JP3980647B2 - 無機、有機および有機金属パラジウム水素スカベンジャー - Google Patents

無機、有機および有機金属パラジウム水素スカベンジャー Download PDF

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Publication number: JP3980647B2
Authority: JP; Japan
Prior art keywords: palladium; impression; compound; positive; composition
Prior art date: 1996-04-09
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

JP53614897A

Other languages

English (en)

Japanese (ja)

Other versions

JP2000509026A (ja

JP2000509026A5 (2

Inventor

エス．コニングス，マーク

ディー．オクスマン，ジョエル

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

3M Co

Original Assignee

3M Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1996-04-09

Filing date

1996-08-07

Publication date

2007-09-26

1996-08-07 Application filed by 3M Co filed Critical 3M Co

2000-07-18 Publication of JP2000509026A publication Critical patent/JP2000509026A/ja

2004-09-02 Publication of JP2000509026A5 publication Critical patent/JP2000509026A5/ja

2007-09-26 Application granted granted Critical

2007-09-26 Publication of JP3980647B2 publication Critical patent/JP3980647B2/ja

2016-08-07 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

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KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 title claims description 104
229910052763 palladium Inorganic materials 0.000 title claims description 56
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims description 46
239000001257 hydrogen Substances 0.000 title claims description 24
229910052739 hydrogen Inorganic materials 0.000 title claims description 24
125000002524 organometallic group Chemical group 0.000 title description 2
239000000203 mixture Substances 0.000 claims description 72
239000000463 material Substances 0.000 claims description 60
BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 52
150000001875 compounds Chemical class 0.000 claims description 39
239000003054 catalyst Substances 0.000 claims description 38
229910052697 platinum Inorganic materials 0.000 claims description 28
238000006243 chemical reaction Methods 0.000 claims description 15
239000003431 cross linking reagent Substances 0.000 claims description 10
125000001931 aliphatic group Chemical group 0.000 claims description 9
150000002484 inorganic compounds Chemical class 0.000 claims description 5
150000002894 organic compounds Chemical class 0.000 claims description 5
150000002902 organometallic compounds Chemical class 0.000 claims description 5
238000004519 manufacturing process Methods 0.000 claims description 4
229910010272 inorganic material Inorganic materials 0.000 claims 2
150000002941 palladium compounds Chemical class 0.000 description 48
229920001296 polysiloxane Polymers 0.000 description 41
-1 organometallic palladium compounds Chemical class 0.000 description 40
229920000642 polymer Polymers 0.000 description 26
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 20
125000000524 functional group Chemical group 0.000 description 17
239000004971 Cross linker Substances 0.000 description 13
125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 13
229910052602 gypsum Inorganic materials 0.000 description 12
239000010440 gypsum Substances 0.000 description 12
229910052751 metal Inorganic materials 0.000 description 12
239000002184 metal Substances 0.000 description 12
238000000034 method Methods 0.000 description 11
238000004132 cross linking Methods 0.000 description 10
239000000243 solution Substances 0.000 description 10
239000000126 substance Substances 0.000 description 10
229920002554 vinyl polymer Polymers 0.000 description 10
125000004432 carbon atom Chemical group C* 0.000 description 9
KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 9
239000007789 gas Substances 0.000 description 9
238000002156 mixing Methods 0.000 description 9
230000003068 static effect Effects 0.000 description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
229910052736 halogen Inorganic materials 0.000 description 8
125000001183 hydrocarbyl group Chemical group 0.000 description 8
238000006459 hydrosilylation reaction Methods 0.000 description 8
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
150000001336 alkenes Chemical class 0.000 description 7
239000003795 chemical substances by application Substances 0.000 description 7
150000002367 halogens Chemical class 0.000 description 7
238000002347 injection Methods 0.000 description 7
239000007924 injection Substances 0.000 description 7
239000011505 plaster Substances 0.000 description 7
239000000725 suspension Substances 0.000 description 7
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
239000000945 filler Substances 0.000 description 6
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 5
239000000654 additive Substances 0.000 description 5
125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 5
238000009472 formulation Methods 0.000 description 5
239000003112 inhibitor Substances 0.000 description 5
229920006136 organohydrogenpolysiloxane Polymers 0.000 description 5
MUJIDPITZJWBSW-UHFFFAOYSA-N palladium(2+) Chemical compound [Pd+2] MUJIDPITZJWBSW-UHFFFAOYSA-N 0.000 description 5
PIBWKRNGBLPSSY-UHFFFAOYSA-L palladium(II) chloride Chemical compound Cl[Pd]Cl PIBWKRNGBLPSSY-UHFFFAOYSA-L 0.000 description 5
125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 5
239000000843 powder Substances 0.000 description 5
229920005989 resin Polymers 0.000 description 5
239000011347 resin Substances 0.000 description 5
239000000758 substrate Substances 0.000 description 5
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
229910002666 PdCl2 Inorganic materials 0.000 description 4
YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 4
239000002253 acid Substances 0.000 description 4
125000004429 atom Chemical group 0.000 description 4
239000002978 dental impression material Substances 0.000 description 4
230000000694 effects Effects 0.000 description 4
125000004435 hydrogen atom Chemical group [H]* 0.000 description 4
238000000465 moulding Methods 0.000 description 4
229910052757 nitrogen Inorganic materials 0.000 description 4
238000005070 sampling Methods 0.000 description 4
229910052710 silicon Inorganic materials 0.000 description 4
239000010703 silicon Substances 0.000 description 4
239000002002 slurry Substances 0.000 description 4
IBXMKLPFLZYRQZ-UHFFFAOYSA-N 1,5-diphenylpenta-1,4-dien-3-one;palladium Chemical class [Pd].[Pd].C=1C=CC=CC=1C=CC(=O)C=CC1=CC=CC=C1 IBXMKLPFLZYRQZ-UHFFFAOYSA-N 0.000 description 3
SNRUBQQJIBEYMU-UHFFFAOYSA-N Dodecane Natural products CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 3
229910019032 PtCl2 Inorganic materials 0.000 description 3
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
230000000996 additive effect Effects 0.000 description 3
239000000853 adhesive Substances 0.000 description 3
230000001070 adhesive effect Effects 0.000 description 3
125000003342 alkenyl group Chemical group 0.000 description 3
125000000217 alkyl group Chemical group 0.000 description 3
229910045601 alloy Inorganic materials 0.000 description 3
239000000956 alloy Substances 0.000 description 3
125000003710 aryl alkyl group Chemical group 0.000 description 3
125000003118 aryl group Chemical group 0.000 description 3
239000000470 constituent Substances 0.000 description 3
125000000392 cycloalkenyl group Chemical group 0.000 description 3
125000000753 cycloalkyl group Chemical group 0.000 description 3
125000000596 cyclohexenyl group Chemical group C1(=CCCCC1)* 0.000 description 3
125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 3
125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 3
INIOZDBICVTGEO-UHFFFAOYSA-L palladium(ii) bromide Chemical compound Br[Pd]Br INIOZDBICVTGEO-UHFFFAOYSA-L 0.000 description 3
239000002245 particle Substances 0.000 description 3
230000000704 physical effect Effects 0.000 description 3
125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
229920005573 silicon-containing polymer Polymers 0.000 description 3
238000012360 testing method Methods 0.000 description 3
RRHPTXZOMDSKRS-PHFPKPIQSA-L (1z,5z)-cycloocta-1,5-diene;dichloropalladium Chemical compound Cl[Pd]Cl.C\1C\C=C/CC\C=C/1 RRHPTXZOMDSKRS-PHFPKPIQSA-L 0.000 description 2
239000004912 1,5-cyclooctadiene Substances 0.000 description 2
125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 2
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 2
QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical class C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
229910021605 Palladium(II) bromide Inorganic materials 0.000 description 2
XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 2
229910020388 SiO1/2 Inorganic materials 0.000 description 2
229910020485 SiO4/2 Inorganic materials 0.000 description 2
UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 2
238000010521 absorption reaction Methods 0.000 description 2
RBYGDVHOECIAFC-UHFFFAOYSA-L acetonitrile;palladium(2+);dichloride Chemical compound [Cl-].[Cl-].[Pd+2].CC#N.CC#N RBYGDVHOECIAFC-UHFFFAOYSA-L 0.000 description 2
125000002877 alkyl aryl group Chemical group 0.000 description 2
150000001412 amines Chemical class 0.000 description 2
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 2
125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
229940057746 calcet Drugs 0.000 description 2
229910000019 calcium carbonate Inorganic materials 0.000 description 2
229910052799 carbon Inorganic materials 0.000 description 2
125000004218 chloromethyl group Chemical group [H]C([H])(Cl)* 0.000 description 2
125000000068 chlorophenyl group Chemical group 0.000 description 2
230000015271 coagulation Effects 0.000 description 2
238000005345 coagulation Methods 0.000 description 2
238000000576 coating method Methods 0.000 description 2
229920001577 copolymer Polymers 0.000 description 2
125000001162 cycloheptenyl group Chemical group C1(=CCCCCC1)* 0.000 description 2
125000000582 cycloheptyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 2
125000000522 cyclooctenyl group Chemical group C1(=CCCCCCC1)* 0.000 description 2
125000002433 cyclopentenyl group Chemical group C1(=CCCC1)* 0.000 description 2
239000004205 dimethyl polysiloxane Substances 0.000 description 2
239000006185 dispersion Substances 0.000 description 2
229920001971 elastomer Polymers 0.000 description 2
BITPLIXHRASDQB-UHFFFAOYSA-N ethenyl-[ethenyl(dimethyl)silyl]oxy-dimethylsilane Chemical compound C=C[Si](C)(C)O[Si](C)(C)C=C BITPLIXHRASDQB-UHFFFAOYSA-N 0.000 description 2
238000001125 extrusion Methods 0.000 description 2
238000011049 filling Methods 0.000 description 2
229940093915 gynecological organic acid Drugs 0.000 description 2
125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 2
125000004356 hydroxy functional group Chemical group O* 0.000 description 2
238000005805 hydroxylation reaction Methods 0.000 description 2
238000001802 infusion Methods 0.000 description 2
125000001624 naphthyl group Chemical group 0.000 description 2
229910017464 nitrogen compound Inorganic materials 0.000 description 2
150000002830 nitrogen compounds Chemical class 0.000 description 2
125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
150000007524 organic acids Chemical class 0.000 description 2
235000005985 organic acids Nutrition 0.000 description 2
125000004430 oxygen atom Chemical group O* 0.000 description 2
YJVFFLUZDVXJQI-UHFFFAOYSA-L palladium(ii) acetate Chemical compound [Pd+2].CC([O-])=O.CC([O-])=O YJVFFLUZDVXJQI-UHFFFAOYSA-L 0.000 description 2
150000003058 platinum compounds Chemical class 0.000 description 2
229920000435 poly(dimethylsiloxane) Polymers 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
230000002000 scavenging effect Effects 0.000 description 2
150000004756 silanes Chemical class 0.000 description 2
229920002379 silicone rubber Polymers 0.000 description 2
239000011734 sodium Substances 0.000 description 2
239000002904 solvent Substances 0.000 description 2
239000003381 stabilizer Substances 0.000 description 2
239000010935 stainless steel Substances 0.000 description 2
229910001220 stainless steel Inorganic materials 0.000 description 2
125000004079 stearyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 2
RIOQSEWOXXDEQQ-UHFFFAOYSA-N triphenylphosphine Chemical compound C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 RIOQSEWOXXDEQQ-UHFFFAOYSA-N 0.000 description 2
125000005023 xylyl group Chemical group 0.000 description 2
RRKODOZNUZCUBN-CCAGOZQPSA-N (1z,3z)-cycloocta-1,3-diene Chemical compound C1CC\C=C/C=C\C1 RRKODOZNUZCUBN-CCAGOZQPSA-N 0.000 description 1
KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 1
PHQVPLFRGMMSCP-UHFFFAOYSA-N 1-chlorocycloocta-1,5-diene Chemical compound ClC1=CCCC=CCC1 PHQVPLFRGMMSCP-UHFFFAOYSA-N 0.000 description 1
VMAWODUEPLAHOE-UHFFFAOYSA-N 2,4,6,8-tetrakis(ethenyl)-2,4,6,8-tetramethyl-1,3,5,7,2,4,6,8-tetraoxatetrasilocane Chemical group C=C[Si]1(C)O[Si](C)(C=C)O[Si](C)(C=C)O[Si](C)(C=C)O1 VMAWODUEPLAHOE-UHFFFAOYSA-N 0.000 description 1
BVTLTBONLZSBJC-UHFFFAOYSA-N 2,4,6-tris(ethenyl)-2,4,6-trimethyl-1,3,5,2,4,6-trioxatrisilinane Chemical compound C=C[Si]1(C)O[Si](C)(C=C)O[Si](C)(C=C)O1 BVTLTBONLZSBJC-UHFFFAOYSA-N 0.000 description 1
FAFGMAGIYHHRKN-UHFFFAOYSA-N 2-diphenylphosphanylethyl(diphenyl)phosphane;palladium Chemical compound [Pd].C=1C=CC=CC=1P(C=1C=CC=CC=1)CCP(C=1C=CC=CC=1)C1=CC=CC=C1.C=1C=CC=CC=1P(C=1C=CC=CC=1)CCP(C=1C=CC=CC=1)C1=CC=CC=C1 FAFGMAGIYHHRKN-UHFFFAOYSA-N 0.000 description 1
229910001020 Au alloy Inorganic materials 0.000 description 1
FERIUCNNQQJTOY-UHFFFAOYSA-M Butyrate Chemical compound CCCC([O-])=O FERIUCNNQQJTOY-UHFFFAOYSA-M 0.000 description 1
FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Natural products CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 1
239000004215 Carbon black (E152) Substances 0.000 description 1
206010053567 Coagulopathies Diseases 0.000 description 1
239000005977 Ethylene Substances 0.000 description 1
229910002621 H2PtCl6 Inorganic materials 0.000 description 1
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 1
IOVCWXUNBOPUCH-UHFFFAOYSA-M Nitrite anion Chemical compound [O-]N=O IOVCWXUNBOPUCH-UHFFFAOYSA-M 0.000 description 1
229910001252 Pd alloy Inorganic materials 0.000 description 1
YNHIGQDRGKUECZ-UHFFFAOYSA-L PdCl2(PPh3)2 Substances [Cl-].[Cl-].[Pd+2].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 YNHIGQDRGKUECZ-UHFFFAOYSA-L 0.000 description 1
OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
239000004820 Pressure-sensitive adhesive Substances 0.000 description 1
XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
BKPKTOIGWIYKJZ-UHFFFAOYSA-N [bis(ethenyl)-methylsilyl]oxy-bis(ethenyl)-methylsilane Chemical compound C=C[Si](C=C)(C)O[Si](C)(C=C)C=C BKPKTOIGWIYKJZ-UHFFFAOYSA-N 0.000 description 1
229960000583 acetic acid Drugs 0.000 description 1
238000013006 addition curing Methods 0.000 description 1
238000007259 addition reaction Methods 0.000 description 1
239000002671 adjuvant Substances 0.000 description 1
150000001338 aliphatic hydrocarbons Chemical class 0.000 description 1
125000003545 alkoxy group Chemical group 0.000 description 1
TWKVUTXHANJYGH-UHFFFAOYSA-L allyl palladium chloride Chemical class Cl[Pd]CC=C.Cl[Pd]CC=C TWKVUTXHANJYGH-UHFFFAOYSA-L 0.000 description 1
HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 description 1
229910052782 aluminium Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
229910052785 arsenic Inorganic materials 0.000 description 1
RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
238000001479 atomic absorption spectroscopy Methods 0.000 description 1
REHNCMANRAWBTN-UHFFFAOYSA-N bis(ethenyl)-[ethenyl(diethyl)silyl]oxy-ethylsilane Chemical compound CC[Si](CC)(C=C)O[Si](CC)(C=C)C=C REHNCMANRAWBTN-UHFFFAOYSA-N 0.000 description 1
QRHCILLLMDEFSD-UHFFFAOYSA-N bis(ethenyl)-dimethylsilane Chemical compound C=C[Si](C)(C)C=C QRHCILLLMDEFSD-UHFFFAOYSA-N 0.000 description 1
FSIJKGMIQTVTNP-UHFFFAOYSA-N bis(ethenyl)-methyl-trimethylsilyloxysilane Chemical compound C[Si](C)(C)O[Si](C)(C=C)C=C FSIJKGMIQTVTNP-UHFFFAOYSA-N 0.000 description 1
150000004758 branched silanes Chemical class 0.000 description 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
238000006555 catalytic reaction Methods 0.000 description 1
150000005829 chemical entities Chemical class 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
QCDFRRQWKKLIKV-UHFFFAOYSA-M chloroplatinum Chemical compound [Pt]Cl QCDFRRQWKKLIKV-UHFFFAOYSA-M 0.000 description 1
230000035602 clotting Effects 0.000 description 1
238000001246 colloidal dispersion Methods 0.000 description 1
239000000084 colloidal system Substances 0.000 description 1
230000000536 complexating effect Effects 0.000 description 1
239000002131 composite material Substances 0.000 description 1
238000001816 cooling Methods 0.000 description 1
238000012937 correction Methods 0.000 description 1
239000006184 cosolvent Substances 0.000 description 1
229920006037 cross link polymer Polymers 0.000 description 1
150000004759 cyclic silanes Chemical class 0.000 description 1
125000000640 cyclooctyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C([H])([H])C1([H])[H] 0.000 description 1
238000013461 design Methods 0.000 description 1
YNHIGQDRGKUECZ-UHFFFAOYSA-N dichloropalladium;triphenylphosphanium Chemical compound Cl[Pd]Cl.C1=CC=CC=C1[PH+](C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1[PH+](C=1C=CC=CC=1)C1=CC=CC=C1 YNHIGQDRGKUECZ-UHFFFAOYSA-N 0.000 description 1
125000005594 diketone group Chemical group 0.000 description 1
239000000975 dye Substances 0.000 description 1
239000000806 elastomer Substances 0.000 description 1
239000003822 epoxy resin Substances 0.000 description 1
KPWVUBSQUODFPP-UHFFFAOYSA-N ethenyl-(ethenyl-methyl-phenylsilyl)oxy-methyl-phenylsilane Chemical compound C=1C=CC=CC=1[Si](C)(C=C)O[Si](C)(C=C)C1=CC=CC=C1 KPWVUBSQUODFPP-UHFFFAOYSA-N 0.000 description 1
ZZDKMMZBGZPOGS-UHFFFAOYSA-N ethoxy(penta-1,4-dien-3-yl)silane Chemical compound C(=C)C(C=C)[SiH2]OCC ZZDKMMZBGZPOGS-UHFFFAOYSA-N 0.000 description 1
125000002534 ethynyl group Chemical group [H]C#C* 0.000 description 1
239000000194 fatty acid Substances 0.000 description 1
238000004817 gas chromatography Methods 0.000 description 1
239000012362 glacial acetic acid Substances 0.000 description 1
239000011521 glass Substances 0.000 description 1
239000011086 glassine Substances 0.000 description 1
239000003353 gold alloy Substances 0.000 description 1
150000004820 halides Chemical class 0.000 description 1
150000004687 hexahydrates Chemical class 0.000 description 1
125000006038 hexenyl group Chemical group 0.000 description 1
229930195733 hydrocarbon Natural products 0.000 description 1
150000002430 hydrocarbons Chemical class 0.000 description 1
238000010348 incorporation Methods 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
229910001504 inorganic chloride Inorganic materials 0.000 description 1
229910002094 inorganic tetrachloropalladate Inorganic materials 0.000 description 1
125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 description 1
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 1
239000010977 jade Substances 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
238000004898 kneading Methods 0.000 description 1
150000004757 linear silanes Chemical class 0.000 description 1
239000007788 liquid Substances 0.000 description 1
229910044991 metal oxide Inorganic materials 0.000 description 1
150000004706 metal oxides Chemical class 0.000 description 1
150000002739 metals Chemical class 0.000 description 1
JFCCVNTYPIUJDJ-UHFFFAOYSA-N methyl-tris(prop-2-enyl)silane Chemical compound C=CC[Si](C)(CC=C)CC=C JFCCVNTYPIUJDJ-UHFFFAOYSA-N 0.000 description 1
239000003607 modifier Substances 0.000 description 1
239000012778 molding material Substances 0.000 description 1
239000002808 molecular sieve Substances 0.000 description 1
239000000178 monomer Substances 0.000 description 1
125000004923 naphthylmethyl group Chemical group C1(=CC=CC2=CC=CC=C12)C* 0.000 description 1
125000000962 organic group Chemical group 0.000 description 1
150000003961 organosilicon compounds Chemical class 0.000 description 1
125000005375 organosiloxane group Chemical group 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
SWELZOZIOHGSPA-UHFFFAOYSA-N palladium silver Chemical compound [Pd].[Ag] SWELZOZIOHGSPA-UHFFFAOYSA-N 0.000 description 1
PBDBXAQKXCXZCJ-UHFFFAOYSA-L palladium(2+);2,2,2-trifluoroacetate Chemical compound [Pd+2].[O-]C(=O)C(F)(F)F.[O-]C(=O)C(F)(F)F PBDBXAQKXCXZCJ-UHFFFAOYSA-L 0.000 description 1
ZVSLRJWQDNRUDU-UHFFFAOYSA-L palladium(2+);propanoate Chemical compound [Pd+2].CCC([O-])=O.CCC([O-])=O ZVSLRJWQDNRUDU-UHFFFAOYSA-L 0.000 description 1
LXNAVEXFUKBNMK-UHFFFAOYSA-N palladium(II) acetate Substances [Pd].CC(O)=O.CC(O)=O LXNAVEXFUKBNMK-UHFFFAOYSA-N 0.000 description 1
NFHFRUOZVGFOOS-UHFFFAOYSA-N palladium;triphenylphosphane Chemical compound [Pd].C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1.C1=CC=CC=C1P(C=1C=CC=CC=1)C1=CC=CC=C1 NFHFRUOZVGFOOS-UHFFFAOYSA-N 0.000 description 1
239000000123 paper Substances 0.000 description 1
DSQPRECRRGZSCV-UHFFFAOYSA-N penta-1,4-dien-3-yl(phenyl)silane Chemical compound C=CC([SiH2]c1ccccc1)C=C DSQPRECRRGZSCV-UHFFFAOYSA-N 0.000 description 1
125000004344 phenylpropyl group Chemical group 0.000 description 1
150000003003 phosphines Chemical class 0.000 description 1
229910052698 phosphorus Inorganic materials 0.000 description 1
239000011574 phosphorus Substances 0.000 description 1
229910000073 phosphorus hydride Inorganic materials 0.000 description 1
239000011295 pitch Substances 0.000 description 1
HRGDZIGMBDGFTC-UHFFFAOYSA-N platinum(2+) Chemical compound [Pt+2] HRGDZIGMBDGFTC-UHFFFAOYSA-N 0.000 description 1
229920000647 polyepoxide Polymers 0.000 description 1
238000010094 polymer processing Methods 0.000 description 1
239000003505 polymerization initiator Substances 0.000 description 1
238000004382 potting Methods 0.000 description 1
239000012255 powdered metal Substances 0.000 description 1
239000000047 product Substances 0.000 description 1
238000010926 purge Methods 0.000 description 1
239000010453 quartz Substances 0.000 description 1
239000002516 radical scavenger Substances 0.000 description 1
230000002285 radioactive effect Effects 0.000 description 1
238000010992 reflux Methods 0.000 description 1
229910052703 rhodium Inorganic materials 0.000 description 1
239000010948 rhodium Substances 0.000 description 1
MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
150000003284 rhodium compounds Chemical class 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
239000000565 sealant Substances 0.000 description 1
150000003377 silicon compounds Chemical class 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
XFTDXEGRBTYXQE-UHFFFAOYSA-N silyl 3-ethenylpent-4-enoate Chemical compound C(=C)C(C=C)CC(=O)O[SiH3] XFTDXEGRBTYXQE-UHFFFAOYSA-N 0.000 description 1
URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 1
229910000030 sodium bicarbonate Inorganic materials 0.000 description 1
235000017557 sodium bicarbonate Nutrition 0.000 description 1
239000007787 solid Substances 0.000 description 1
238000007711 solidification Methods 0.000 description 1
230000008023 solidification Effects 0.000 description 1
238000003860 storage Methods 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
UFHILTCGAOPTOV-UHFFFAOYSA-N tetrakis(ethenyl)silane Chemical compound C=C[Si](C=C)(C=C)C=C UFHILTCGAOPTOV-UHFFFAOYSA-N 0.000 description 1
229920001169 thermoplastic Polymers 0.000 description 1
125000003944 tolyl group Chemical group 0.000 description 1
IGJPWUZGPMLVDT-UHFFFAOYSA-N tris(ethenyl)-tris(ethenyl)silyloxysilane Chemical compound C=C[Si](C=C)(C=C)O[Si](C=C)(C=C)C=C IGJPWUZGPMLVDT-UHFFFAOYSA-N 0.000 description 1
229930195735 unsaturated hydrocarbon Natural products 0.000 description 1
238000011179 visual inspection Methods 0.000 description 1
239000004636 vulcanized rubber Substances 0.000 description 1
239000008207 working material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/10—Metal compounds
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K6/00—Preparations for dentistry
- A61K6/90—Compositions for taking dental impressions
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B6/00—Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings
- G02B6/44—Mechanical structures for providing tensile strength and external protection for fibres, e.g. optical transmission cables
- G02B6/4401—Optical cables
- G02B6/4429—Means specially adapted for strengthening or protecting the cables
- G02B6/44382—Means specially adapted for strengthening or protecting the cables the means comprising hydrogen absorbing materials
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/12—Polysiloxanes containing silicon bound to hydrogen
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups

Landscapes

Health & Medical Sciences (AREA)
Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Physics & Mathematics (AREA)
Oral & Maxillofacial Surgery (AREA)
Polymers & Plastics (AREA)
Medicinal Chemistry (AREA)
Veterinary Medicine (AREA)
Epidemiology (AREA)
Life Sciences & Earth Sciences (AREA)
Public Health (AREA)
General Health & Medical Sciences (AREA)
Animal Behavior & Ethology (AREA)
General Physics & Mathematics (AREA)
Optics & Photonics (AREA)
Dental Preparations (AREA)
Compositions Of Macromolecular Compounds (AREA)
Solid-Sorbent Or Filter-Aiding Compositions (AREA)

JP53614897A 1996-04-09 1996-08-07 無機、有機および有機金属パラジウム水素スカベンジャー Expired - Fee Related JP3980647B2 (ja)

Applications Claiming Priority (3)

Application Number	Priority Date	Filing Date	Title
US08/629,864		1996-04-09
US08/629,864 US5684060A (en)	1996-04-09	1996-04-09	Compositions containing inorganic, organic and organometallic palladium hydrogen scavengers
PCT/US1996/012853 WO1997037632A1 (en)	1996-04-09	1996-08-07	Compositions containing inorganic, organic and organometallic palladium hydrogen scavengers

Related Child Applications (1)

Application Number	Title	Priority Date	Filing Date
JP2007085304A Division JP2007191722A (ja)	1996-04-09	2007-03-28	印象用硬化組成物およびその製造方法

Publications (3)

Publication Number	Publication Date
JP2000509026A JP2000509026A (ja)	2000-07-18
JP2000509026A5 JP2000509026A5 (2)	2004-09-02
JP3980647B2 true JP3980647B2 (ja)	2007-09-26

Family

ID=24524811

Family Applications (2)

Application Number	Title	Priority Date	Filing Date
JP53614897A Expired - Fee Related JP3980647B2 (ja)	1996-04-09	1996-08-07	無機、有機および有機金属パラジウム水素スカベンジャー
JP2007085304A Pending JP2007191722A (ja)	1996-04-09	2007-03-28	印象用硬化組成物およびその製造方法

Family Applications After (1)

Application Number	Title	Priority Date	Filing Date
JP2007085304A Pending JP2007191722A (ja)	1996-04-09	2007-03-28	印象用硬化組成物およびその製造方法

Country Status (8)

Country	Link
US (1)	US5684060A (2)
EP (1)	EP0892630B1 (2)
JP (2)	JP3980647B2 (2)
AU (1)	AU718483B2 (2)
BR (1)	BR9612590A (2)
CA (1)	CA2250001C (2)
DE (1)	DE69618675T2 (2)
WO (1)	WO1997037632A1 (2)

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JP5559061B2 (ja)	2007-12-18	2014-07-23	スリーエムイノベイティブプロパティズカンパニー	界面活性剤及びｆ−含有化合物を含有する歯科用組成物、その作製プロセス及び使用
EP2133063A1 (en)	2008-06-10	2009-12-16	3M Innovative Properties Company	Initiator system with biphenylene derivates, method of production and use thereof
JP5539763B2 (ja) *	2010-03-24	2014-07-02	株式会社松風	医科・歯科用シリコーン印象材組成物
JP5727033B2 (ja) *	2010-12-13	2015-06-03	ブルースターシリコンズフランスＢｌｕｅｓｔａｒＳｉｌｉｃｏｎｅｓＦｒａｎｃｅ	特に歯科印象採得を目的として使用可能なシリコーンエラストマー材料
BR112013031095A2 (pt)	2011-06-08	2016-12-06	3M Innovative Properties Co	composição contendo compostos de siloxano, método de produção e uso da mesma
WO2013025494A1 (en)	2011-08-12	2013-02-21	3M Innovative Properties Company	Curable composition with shortened setting time, process of production and use thereof
TW201414796A (zh)	2012-07-27	2014-04-16	Dow Corning	自黏結可固化聚矽氧黏著劑之組成物及製造彼之方法
WO2014130603A1 (en)	2013-02-25	2014-08-28	3M Innovative Properties Company	Stabilized dental impression composition, kit of parts and use thereof
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EP3302402B1 (en)	2015-05-29	2020-04-29	3M Innovative Properties Company	Kit of parts for conducting a dental impression and retraction process
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1996
- 1996-04-09 US US08/629,864 patent/US5684060A/en not_active Expired - Lifetime
- 1996-08-07 BR BR9612590A patent/BR9612590A/pt not_active IP Right Cessation
- 1996-08-07 JP JP53614897A patent/JP3980647B2/ja not_active Expired - Fee Related
- 1996-08-07 DE DE69618675T patent/DE69618675T2/de not_active Expired - Lifetime
- 1996-08-07 EP EP96927337A patent/EP0892630B1/en not_active Expired - Lifetime
- 1996-08-07 WO PCT/US1996/012853 patent/WO1997037632A1/en not_active Ceased
- 1996-08-07 CA CA002250001A patent/CA2250001C/en not_active Expired - Fee Related
- 1996-08-07 AU AU67197/96A patent/AU718483B2/en not_active Ceased
2007
- 2007-03-28 JP JP2007085304A patent/JP2007191722A/ja active Pending

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
JP2007191722A (ja) *	1996-04-09	2007-08-02	3M Co	印象用硬化組成物およびその製造方法

Also Published As

Publication number	Publication date
EP0892630B1 (en)	2002-01-09
DE69618675T2 (de)	2002-08-22
AU718483B2 (en)	2000-04-13
DE69618675D1 (de)	2002-02-28
JP2000509026A (ja)	2000-07-18
JP2007191722A (ja)	2007-08-02
BR9612590A (pt)	1999-07-20
AU6719796A (en)	1997-10-29
US5684060A (en)	1997-11-04
CA2250001A1 (en)	1997-10-16
EP0892630A1 (en)	1999-01-27
WO1997037632A1 (en)	1997-10-16
CA2250001C (en)	2008-10-14

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Publication	Publication Date	Title
JP3980647B2 (ja)	2007-09-26	無機、有機および有機金属パラジウム水素スカベンジャー
EP1512724B1 (en)	2007-04-11	Allylsilane containing composition
JP3122238B2 (ja)	2001-01-09	歯科的応用面用の透明材料
CA1338813C (en)	1996-12-24	Visible radiation activated hydrosilation reaction
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JP3980647B2 - 無機、有機および有機金属パラジウム水素スカベンジャー - Google Patents

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