	Patent not in force due to non-payment of renewal fees

Publication	Publication Date	Title
US6123850A (en)	2000-09-26	Process for the purification of virtually anhydrous organic liquids
IL124258A (en)	2002-07-25	Process for purification of dimethyl sulphoxide (dmso)
KR100284349B1 (ko)	2001-04-02	디메틸술폭시드(dmso)의정제방법
US6235198B1 (en)	2001-05-22	Process for purification of dimethyl sulphoxide (DMSO)
Shimomura et al.	1967	Separation of amines by ligand exchange: Part IV ligand exchange with chelating resins and cellulosic exchangers
Rudling	1971	Determination of nitrilotriacetic acid
EP0183083A1 (de)	1986-06-04	Verfahren zur Herstellung von (2,2)-Paracyclophan
Lau et al.	1982	The determination of selenium by atom-trapping atomic absorption spectrometry
Ikeda et al.	1983	Preparation and characterization of unsymmetrical bis (benzocrown ether) s: Preferential complexation with rubidium cation
MXPA98003782A (es)	1999-09-20	Procedimiento de purificación de dimetilsulfoxido (dmso)
Chadwick	1974	Gravimetric determination of gold and platinum using 2, 4, 6-triphenylpyrylium chloride
CA1119416A (en)	1982-03-09	Process for nickel removal from concentrated aqueous cobaltous sulfate solutions
Bulska et al.	1996	The application of solid sorbents for the purification of aluminum contaminated chemicals used as modifiers in electrothermal atomic absorption spectrometry
SU616312A1 (ru)	1978-07-25	Способ сорбционного извлечени цветных металлов из аммиачно-карбонатных растворов
Suvardhan et al.	2007	Novel solid-phase extraction and preconcentration technique coupled with ICP-AES for the determination of Cr (III), Ni (II), and Zn (II) in various water samples
Hamilton	1991	The synthesis of cobalt (III) sepulcrate from tris (ethylenediamine) cobalt (III) and its purification by ion-exchange chromatography: An experiment for the advanced undergraduate inorganic laboratory
RU2063457C1 (ru)	1996-07-10	Способ очистки концентрированных растворов молибдатов от вольфрама
Varshney et al.	1983	Quantitative determination of iron and aluminium in some alloys and silicate rocks after a cation exchange separation on zirconium (IV) phospho and silico arsenates
Manjarekar et al.	1995	Cation exchange chromatographic separation of zinc in mixed solvents and non-aqueous hydrobromic acid media
Strelow et al.	1992	Improved separation of ruthenium from base metals by cation exchange chromatography in hydrochloric acid
JPS5850790B2 (ja)	1983-11-12	ピロリンサンエンオキヨウゾンシタドウイオンガンユウハイスイノシヨリホウ