JPH0122346B2 - - Google Patents
Info
- Publication number
- JPH0122346B2 JPH0122346B2 JP61214488A JP21448886A JPH0122346B2 JP H0122346 B2 JPH0122346 B2 JP H0122346B2 JP 61214488 A JP61214488 A JP 61214488A JP 21448886 A JP21448886 A JP 21448886A JP H0122346 B2 JPH0122346 B2 JP H0122346B2
- Authority
- JP
- Japan
- Prior art keywords
- aluminum alloy
- directionality
- content
- heating
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
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- Metal Rolling (AREA)
Description
〔産業上の利用分野〕
本発明は方向性の優れたアルミニウム合金の製
造法に関し、さらに詳しくは、深絞り用の方向性
の優れたアルミニウム合金の製造法に関する。
〔従来技術〕
深絞り加工により製造されるPPキヤツプ等の
材料としては純アルミニウムA3003合金の半硬質
材、A3105、A5052合金の硬質材等が使用されて
いる。
しかして、Al―Mg系合金は方向性のバラツキ
が大きく、深絞り加工後、裾部のトリミング量を
多くする必要があり、歩留りが低かつた。
〔発明が解決しようとする問題点〕
本発明は上記に説明した従来のアルミニウム合
金の方向性のバラツキの問題に鑑み、本発明者が
鋭意研究を行つた結果、方向性のバラツキを低く
抑制し、深絞り加工後のトリミングの省略あるい
は減少させ、打ち抜きブランク径を小さくするこ
とができ、成形加工時の歩留りの向上を図ること
ができる方向性の優れたアルミニウム合金の製造
法を開発したのである。
〔問題点を解決するための手段〕
本発明に係る方向性のすぐれたアルミニウム合
金の製造法は、
(1) Si0.20〜0.80wt%、Fe0.30〜1.75wt%、
Mg0.20〜5wt%
を含有し、残部Alおよび不純物からなるアル
ミニウム合金を、冷間圧延途中に400〜600℃の
温度に100℃/分以上の加熱速度で加熱し、加
熱後直ちに、または10分以内保持した後、100
℃/分以上の冷却速度で冷却し、さらに、10%
以上の冷間圧延を行うことを特徴とする方向性
の優れたアルミニウム合金の製造法を第1の発
明とし、
(2) Si0.20〜0.80wt%、Fe0.30〜1.75wt%、
Mg0.20〜5wt%
を含有し、かつ、
Cu0.05〜0.5wt%、Cr0.03〜0.5wt%の1種ま
たは2種
を含有し、残部Alおよび不純物からなるアル
ミニウム合金を、冷間圧延途中に400〜600℃の
温度に100℃/分以上の加熱速度で加熱し、加
熱後直ちに、または、10分以内保持した後、
100℃/分以上の冷却速度で冷却し、さらに、
10%以上の冷間圧延を行うことを特徴とする方
向性の優れたアルミニウム合金の製造法を第2
の発明とする2つの発明よりなるものである。
本発明に係る方向性の優れたアルミニウム合金
の製造法について以下詳細に説明する。
先ず、本発明に係る方向性の優れたアルミニウ
ム合金の製造法において使用するアルミニウム合
金の含有成分および含有割合について説明する。
Siは深絞り耳のバラツキを抑制し、伸びを大き
くする作用を有する元素であり、含有量が0.20wt
%未満では耳率のバラツキ抑制効果が劣り、ま
た、0.80wt%を越えて含有されると結晶粒が大き
くなり、加工性が劣るようになる。よつて、Si含
有量は0.20〜0.80wt%とする。
FeはSiと共に深絞り耳のバラツキを抑制し、
結晶粒を微細化する作用があり、含有量が0.30wt
%未満ではこの効果は少なく、また、1.75wt%を
越えて含有されると脆化が進み、伸びが得られな
い。よつて、Fe含有量は0.30〜1.75wt%とする。
Mgは伸びに影響することなく材料の強度を高
め、耳率のバラツキを抑制する作用を有し、含有
量が0.20wt%未満では所望の効果が得られず、ま
た、5wt%を越えて含有されると脆くなり、加工
性が劣化する。よつて、Mg含有量は0.20〜5wt
%とする。
CuはMgと同時に含有させることにより、Mg
と共に溶体化に固溶してベーキング時に微細な
Al−Cu−Mg系析出物を生成して硬化させ、耳率
のバラツキには悪影響を及ぼさず、また、溶体化
処理の温度を制御することにより、種々の強度の
アルミニウム合金を製造可能であり、含有量が
0.05wt%未満では上記の効果は期待できず、
0.5wt%を越えて含有させると上記の効果は満た
すが、深絞り用材料として耐蝕性が非常に劣化す
る。よつて、Cu含有量は0.05〜0.5wt%とする。
Crはアルミニウム合金の強度を高めると共に
金属間化合物の効果により開栓性をよくする元素
であり、含有量が0.03wt%未満では上記の効果は
期待できず、また、0.5wt%を越えて含有される
と深絞り性が劣化する。よつて、Cr含有量は0.03
〜0.5wt%とする。
次に、本発明に係る方向性の優れたアルミニウ
ム合金の製造法について説明する。
方向性のバラツキを抑制するには、急速加熱、
急速冷却、中間焼鈍の効果が大きい。
この方向性のバラツキを抑制するには、種々の
要因がある析出物のコントロールが非常に重要で
あり、均熱温度、時間、熱間圧延条件等も影響力
が大きいが、中間焼鈍を急速加熱、短時間保持、
急速冷却をすることにより、方向性のバラツキを
抑制することができる。合わせて結晶粒が微細に
なるため、深絞り性、肌荒性にも優れている。ま
た、仕上げ冷間圧延率は方向性のコントロールに
重要であるが、仕上げ冷間圧延率と方向性の関係
は概ね第1図に示すようになる。
方向性が0%となる冷間加工率は組成および熱
間仕上げ板厚、熱間圧延条件、均熱条件等によつ
て異なるが、0%になるように決定すればよい。
また、熱間圧延終了後直ちに中間焼鈍を実施す
れば方向性のバラツキはさらに小さくなる。仕上
げ圧延後、強度調整または残留応力除去のために
250℃以下の低温で仕上げ焼鈍を実施しても方向
性には変化はない。
〔実施例〕
本発明に係る方向性の優れたアルミニウム合金
の製造法の実施例を説明する。
実施例
第1表に示す含有成分および含有割合のアルミ
ニウム合金を造塊し、面削後、510℃×6時間の
均熱処理後、直ちに熱間圧延を開始し、310℃±
10℃で3mmtに熱間圧延を終了した。
その後、方向性が1%となる冷間加工率で中間
焼鈍を実施した(バツチ中間焼鈍:340℃×2Hr、
急速加熱冷却:450℃×0sec、昇降温スピード900
℃/分)。さらに、最終0.25mmtまで冷間圧延を
行つた。
その後、塗装焼付処理に相当する190℃×10分
の熱処理を行つた。
このようにして得られた薄板の機械的性質、耳
率の測定結果を第1表に示す。
第1表において、
・方向性は33mmtφポンチ径、48%絞り率、n=
3。
・方向性はそれぞれ10チヤージ分溶解鋳造し、同
一工程により製造し、強度および耳率を測定し
た。
・製造工程
:中間焼鈍:到達温度、450℃×0秒、昇降
温スピード900℃/分。
:中間焼鈍:340℃×2時間(40℃/時間、
昇降温スピード)。
:熱間圧延終了後、340℃×2Hr(40℃/時
間、昇降温スピード)の熱処理を実施後
の工程。
:熱間圧延終了後、340℃×2Hr(40℃/時
間、昇降温スピード)の熱処理を実施後
の工程。
である。
[Industrial Application Field] The present invention relates to a method for producing an aluminum alloy with excellent directionality, and more particularly, to a method for producing an aluminum alloy with excellent directionality for deep drawing. [Prior Art] Semi-hard materials such as pure aluminum A3003 alloy and hard materials such as A3105 and A5052 alloys are used as materials for PP caps and the like manufactured by deep drawing. However, Al--Mg alloys have large variations in directionality, and after deep drawing, it is necessary to trim a large amount of the skirt, resulting in low yields. [Problems to be Solved by the Invention] In view of the above-mentioned problem of the variation in orientation of conventional aluminum alloys, the present inventor has conducted extensive research, and as a result, the present invention has been developed to suppress the variation in orientation to a low level. We have developed a method for producing aluminum alloys with excellent directionality that can eliminate or reduce the need for trimming after deep drawing, reduce the diameter of the punched blank, and improve the yield during forming. . [Means for solving the problem] The method for producing an aluminum alloy with excellent directionality according to the present invention includes: (1) 0.20 to 0.80 wt% Si, 0.30 to 1.75 wt% Fe,
An aluminum alloy containing 0.20 to 5 wt% Mg and the remainder Al and impurities is heated to a temperature of 400 to 600 °C during cold rolling at a heating rate of 100 °C/min or more, and immediately after heating or After holding for less than 100 minutes
Cooled at a cooling rate of ℃/min or more, and further reduced by 10%
The first invention is a method for producing an aluminum alloy with excellent orientation, characterized by performing the above cold rolling, (2) Si0.20-0.80wt%, Fe0.30-1.75wt%,
An aluminum alloy containing 0.20 to 5 wt% Mg, and one or both of Cu 0.05 to 0.5 wt% and Cr 0.03 to 0.5 wt%, with the balance Al and impurities is cold-rolled. During heating, heat to a temperature of 400 to 600°C at a heating rate of 100°C/min or more, and immediately after heating, or after holding for less than 10 minutes,
Cooled at a cooling rate of 100℃/min or more, and
The second method for producing an aluminum alloy with excellent orientation, which is characterized by cold rolling of 10% or more.
This invention consists of two inventions. The method for producing an aluminum alloy with excellent directionality according to the present invention will be described in detail below. First, the components and content ratios of the aluminum alloy used in the method for producing an aluminum alloy with excellent directionality according to the present invention will be explained. Si is an element that suppresses variations in deep-drawn selvedges and increases elongation, and the content is 0.20wt.
If the content is less than 0.80wt%, the effect of suppressing variation in the ear ratio will be poor, and if the content exceeds 0.80wt%, the crystal grains will become large and the processability will be poor. Therefore, the Si content is set to 0.20 to 0.80 wt%. Together with Si, Fe suppresses the variation in deep drawing edges,
It has the effect of refining crystal grains, and the content is 0.30wt.
If the content is less than 1.75wt%, this effect will be small, and if the content exceeds 1.75wt%, embrittlement will progress and elongation will not be obtained. Therefore, the Fe content is set to 0.30 to 1.75 wt%. Mg has the effect of increasing the strength of the material without affecting elongation and suppressing variations in the selvedge ratio. If the content is less than 0.20wt%, the desired effect cannot be obtained, and if the content exceeds 5wt%, If it is damaged, it becomes brittle and its workability deteriorates. Therefore, the Mg content is 0.20~5wt
%. By containing Cu at the same time as Mg, Mg
It also dissolves in solution and forms fine particles during baking.
By producing Al-Cu-Mg-based precipitates and hardening them, it does not adversely affect the variation in selvedge ratio, and by controlling the temperature of solution treatment, it is possible to manufacture aluminum alloys with various strengths. , the content is
Below 0.05wt%, the above effects cannot be expected;
When the content exceeds 0.5 wt%, the above effects are achieved, but the corrosion resistance as a material for deep drawing is greatly deteriorated. Therefore, the Cu content is set to 0.05 to 0.5 wt%. Cr is an element that increases the strength of aluminum alloys and improves the opening performance due to the effect of intermetallic compounds.The above effects cannot be expected if the content is less than 0.03wt%, and if the content exceeds 0.5wt%. If this happens, the deep drawability will deteriorate. Therefore, the Cr content is 0.03
~0.5wt%. Next, a method for producing an aluminum alloy with excellent directionality according to the present invention will be explained. To suppress variations in directionality, rapid heating,
Rapid cooling and intermediate annealing have great effects. In order to suppress this variation in directionality, it is very important to control precipitates due to various factors, and soaking temperature, time, hot rolling conditions, etc. also have a large influence, but rapid heating during intermediate annealing , short-term retention,
By performing rapid cooling, variations in directionality can be suppressed. In addition, since the crystal grains are fine, it has excellent deep drawability and roughness. Furthermore, the finish cold rolling rate is important for controlling the directionality, and the relationship between the finish cold rolling rate and the directionality is generally shown in FIG. 1. The cold working rate at which the directionality becomes 0% varies depending on the composition, hot finished plate thickness, hot rolling conditions, soaking conditions, etc., but may be determined so that the directionality becomes 0%. Furthermore, if intermediate annealing is performed immediately after hot rolling, the variation in directionality will be further reduced. For strength adjustment or residual stress removal after finish rolling
There is no change in directionality even if finish annealing is performed at a low temperature of 250°C or lower. [Example] An example of the method for producing an aluminum alloy with excellent directionality according to the present invention will be described. Example An aluminum alloy having the components and content ratios shown in Table 1 was formed into an ingot, and after facing and soaking treatment at 510°C for 6 hours, hot rolling was immediately started and the aluminum alloy was rolled at 310°C ±
Hot rolling was completed at 10°C to a thickness of 3 mm. After that, intermediate annealing was performed at a cold working rate that gave a directionality of 1% (batch intermediate annealing: 340°C x 2Hr,
Rapid heating and cooling: 450℃ x 0sec, temperature rise and fall speed 900
°C/min). Furthermore, cold rolling was performed to a final thickness of 0.25 mm. Thereafter, heat treatment was performed at 190°C for 10 minutes, which corresponds to paint baking treatment. Table 1 shows the results of measuring the mechanical properties and selvage ratio of the thin plate thus obtained. In Table 1, ・Direction is 33mmtφ punch diameter, 48% drawing ratio, n=
3.・For each directionality, 10 charges were melted and cast, manufactured using the same process, and the strength and selvedge ratio were measured.・Manufacturing process: Intermediate annealing: Achieved temperature: 450°C x 0 seconds, temperature increase/decrease speed: 900°C/min. : Intermediate annealing: 340℃ x 2 hours (40℃/hour,
temperature increase/decrease speed). : Process after heat treatment at 340℃ x 2 hours (40℃/hour, temperature increase/decrease speed) after hot rolling. : Process after heat treatment at 340℃ x 2 hours (40℃/hour, temperature increase/decrease speed) after hot rolling. It is.
【表】
実施例 2
第2表に示す含有成分および含有割合のアルミ
ニウム合金を造塊し、面削の後、510℃×4時間
の均熱処理後、直ちに熱間圧延を開始し、310±
10℃で3mmtに仕上げた。その後、方向性1%と
なる冷間加工率で中間焼鈍を実施した。
さらに、最終0.24mmtまで冷間圧延を行つた。
その後、塗装焼付処理に相当する190℃×10分
の熱処理を加えた。
このようにして得られた薄板の機械的性質、耳
率の測定結果を第2表に示す。
この第2表より、本発明に係る方向性の優れた
アルミニウム合金の製造法によりえられた製品
は、Cuの含有により方向性のバラツキに影響な
く、強度を高める効果があり、また、Crの含有
は強度を高めると共に開栓性改善に効果のあるこ
とがわかる。[Table] Example 2 An aluminum alloy having the components and content ratios shown in Table 2 was formed into an ingot, and after facing and soaking treatment at 510°C for 4 hours, hot rolling was immediately started.
Finished to 3mmt at 10℃. Thereafter, intermediate annealing was performed at a cold working rate that gave a directionality of 1%. Furthermore, cold rolling was performed to a final thickness of 0.24 mm. After that, heat treatment was applied at 190°C for 10 minutes, which corresponds to paint baking treatment. Table 2 shows the results of measuring the mechanical properties and selvage ratio of the thin plates thus obtained. From this Table 2, it can be seen that the products obtained by the method of manufacturing aluminum alloys with excellent orientation according to the present invention have the effect of increasing strength without affecting the variation in orientation due to the inclusion of Cu, and also have the effect of increasing strength due to the inclusion of Cu. It can be seen that the inclusion is effective in increasing strength and improving openability.
以上説明したように、本発明に係る方向性の優
れたアルミニウム合金の製造法は上記の構成であ
るから、耳率のバラツキが非常に少ないアルミニ
ウム合金が製造でき、かつ、深絞り加工後、裾部
のトリミング量を省略、或いは、減少することが
でき。抜絞りの時のブランク径を小さくでき、加
工歩留りが大幅に向上するという効果がある。
As explained above, since the method for manufacturing an aluminum alloy with excellent directionality according to the present invention has the above configuration, an aluminum alloy with very little variation in selvage ratio can be manufactured, and after deep drawing, the hem The amount of trimming can be omitted or reduced. This has the effect of reducing the blank diameter during drawing and drawing, and greatly improving processing yield.
第1図は仕上げ圧延率と方向性の関係を示す図
である。
FIG. 1 is a diagram showing the relationship between finish rolling rate and directionality.
Claims (1)
Mg0.20〜5wt% を含有し、残部Alおよび不純物からなるアルミ
ニウム合金を、冷間圧延途中に400〜600℃の温度
に100℃/分以上の加熱速度で加熱し、加熱後直
ちに、または、10分以内保持した後、100℃/分
以上の冷却速度で冷却し、さらに、10%以上の冷
間圧延を行うことを特徴とする方向性の優れたア
ルミニウム合金の製造法。 2 Si0.20〜0.80wt%、Fe0.30〜1.75wt%、
Mg0.20〜5wt% を含有し、かつ、 Cu0.05〜0.5wt%、Cr0.03〜0.5wt%の1種また
は2種 を含有し、残部Alおよび不純物からなるアルミ
ニウム合金を、冷間圧延途中に400〜600℃の温度
に100℃/分以上の加熱速度で加熱し、加熱後直
ちに、または、10分以内保持した後、100℃/分
以上の冷却速度で冷却し、さらに、10%以上の冷
間圧延を行うことを特徴とする方向性の優れたア
ルミニウム合金の製造法。[Claims] 1 Si0.20-0.80wt%, Fe0.30-1.75wt%,
An aluminum alloy containing 0.20 to 5 wt% Mg and the remainder Al and impurities is heated to a temperature of 400 to 600°C at a heating rate of 100°C/min or more during cold rolling, and immediately after heating, or A method for producing an aluminum alloy with excellent orientation, which comprises holding for 10 minutes or less, cooling at a cooling rate of 100°C/min or more, and then cold rolling by 10% or more. 2 Si0.20~0.80wt%, Fe0.30~1.75wt%,
An aluminum alloy containing 0.20 to 5 wt% Mg, and one or both of Cu 0.05 to 0.5 wt% and Cr 0.03 to 0.5 wt%, with the balance Al and impurities is cold-rolled. During heating, heat to a temperature of 400 to 600°C at a heating rate of 100°C/min or more, immediately after heating, or after holding for less than 10 minutes, cool at a cooling rate of 100°C/min or more, and further, 10% A method for producing an aluminum alloy with excellent orientation, characterized by performing the above cold rolling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP21448886A JPS6369953A (en) | 1986-09-11 | 1986-09-11 | Manufacture of aluminum alloy excellent in directionality |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP21448886A JPS6369953A (en) | 1986-09-11 | 1986-09-11 | Manufacture of aluminum alloy excellent in directionality |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6369953A JPS6369953A (en) | 1988-03-30 |
| JPH0122346B2 true JPH0122346B2 (en) | 1989-04-26 |
Family
ID=16656543
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP21448886A Granted JPS6369953A (en) | 1986-09-11 | 1986-09-11 | Manufacture of aluminum alloy excellent in directionality |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6369953A (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP4260510B2 (en) * | 2002-03-07 | 2009-04-30 | ユニバーサル製缶株式会社 | Cap and screw type sealed bottle |
| CN107243696A (en) * | 2017-06-06 | 2017-10-13 | 沈阳工业大学 | A kind of aluminium alloy liquid nitrogen bath laser heat treatment strengthening process |
| CN111118421A (en) * | 2020-01-16 | 2020-05-08 | 南京理工大学 | Method for eliminating transverse grain boundary of high-conductivity pure copper wire |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58224142A (en) * | 1982-06-22 | 1983-12-26 | Sumitomo Light Metal Ind Ltd | Aluminum alloy plate with superior formability and its manufacture |
| JPS59193252A (en) * | 1983-03-10 | 1984-11-01 | Kobe Steel Ltd | Preparation of deep drawing aluminum alloy thin plate |
| JPS59193253A (en) * | 1983-03-31 | 1984-11-01 | Kobe Steel Ltd | Preparation of deep drawing aluminum alloy plate |
| IT1196142B (en) * | 1984-06-11 | 1988-11-10 | Sicor Spa | PROCEDURE FOR THE PREPARATION OF 16.17-ACETALS OF PREGNANIC DERIVATIVES AND NEW COMPOUNDS OBTAINED |
-
1986
- 1986-09-11 JP JP21448886A patent/JPS6369953A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6369953A (en) | 1988-03-30 |
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