JP3133708B2 - カプサイシンの工業的精製方法 - Google Patents

カプサイシンの工業的精製方法

Info

Publication number
JP3133708B2
JP3133708B2 JP09193760A JP19376097A JP3133708B2 JP 3133708 B2 JP3133708 B2 JP 3133708B2 JP 09193760 A JP09193760 A JP 09193760A JP 19376097 A JP19376097 A JP 19376097A JP 3133708 B2 JP3133708 B2 JP 3133708B2
Authority
JP
Japan
Prior art keywords
capsaicin
aqueous solution
silver
dissolved
purity
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP09193760A
Other languages
English (en)
Japanese (ja)
Other versions
JPH1135538A (ja
Inventor
幾 瀬木
修嗣 山田
悟史 加藤
正治 村杉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Alps Pharmaceutical Ind Co Ltd
Original Assignee
Alps Pharmaceutical Ind Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Alps Pharmaceutical Ind Co Ltd filed Critical Alps Pharmaceutical Ind Co Ltd
Priority to JP09193760A priority Critical patent/JP3133708B2/ja
Priority to DE69813397T priority patent/DE69813397T2/de
Priority to EP98113227A priority patent/EP0891966B1/fr
Priority to US09/116,453 priority patent/US5955631A/en
Publication of JPH1135538A publication Critical patent/JPH1135538A/ja
Application granted granted Critical
Publication of JP3133708B2 publication Critical patent/JP3133708B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00—Preparation of carboxylic acid amides
    • C07C231/22—Separation; Purification; Stabilisation; Use of additives
    • C07C231/24—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP09193760A 1997-07-18 1997-07-18 カプサイシンの工業的精製方法 Expired - Fee Related JP3133708B2 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP09193760A JP3133708B2 (ja) 1997-07-18 1997-07-18 カプサイシンの工業的精製方法
DE69813397T DE69813397T2 (de) 1997-07-18 1998-07-16 Verfahren zum industriellen Reinigen von Capsaicin
EP98113227A EP0891966B1 (fr) 1997-07-18 1998-07-16 Procédé pour la purification industrielle de la capsaicine
US09/116,453 US5955631A (en) 1997-07-18 1998-07-16 Method for industrial purification of capsaicin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP09193760A JP3133708B2 (ja) 1997-07-18 1997-07-18 カプサイシンの工業的精製方法

Publications (2)

Publication Number Publication Date
JPH1135538A JPH1135538A (ja) 1999-02-09
JP3133708B2 true JP3133708B2 (ja) 2001-02-13

Family

ID=16313360

Family Applications (1)

Application Number Title Priority Date Filing Date
JP09193760A Expired - Fee Related JP3133708B2 (ja) 1997-07-18 1997-07-18 カプサイシンの工業的精製方法

Country Status (4)

Country Link
US (1) US5955631A (fr)
EP (1) EP0891966B1 (fr)
JP (1) JP3133708B2 (fr)
DE (1) DE69813397T2 (fr)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4637377B2 (ja) * 2001-02-01 2011-02-23 長谷川香料株式会社 トウガラシからのカプサイシノイド様物質の抽出方法
US20030012828A1 (en) * 2001-07-13 2003-01-16 Joe Ajrulahi Topical medicine and process and apparatus for making same
CN1293043C (zh) * 2002-08-20 2007-01-03 中国科学院广州地球化学研究所 以辣椒素为原料制造高纯度辣椒碱的方法
US20050085652A1 (en) * 2003-04-08 2005-04-21 Algorx Pharmaceuticals, Inc. Preparation and purification of synthetic capsaicin
CN100406432C (zh) * 2005-01-18 2008-07-30 天津科技大学 从辣椒中提取辣椒碱晶体的方法
EA013056B1 (ru) * 2005-04-01 2010-02-26 Ньюроджесэкс, Инк. Масла капсаициноидов и способы их получения и применения
JP4981375B2 (ja) * 2006-07-12 2012-07-18 秀樹 山本 唐辛子からカプシノイド化合物を抽出分離する方法及び唐辛子抽出物
CN100348574C (zh) * 2006-09-08 2007-11-14 山东省科学院生物研究所 一种单体辣椒碱的纯化制备方法
CN101200433B (zh) * 2007-11-08 2010-04-07 山东省分析测试中心 高纯度辣椒碱单体的制备方法
CN101619028B (zh) * 2009-06-17 2012-06-27 张鹏 一种制备辣椒碱单体的方法
CN102432489B (zh) * 2011-11-29 2014-02-26 山东轻工业学院 一种制备辣椒碱和二氢辣椒碱单体的方法
CN103739511A (zh) * 2013-12-20 2014-04-23 白城艾高食品有限公司 一种萃取辣椒碱的方法
CN106946730B (zh) * 2017-03-27 2019-02-22 北京理工大学 一种从催泪喷射剂及其废液中回收刺激成分oc的方法
CN109180517B (zh) * 2018-10-11 2021-10-26 许昌学院 一种制备高纯白色固态辣椒碱的方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Ｃｈｅｍｉｃａｌ Ａｂｓｔｒａｃｔｓ，Ｎｏ．９３：６８７６５（１９８０）

Also Published As

Publication number Publication date
DE69813397D1 (de) 2003-05-22
JPH1135538A (ja) 1999-02-09
EP0891966A2 (fr) 1999-01-20
US5955631A (en) 1999-09-21
DE69813397T2 (de) 2004-03-04
EP0891966B1 (fr) 2003-04-16
EP0891966A3 (fr) 2000-04-12

Similar Documents

Publication Publication Date Title
JP3133708B2 (ja) カプサイシンの工業的精製方法
US20070293703A1 (en) Preparation and purification of synthetic capsaicin
CA2317951A1 (fr) Nouveaux amides aromatiques, leur procede de preparation et leur application comme medicaments
JPS60358B2 (ja) ベンゾモルフアン化合物の製法
DE69229339T2 (de) Kristallines tiagabinehydrochlorid-monohydrat, seine herstellung und verwendung
JPH0310630B2 (fr)
JPS6150985A (ja) 新規なカンプトテシン誘導体
CN110078686A (zh) 10-去乙酰基巴卡亭ⅲ合成卡巴他赛的方法
WO2000063222A2 (fr) Nouveaux amides aromatiques substitues par un ribose, leur procede de preparation et leur application comme medicaments
JPH04266880A (ja) ３　−ｄｐａ−　ラクトンの製造方法
JP2524803B2 (ja) 新規なカンプトテシン誘導体およびその製造法
CN115611855B (zh) 烟碱酰胺型化合物及其在制备减肥药物中的应用
KR101119625B1 (ko) 베툴론산의 고순도 정제방법, 고순도 베툴론산을 이용한 피페라진 베툴론산 아마이드 유도체의 제조방법과 그 유도체, 고순도 베툴론산을 이용한 고순도 비오씨-라이시네이티드 베툴론산 정제방법
CN110698398B (zh) 一种米库氯铵的纯化方法
CH387022A (fr) Procédé de préparation de 6-désoxy-tétracyclines
DE69615562T2 (de) Verfahren zu extrahieren und isolierung von 10-desacetylbachatin iii
EP2848251B1 (fr) Extraits et composés isolés à partir de Cakile arabica pour le traitements des ulcers
JP2002234896A (ja) シアタン誘導体
JP4334194B2 (ja) エクチナサイジン７８６およびその取得方法
CN102659639A (zh) 一种益母草碱的制备工艺
CN109517026B (zh) L-苯丙氨酸修饰的山楂酸及其合成方法和应用
CN103974926B (zh) 分离巨大戟醇的方法
JP2009533432A (ja) ナルコチンの精製方法
CN113698369A (zh) 一种除去卡巴他赛中特定单杂的方法
CN117209390A (zh) 一种制备金刚烷类化合物的方法

Legal Events

Date Code Title Description
LAPS Cancellation because of no payment of annual fees