JPH02204353A - Sound absorbing material - Google Patents
Sound absorbing materialInfo
- Publication number
- JPH02204353A JPH02204353A JP1022357A JP2235789A JPH02204353A JP H02204353 A JPH02204353 A JP H02204353A JP 1022357 A JP1022357 A JP 1022357A JP 2235789 A JP2235789 A JP 2235789A JP H02204353 A JPH02204353 A JP H02204353A
- Authority
- JP
- Japan
- Prior art keywords
- sound absorbing
- absorbing material
- slag
- size
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000011358 absorbing material Substances 0.000 title claims abstract description 26
- 239000002893 slag Substances 0.000 claims abstract description 23
- 239000011347 resin Substances 0.000 claims abstract description 16
- 229920005989 resin Polymers 0.000 claims abstract description 16
- 229920001187 thermosetting polymer Polymers 0.000 claims abstract description 15
- 239000003350 kerosene Substances 0.000 claims abstract description 11
- 238000010438 heat treatment Methods 0.000 claims abstract description 6
- 238000000465 moulding Methods 0.000 claims abstract description 6
- 239000000843 powder Substances 0.000 claims description 18
- 239000002245 particle Substances 0.000 abstract description 16
- 238000010521 absorption reaction Methods 0.000 abstract description 5
- 239000000203 mixture Substances 0.000 abstract description 4
- 150000001875 compounds Chemical class 0.000 abstract 2
- 230000001771 impaired effect Effects 0.000 abstract 2
- 230000001105 regulatory effect Effects 0.000 abstract 1
- 239000000463 material Substances 0.000 description 11
- 229910052751 metal Inorganic materials 0.000 description 7
- 239000002184 metal Substances 0.000 description 7
- 238000005245 sintering Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000011230 binding agent Substances 0.000 description 2
- 238000009415 formwork Methods 0.000 description 2
- 238000004898 kneading Methods 0.000 description 2
- 235000019738 Limestone Nutrition 0.000 description 1
- 101100276210 Rhizobium meliloti (strain 1021) cya2 gene Proteins 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 239000002440 industrial waste Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000006082 mold release agent Substances 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/02—Macromolecular compounds
- C04B26/10—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Building Environments (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Soundproofing, Sound Blocking, And Sound Damping (AREA)
Abstract
Description
【発明の詳細な説明】
〔産業上の利用分野〕
本発明は、スラグを主体に形成した吸音材に関するもの
である。DETAILED DESCRIPTION OF THE INVENTION [Field of Industrial Application] The present invention relates to a sound absorbing material mainly made of slag.
従来、吸汗材として金属粉を焼結成形したものがある。 Conventionally, sweat absorbent materials have been made by sintering metal powder.
これは、同一種類の金属粉を耐火性熱プレスにより加圧
しつつ高温焼結することによって製造するものである。This is manufactured by sintering the same type of metal powder at high temperature while pressurizing it with a fire-resistant heat press.
ところが、係る従来の吸音材は、金属粉を焼結させて作
るものであるため１表面が融着状態となり、従って吸音
特性が低下してしまうという欠点がある。However, since such conventional sound absorbing materials are made by sintering metal powder, one surface becomes fused, resulting in a reduction in sound absorbing properties.
また、これを防止するため焼結度を低くして板状に成形
すると強度が低下するという問題を生ずる。Furthermore, in order to prevent this, if the degree of sintering is lowered and formed into a plate shape, a problem arises in that the strength decreases.
本領１の発明は、前記課題を解決するため、吸音材とし
て、１〜５ ｍ ３の大きさに粗砕されたスラグ８０〜
９８重量％、熱硬化性粉末レジン１．５〜１５重量％、
灯油０．２〜２．０重量％が混練され、加圧力１５〜５
０ ｋｇ／ ＞ ’、加圧時間５〜１５秒の条件の下に
プレスされ、温度１５０〜３５０℃で加熱成形されてな
る構成を採用している。In order to solve the above-mentioned problem, the main invention of the invention is to use slag 80~ which is roughly crushed into a size of 1~5 m3 as a sound absorbing material.
98% by weight, thermosetting powder resin 1.5-15% by weight,
Kerosene 0.2 to 2.0% by weight is kneaded, and the pressing force is 15 to 5%.
0 kg/>', pressure time is 5 to 15 seconds, and heat molding is performed at a temperature of 150 to 350°C.
また１本第２の発明は、水弟１の発明のものが、板状に
成形され、中間に金網が介装された構成を採用している
。In addition, the second invention employs a configuration in which the invention of Mizui 1 is formed into a plate shape and a wire mesh is interposed in the middle.
なお１本ｆ！ｃ１及び第２の発明において、吸音材を板
状体として成形する場合、各板の大きさは、厚さ１０〜
２０ＩＩＩｌ１面積２００ｎ＊ Ｘ ２００ｍ〜３００
■Ｘ ３００■であるのが望ましい。In addition, one f! In c1 and the second invention, when the sound absorbing material is formed into a plate-shaped body, the size of each plate is 10 to 10 mm thick.
20III1 Area 200n* X 200m~300
■X 300■ is desirable.
また、その場合、各板状体の四囲には枠材をはめ込んで
おき、その枠材を利用して多数の板状体を接合し、吸音
壁等として構成することもできる。Further, in that case, a frame material may be fitted around the four sides of each plate-like body, and a large number of plate-like bodies may be joined using the frame material to form a sound-absorbing wall or the like.
水弟１の発明及び水弟２の発明において、吸音材のスラ
グ粒子自体が多孔性であると共にスラグ粒子間にも多数
の隙間を生じていることから吸音性を発揮する。In the inventions of Mizui 1 and Mizui 2, the slag particles of the sound absorbing material themselves are porous and have many gaps between the slag particles, so they exhibit sound absorbing properties.
また１本ｔＪ２の発明において、金網の介在によって板
状の吸音材の機械的強度が高まる。Further, in the invention of 1 tJ2, the mechanical strength of the plate-shaped sound absorbing material is increased by the interposition of the wire mesh.
図面に基づき１本発明の詳細な説明する。 The present invention will be explained in detail based on the drawings.
実」１例」−
１〜５鵬３の大きさに粗砕したスラグを９０重量％、粘
結剤として熱硬化性粉末レジンを５．０重量％、混線液
として灯油を１．０重量％混ぜ合わせて混練し、次にこ
れを、離型剤を塗布した型枠（ｆｌｉｔ示せず）内に投
入し、板状に均した。Example 1 - 90% by weight of slag roughly crushed to a size of 1 to 5 3, 5.0% by weight of thermosetting powder resin as a binder, and 1.0% by weight of kerosene as a mixing liquid. The mixture was mixed and kneaded, and then placed in a mold (flit not shown) coated with a mold release agent and leveled into a plate shape.
この板状体の大きさは、厚さ１５腫、面積２５０ｍ Ｘ
２５０■とした。The size of this plate-like body is 15 m thick and 250 m in area.
It was set to 250■.
また、前記スラグとしては、キュポラで生じたスラグ（
ノロ）を水砕処理して１〜５ ａｍ３の粒度としたもの
を用いた。キュポラのスラグは石灰石、地金の酸化物、
コークス中の灰分、侵食された炉壁材料等が溶は合って
できたもので。In addition, as the slag, slag generated in a cupola (
The material used was one obtained by pulverizing slag) to a particle size of 1 to 5 am3. Cupola slag is made of limestone, oxides of bare metal,
It is formed when the ash in the coke and the eroded furnace wall material melt together.
５ｉ０２が４０〜５０重量％、ＣａＯが２０〜３５重量
％、ＭｇＯが０〜３％、Ａｌ２Ｏ３が５〜１２重量％、
ＦｓＯが０．５−０．７重量％。5i02 is 40-50% by weight, CaO is 20-35% by weight, MgO is 0-3%, Al2O3 is 5-12% by weight,
0.5-0.7% by weight FsO.
Ｍ ｎ Ｏが０．５−２．０重量％、Ｓが０．１−０．
４重量％の組成成分からなるものを用いた。MnO is 0.5-2.0% by weight, S is 0.1-0.
A composition consisting of 4% by weight of components was used.
熱硬化性粉末レジンとしては、フェノールレジンを用い
た。Phenol resin was used as the thermosetting powder resin.
灯油は市販のものを用い、この灯油により熱硬化性粉末
レジンを半溶融状態にして前記混練時においてスラグの
表面に均一にコーティングした。A commercially available kerosene was used, and the thermosetting powder resin was semi-molten with this kerosene, and was uniformly coated on the surface of the slag during the kneading.
次いで、型枠内の板状体をプレス機により。Next, the plate-shaped body inside the formwork is pressed using a press machine.
５０ｋｇ／ａ１１２の加圧力で、１０秒間だけプレスし
た。Pressing was carried out for only 10 seconds at a pressure of 50 kg/a112.
しかる後、加熱炉にて２００〜３００℃の温度下で加熱
し、スラグの粒子を前記粘結剤によって結合させた。Thereafter, it was heated in a heating furnace at a temperature of 200 to 300°C to bind the slag particles together with the binder.
この段階において、第１図で示されるように。At this stage, as shown in FIG.
板状体を構成する個々のスラグの粒子１の隣接静間に膜
状に付着した熱硬化性粉末レジン２の硬化によって粒子
１同士が結合され１個々の粒子１は多くの露出面６を有
すると共に粒子１間には多くの空隙３が随所に形成され
る。The particles 1 are bonded to each other by the curing of the thermosetting powder resin 2 that adheres in a film form between the adjacent slag particles 1 constituting the plate-shaped body, and each particle 1 has many exposed surfaces 6. Many voids 3 are formed everywhere between the particles 1.
この加熱成形の後、型枠から板状体を取り出し、該板状
体の四囲に第２図で示されるような溝を有したアルミニ
ュウム製の枠材４をはめ込んで第３図の如く構成した。After this hot forming, the plate-like body was taken out from the mold, and an aluminum frame 4 having grooves as shown in Fig. 2 was fitted around the four sides of the plate-like body, so that it was constructed as shown in Fig. 3. .
もちろん、このような枠材４をはめ込まないでも、当業
者間において通常用いられる手段により板状体同士を接
合し、壁等として構成することもできる。Of course, without fitting such a frame member 4, it is also possible to construct a wall or the like by joining the plate-like bodies together by means commonly used by those skilled in the art.
なお、第３図において符号５は前記板状体を示している
。In addition, in FIG. 3, the reference numeral 5 indicates the plate-shaped body.
前記枠材４は、板状体を保護すると共に板状体相互間を
連結できるようにするため取り付けられるものであり、
樹ｎ製であってもよいものである。The frame material 4 is attached to protect the plate-like bodies and to connect the plate-like bodies to each other,
It may be made of wood.
このようにして作った吸音材の吸音特性を測定したとこ
ろ、第４図の様な結果が得られた。When the sound absorbing properties of the sound absorbing material made in this manner were measured, the results shown in FIG. 4 were obtained.
この図から明らかなように、ごく一部の周波数領域を除
き１本発明に係る板状体の方が、従来の市販されている
金属屑焼結吸音材よりも吸音率が格段に優れている。As is clear from this figure, the plate-shaped body according to the present invention has a much better sound absorption coefficient than the conventional commercially available sintered metal scrap sound absorbing material except for a very small frequency range. .
支五舅ユ
前記第１実施例において、混線材を型枠内に充填する際
に、金網（図示せず）を中間層として挿入した。In the first embodiment, a wire mesh (not shown) was inserted as an intermediate layer when filling the formwork with the cross-wire material.
その後、第１実施例におけると同様にして吸音材を作製
した。Thereafter, a sound absorbing material was produced in the same manner as in the first example.
なお１本発明において、スラグの粒子の大きさは、最大
で５麿■３となるように粗砕すると必然的に１■■３１
１度のものが生ずるものであり。In addition, in the present invention, when the slag particle size is coarsely crushed to a maximum of 5 mm and 3 mm, the size of the slag particles inevitably becomes 1 mm and 31 mm.
It is something that occurs once.
１ ａｍ”より小さい粒子は吸音材としての多孔性を阻
害するので除去し、また５■３程度以上のものは、結合
性あるいは外観を損ねるので除去するのが好ましい。Particles smaller than 1 am'' are preferably removed because they impede the porosity of the sound absorbing material, and particles larger than about 5×3 are preferably removed because they impair bonding properties or appearance.
また、熱硬化性粉末レジン、灯油などの添加量は、該熱
硬化性粉末レジンの種別による接着能の大小、混練時の
粘性などによって種々選択。Further, the amount of the thermosetting powder resin, kerosene, etc. to be added is selected depending on the adhesive ability of the type of the thermosetting powder resin, the viscosity during kneading, etc.
決定されるものであり、現在市販されている熱硬化性粉
末レジンを使用する限りでは１機能面及びコスト面で１
．５〜１５重量％及び０．２〜２．０重量％の範囲が好
ましいものである。As long as currently commercially available thermosetting powder resins are used, it is 1 in terms of functionality and cost.
．． Preferred ranges are 5-15% by weight and 0.2-2.0% by weight.
加熱温度も前記市販の熱硬化性粉末レジンの種別によっ
て異なり、実用上は１５０℃〜３５０℃の範囲内で選択
、決定される。The heating temperature also varies depending on the type of the commercially available thermosetting powder resin, and is practically selected and determined within the range of 150°C to 350°C.
他方、加圧力は、１５ｋｇ／ｃ１１２以下では成形不十
分となるし、５０ ｋｇ ／ ｃｓ ’以上では消費動
力の無駄が生じるので、実用上は１５〜５０ｋｇ／ａｍ
２の範囲で選択される。On the other hand, if the pressurizing force is less than 15 kg/cs', forming will be insufficient, and if it is more than 50 kg/cs', power consumption will be wasted, so in practice it should be 15 to 50 kg/am.
Selected within the range of 2.
また、加圧時間は、スラグを成形し得る時間であれば足
り、実用上は５〜１５秒で成形が完了する。Further, the pressurizing time is sufficient as long as it is enough to mold the slag, and in practical terms, molding is completed in 5 to 15 seconds.
本領１の発明に係る吸音材は１以上のように。 The sound absorbing material according to the invention of main point 1 is like 1 or more.
１〜５１の大きさに粗砕されたスラグ８０〜９８重量％
、熱硬化性粉末レジン１．５〜１５重量％。80-98% by weight of slag crushed to a size of 1-51
, 1.5-15% by weight of thermosetting powder resin.
灯油０．２〜２．０重量％が混練され、加圧力１５〜５
０ ｋｇ／ ｃｙａ２．加圧時間５〜１５秒の条件の下
にプレスされ、温度１５０〜３５０℃で加熱成形されて
なるので、従来の金属粉を用いたものに比し、表面が融
着状になることがなく、板状体の全体にわたり多孔性を
有することとなって優れた吸音特性を発揮するものであ
る。Kerosene 0.2 to 2.0% by weight is kneaded, and the pressing force is 15 to 5%.
0 kg/cya2. Since it is pressed under conditions of pressure time of 5 to 15 seconds and heat-formed at a temperature of 150 to 350 degrees Celsius, the surface does not become fused compared to those using conventional metal powder. , the entire plate-like body has porosity and exhibits excellent sound absorption properties.
また、金属粉を用いたものと比べ、吸音材を軽量化する
ことができ、錆を発生することもない。Furthermore, compared to those using metal powder, the sound absorbing material can be made lighter and does not rust.
また１本第２の発明に係る吸音材は、板状に成形され、
中間に金網が介装されてなるので。Further, the sound absorbing material according to the second invention is formed into a plate shape,
Because there is a wire mesh interposed in the middle.
機械的強度優れ１例えば工場の壁材として使用して有益
なるものである。Excellent mechanical strength 1 It is useful for use as a wall material in factories, for example.
更に１本第１及びＷ２の発明において、吸音材の重量の
大部分を占める部分を産業廃棄物であるスラグで構成す
るので、低度にて吸音材をＷｉ造することができるもの
であり、しかもスラグの大きさ、スラグや熱硬化性粉末
レジン、灯油等の量、加圧力、加熱温度などを本発明の
範囲に選択すると、吸音効果の良い吸音材を最も低いコ
ストで短時間に成形できる効果がある。Furthermore, in the first and W2 inventions, since the majority of the weight of the sound absorbing material is composed of slag, which is an industrial waste, the sound absorbing material can be manufactured at a low level, Furthermore, by selecting the size of slag, the amount of slag, thermosetting powder resin, kerosene, etc., pressing force, heating temperature, etc. within the range of the present invention, a sound absorbing material with good sound absorbing effect can be formed in the shortest time at the lowest cost. effective.
図は本発明の実施例を示し、第１図は吸音材の内部構造
を断面として示した模式図１ｍ２図は枠材の部分切欠斜
視図、第３図は板状に成形され四囲に枠材をはめ込まれ
た吸音材の斜視図。
第４図は吸音材の吸音率を従来のものと対比して示すグ
ラフである。
１ニスラグの破砕粒子、２：熱硬化性粉末レジン、３：
空隙、４：枠材、５：板状体、６： 露出面。The figures show an embodiment of the present invention. Fig. 1 is a schematic cross-sectional view of the internal structure of the sound absorbing material. Fig. 1m2 is a partially cutaway perspective view of the frame material, and Fig. 3 is a plate-shaped structure with the frame material surrounding the four sides. A perspective view of the sound absorbing material fitted with the. FIG. 4 is a graph showing the sound absorption coefficient of the sound absorbing material in comparison with that of a conventional sound absorbing material. 1: Crushed particles of Nislag, 2: Thermosetting powder resin, 3:
void, 4: frame material, 5: plate-shaped body, 6: exposed surface.
Claims (1)
９８重量％、熱硬化性粉末レジン １．５〜１５重量％、灯油０．２〜２．０重量％が混練
され、加圧力１５〜５０ｋｇ／ｃｍ＾２、加圧時間５〜
１５秒の条件の下にプレスされ、温度１５０〜３５０℃
で加熱成形されてなる吸音材。 ２、板状に成形され、中間に金網が介装された特許請求
の範囲第１項記載の吸音材。[Claims] 1. Slag 80~ roughly crushed to a size of 1~5mm^3
98% by weight, thermosetting powder resin 1.5-15% by weight, and kerosene 0.2-2.0% by weight are kneaded, pressure is 15-50 kg/cm^2, and pressing time is 5-50%.
Pressed under the conditions of 15 seconds, temperature 150-350℃
A sound-absorbing material made by heating and molding. 2. The sound absorbing material according to claim 1, which is formed into a plate shape and has a wire mesh interposed in the middle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1022357A JPH02204353A (en) | 1989-01-31 | 1989-01-31 | Sound absorbing material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1022357A JPH02204353A (en) | 1989-01-31 | 1989-01-31 | Sound absorbing material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH02204353A true JPH02204353A (en) | 1990-08-14 |
Family
ID=12080388
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP1022357A Pending JPH02204353A (en) | 1989-01-31 | 1989-01-31 | Sound absorbing material |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH02204353A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04191800A (en) * | 1990-11-27 | 1992-07-10 | Mitsubishi Heavy Ind Ltd | Sound absorbing material |
| AU671162B2 (en) * | 1992-12-04 | 1996-08-15 | Resin Sands (S.A.) Pty Ltd | Building component |
| KR100402484B1 (en) * | 2001-02-28 | 2003-10-22 | 최연왕 | Manufacturing method of light weight aggregate making use of waste-pet bottle and blast furnace powdered slag |
-
1989
- 1989-01-31 JP JP1022357A patent/JPH02204353A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04191800A (en) * | 1990-11-27 | 1992-07-10 | Mitsubishi Heavy Ind Ltd | Sound absorbing material |
| AU671162B2 (en) * | 1992-12-04 | 1996-08-15 | Resin Sands (S.A.) Pty Ltd | Building component |
| KR100402484B1 (en) * | 2001-02-28 | 2003-10-22 | 최연왕 | Manufacturing method of light weight aggregate making use of waste-pet bottle and blast furnace powdered slag |
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