JPH0254815B2 - - Google Patents

Info

Publication number: JPH0254815B2
Authority: JP; Japan
Prior art keywords: trans; liquid crystal; fluoroacetophenone; added; fluorobenzene
Prior art date: 1983-04-18
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP6818883A

Other languages

English (en)

Japanese (ja)

Other versions

JPS59193843A (ja

Inventor

Shigeru Sugimori

Tetsuhiko Kojima

Yasuyuki Goto

Toyoshiro Isoyama

Kazunori Nigorikawa

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

JNC Corp

Original Assignee

Chisso Corp

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1983-04-18

Filing date

1983-04-18

Publication date

1990-11-22

1983-04-18 Application filed by Chisso Corp filed Critical Chisso Corp

1983-04-18 Priority to JP6818883A priority Critical patent/JPS59193843A/ja

1984-02-16 Priority to US06/580,628 priority patent/US4536321A/en

1984-02-20 Priority to DE8484301072T priority patent/DE3462249D1/de

1984-02-20 Priority to EP84301072A priority patent/EP0119756B1/de

1984-11-02 Publication of JPS59193843A publication Critical patent/JPS59193843A/ja

1990-11-22 Publication of JPH0254815B2 publication Critical patent/JPH0254815B2/ja

Status Granted legal-status Critical Current

Links

239000004973 liquid crystal related substance Substances 0.000 claims description 14
239000000203 mixture Substances 0.000 claims description 8
YOMBUJAFGMOIGS-UHFFFAOYSA-N 2-fluoro-1-phenylethanone Chemical class FCC(=O)C1=CC=CC=C1 YOMBUJAFGMOIGS-UHFFFAOYSA-N 0.000 claims description 4
125000000217 alkyl group Chemical group 0.000 claims description 3
125000004432 carbon atom Chemical group C* 0.000 claims description 3
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 12
IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 9
150000001875 compounds Chemical class 0.000 description 8
WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 6
239000000463 material Substances 0.000 description 6
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 4
VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 4
PYLWMHQQBFSUBP-UHFFFAOYSA-N monofluorobenzene Chemical compound FC1=CC=CC=C1 PYLWMHQQBFSUBP-UHFFFAOYSA-N 0.000 description 4
-1 4-substituted cyclohexanone Chemical class 0.000 description 3
QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 3
FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
239000011777 magnesium Substances 0.000 description 3
229910052749 magnesium Inorganic materials 0.000 description 3
230000007935 neutral effect Effects 0.000 description 3
CHKVPAROMQMJNQ-UHFFFAOYSA-M potassium bisulfate Chemical compound [K+].OS([O-])(=O)=O CHKVPAROMQMJNQ-UHFFFAOYSA-M 0.000 description 3
229910000343 potassium bisulfate Inorganic materials 0.000 description 3
239000000126 substance Substances 0.000 description 3
YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 3
238000005406 washing Methods 0.000 description 3
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
239000007868 Raney catalyst Substances 0.000 description 2
NPXOKRUENSOPAO-UHFFFAOYSA-N Raney nickel Chemical compound [Al].[Ni] NPXOKRUENSOPAO-UHFFFAOYSA-N 0.000 description 2
229910000564 Raney nickel Inorganic materials 0.000 description 2
WETWJCDKMRHUPV-UHFFFAOYSA-N acetyl chloride Chemical compound CC(Cl)=O WETWJCDKMRHUPV-UHFFFAOYSA-N 0.000 description 2
239000012346 acetyl chloride Substances 0.000 description 2
239000003054 catalyst Substances 0.000 description 2
238000001816 cooling Methods 0.000 description 2
239000007788 liquid Substances 0.000 description 2
ZIULUUPYEQPRAQ-UHFFFAOYSA-L magnesium;fluorobenzene;dibromide Chemical compound [Mg+2].[Br-].[Br-].FC1=CC=CC=C1 ZIULUUPYEQPRAQ-UHFFFAOYSA-L 0.000 description 2
238000004519 manufacturing process Methods 0.000 description 2
238000002844 melting Methods 0.000 description 2
230000008018 melting Effects 0.000 description 2
QDFKKJYEIFBEFC-UHFFFAOYSA-N 1-bromo-3-fluorobenzene Chemical compound FC1=CC=CC(Br)=C1 QDFKKJYEIFBEFC-UHFFFAOYSA-N 0.000 description 1
QWHCPRHASHNSDA-UHFFFAOYSA-N 4-heptylcyclohexan-1-one Chemical compound CCCCCCCC1CCC(=O)CC1 QWHCPRHASHNSDA-UHFFFAOYSA-N 0.000 description 1
XXUSEPRYHRDKFV-CTYIDZIISA-N C1C[C@@H](CCC)CC[C@@H]1C1=CC=C(C#N)C=C1 Chemical compound C1C[C@@H](CCC)CC[C@@H]1C1=CC=C(C#N)C=C1 XXUSEPRYHRDKFV-CTYIDZIISA-N 0.000 description 1
FURZYCFZFBYJBT-JCNLHEQBSA-N C1C[C@@H](CCCCC)CC[C@@H]1C1=CC=C(C#N)C=C1 Chemical compound C1C[C@@H](CCCCC)CC[C@@H]1C1=CC=C(C#N)C=C1 FURZYCFZFBYJBT-JCNLHEQBSA-N 0.000 description 1
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
239000008186 active pharmaceutical agent Substances 0.000 description 1
125000004429 atom Chemical group 0.000 description 1
238000009835 boiling Methods 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
238000010531 catalytic reduction reaction Methods 0.000 description 1
238000002156 mixing Methods 0.000 description 1
229910052757 nitrogen Inorganic materials 0.000 description 1
239000012299 nitrogen atmosphere Substances 0.000 description 1
230000003287 optical effect Effects 0.000 description 1
238000001953 recrystallisation Methods 0.000 description 1
238000010992 reflux Methods 0.000 description 1
239000002904 solvent Substances 0.000 description 1
238000003756 stirring Methods 0.000 description 1
230000007704 transition Effects 0.000 description 1

Landscapes

Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Liquid Crystal Substances (AREA)

JP6818883A 1983-02-18 1983-04-18 フルオロアセトフエノン誘導体 Granted JPS59193843A (ja)

Priority Applications (4)

Application Number	Priority Date	Filing Date	Title
JP6818883A JPS59193843A (ja)	1983-04-18	1983-04-18	フルオロアセトフエノン誘導体
US06/580,628 US4536321A (en)	1983-02-18	1984-02-16	Fluorobenzene derivatives and liquid crystal compositions containing the same
DE8484301072T DE3462249D1 (en)	1983-02-18	1984-02-20	Fluorobenzene derivatives and liquid crystal compositions containing the same
EP84301072A EP0119756B1 (de)	1983-02-18	1984-02-20	Fluorbenzolderivate und sie enthaltende flüssigkristalline Zusammensetzungen

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP6818883A JPS59193843A (ja)	1983-04-18	1983-04-18	フルオロアセトフエノン誘導体

Publications (2)

Publication Number	Publication Date
JPS59193843A JPS59193843A (ja)	1984-11-02
JPH0254815B2 true JPH0254815B2 (de)	1990-11-22

Family

ID=13366553

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP6818883A Granted JPS59193843A (ja)	1983-02-18	1983-04-18	フルオロアセトフエノン誘導体

Country Status (1)

Country	Link
JP (1)	JPS59193843A (de)

1983
- 1983-04-18 JP JP6818883A patent/JPS59193843A/ja active Granted

Also Published As

Publication number	Publication date
JPS59193843A (ja)	1984-11-02

Publication	Publication Date	Title
JPH0322855B2 (de)	1991-03-27
JPS64373B2 (de)	1989-01-06
JPH0684339B2 (ja)	1994-10-26	シクロヘキサン誘導体
JPS6239136B2 (de)	1987-08-21
JPH04506815A (ja)	1992-11-26	フェニルシクロヘキサン化合物、および液晶相
JPH0253415B2 (de)	1990-11-16
JPS6313411B2 (de)	1988-03-25
JPS644497B2 (de)	1989-01-25
US5055220A (en)	1991-10-08	Dicyclohexylethylene derivatives
JPH01272537A (ja)	1989-10-31	シクロヘキサン誘導体
JPS6313424B2 (de)	1988-03-25
JPS5916840A (ja)	1984-01-28	３−フルオロ−４−置換−〔トランス−４′−（トランス−４″−アルキルシクロヘキシル）シクロヘキシル〕ベンゼン
JPH0254815B2 (de)	1990-11-22
JPS6353177B2 (de)	1988-10-21
JPH0359050B2 (de)	1991-09-09
JPS642112B2 (de)	1989-01-13
JPS6332051B2 (de)	1988-06-28
JPH0229055B2 (ja)	1990-06-27	Jishikurohekishirubenzenjudotai
JPS6361292B2 (de)	1988-11-28
JPH0359884B2 (de)	1991-09-12
JPH0233698B2 (ja)	1990-07-30	Futsusoganjushikurohekishiruansokukosanfueniruesuterujudotai
JPH0121817B2 (de)	1989-04-24
JP2508166B2 (ja)	1996-06-19	新規シクロヘキセニルシクロヘキサン誘導体
JPS5944330A (ja)	1984-03-12	３，４−ジメチル−ビシクロヘキシルベンゼン誘導体
JPS58194822A (ja)	1983-11-12	４−置換−４′↓−〔トランス−４″−（トランス−４′′′−置換シクロヘキシル）シクロヘキシル〕ビフエニル