JPH0458868A - Production of aseptic packed liquid stock - Google Patents
Production of aseptic packed liquid stockInfo
- Publication number
- JPH0458868A JPH0458868A JP2168442A JP16844290A JPH0458868A JP H0458868 A JPH0458868 A JP H0458868A JP 2168442 A JP2168442 A JP 2168442A JP 16844290 A JP16844290 A JP 16844290A JP H0458868 A JPH0458868 A JP H0458868A
- Authority
- JP
- Japan
- Prior art keywords
- liquid stock
- amount
- oxygen
- sterilization
- stock
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000015073 liquid stocks Nutrition 0.000 title claims abstract 14
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000001301 oxygen Substances 0.000 claims abstract description 26
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 230000001954 sterilising effect Effects 0.000 claims abstract description 17
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 15
- 239000008213 purified water Substances 0.000 claims abstract description 6
- 239000012153 distilled water Substances 0.000 claims abstract description 5
- 238000007789 sealing Methods 0.000 claims abstract 5
- 238000011049 filling Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 3
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims 1
- 239000003456 ion exchange resin Substances 0.000 claims 1
- 229920003303 ion-exchange polymer Polymers 0.000 claims 1
- 239000000796 flavoring agent Substances 0.000 abstract description 12
- 235000019634 flavors Nutrition 0.000 abstract description 11
- 238000004806 packaging method and process Methods 0.000 abstract description 9
- 235000019640 taste Nutrition 0.000 abstract description 7
- 241000269851 Sarda sarda Species 0.000 abstract description 5
- 238000012856 packing Methods 0.000 abstract 3
- 239000003205 fragrance Substances 0.000 abstract 1
- 235000014347 soups Nutrition 0.000 description 12
- 230000006866 deterioration Effects 0.000 description 9
- 238000011156 evaluation Methods 0.000 description 9
- 239000007788 liquid Substances 0.000 description 7
- 238000003860 storage Methods 0.000 description 7
- 239000008399 tap water Substances 0.000 description 6
- 235000020679 tap water Nutrition 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 239000008609 bushi Substances 0.000 description 3
- 238000010411 cooking Methods 0.000 description 3
- 238000010790 dilution Methods 0.000 description 3
- 239000012895 dilution Substances 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000011282 treatment Methods 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- 241000555825 Clupeidae Species 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 235000019512 sardine Nutrition 0.000 description 2
- RQFCJASXJCIDSX-UHFFFAOYSA-N 14C-Guanosin-5'-monophosphat Natural products C1=2NC(N)=NC(=O)C=2N=CN1C1OC(COP(O)(O)=O)C(O)C1O RQFCJASXJCIDSX-UHFFFAOYSA-N 0.000 description 1
- 241000251468 Actinopterygii Species 0.000 description 1
- 241000512259 Ascophyllum nodosum Species 0.000 description 1
- 239000004278 EU approved seasoning Substances 0.000 description 1
- GRSZFWQUAKGDAV-KQYNXXCUSA-N IMP Chemical compound O[C@@H]1[C@H](O)[C@@H](COP(O)(O)=O)O[C@H]1N1C(NC=NC2=O)=C2N=C1 GRSZFWQUAKGDAV-KQYNXXCUSA-N 0.000 description 1
- GRSZFWQUAKGDAV-UHFFFAOYSA-N Inosinic acid Natural products OC1C(O)C(COP(O)(O)=O)OC1N1C(NC=NC2=O)=C2N=C1 GRSZFWQUAKGDAV-UHFFFAOYSA-N 0.000 description 1
- 240000000599 Lentinula edodes Species 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 235000019606 astringent taste Nutrition 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000011437 continuous method Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- GYOZYWVXFNDGLU-XLPZGREQSA-N dTMP Chemical compound O=C1NC(=O)C(C)=CN1[C@@H]1O[C@H](COP(O)(O)=O)[C@@H](O)C1 GYOZYWVXFNDGLU-XLPZGREQSA-N 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 235000006694 eating habits Nutrition 0.000 description 1
- 235000019688 fish Nutrition 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 description 1
- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 239000004223 monosodium glutamate Substances 0.000 description 1
- 238000005464 sample preparation method Methods 0.000 description 1
- 238000010187 selection method Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Landscapes
- Basic Packing Technique (AREA)
- Seasonings (AREA)
Abstract
Description
【発明の詳細な説明】
[産業上の利用分野コ
本発明は、だし本来の香り・風味・味を保持した、長期
常温流通可能なアセブチイック包装液体だしの製造法に
関する。[Detailed Description of the Invention] [Industrial Field of Application] The present invention relates to a method for producing an acebutic packaged liquid soup stock that retains the original aroma, flavor, and taste of the stock and can be distributed at room temperature for a long period of time.
[従来の技術とその問題点]
近年、食生活の変化に伴い調理、料理は簡便化傾向にあ
り、料理、調理の基本であるだしにおいても、だしを取
る手間のかからない液体の和風だし、洋風スープストッ
ク等が数多く市販されている。常温流通品ではレトルト
殺菌品、アセブチイック包装品、低温流逸品では冷凍品
、チルド品などがあるが、レトルト殺菌品は殺菌による
風味劣化、アセブチイック包装品では保存中の風味劣化
等の問題点がある。また低温流逸品では流通・保管時の
コスト高、冷凍品はさらに解凍の手間がかかるといった
問題点がある。[Conventional techniques and their problems] In recent years, cooking has become simpler due to changes in eating habits, and the basics of cooking and cooking, such as dashi, are becoming more and more popular. There are many kinds of soup stock etc. on the market. Room-temperature products include retort sterilized products and acebutically packaged products, and low-temperature products include frozen products and chilled products. However, retort sterilized products have problems such as flavor deterioration due to sterilization, and acetic packaged products have problems such as flavor deterioration during storage. . In addition, low-temperature products have the problem of high costs during distribution and storage, and frozen products require more time and effort to thaw.
[問題点を解決するための手段]
本発明者らは、上記問題点について鋭意検討を重ねた結
果、だし本来の香り・風味・味を保持し簡便であり、さ
らには常温保存時の香り・風味の劣化が著しく小さく、
長期常温流通可能な液体だしの製造法を発明するに至っ
た。つまり本発明は、抽出しただしの溶存酸素量を予め
低減させた後殺菌し、充填するに際し、容器内酸素量を
低レベルに制限するアセブチイック包装液体だしの製造
法に関するものである。まずだしの抽出であるが、抽出
用水について本発明者らは、水道水に比べ精製水で抽出
しただしは、だし素材本来の風味・味を有することを見
い出した。つまり精製水により抽出しただしは、水道水
で抽出しただしに発現するえぐ味・渋味がなく、こく・
厚みに富み、いわば上質のだしと言える。ここで精製水
とは、蒸留、イオン交換等の処理をおこない、不純物を
極力除去した水のことである。だし原料としては鰹節、
宗田節、鯖節、鰺節、鰹節及びその他の節類、煮干、昆
布、椎茸等通常の和風だし素材、その他洋風・中華風だ
し素材を用いることができ、その形状としては粉末状、
粒状、薄片状、プロ・ツク状のいずれでもよい。抽出方
法は、バッチ方式、連続方式のいずれも用いることがで
き、フレッシュなだしの香りを得る場合には短時間抽出
、煮立てた香り・風味を得る場合には、長時間抽出が望
ましい。さらに精製水で抽出しただしに5’−TMP。[Means for Solving the Problems] As a result of intensive studies on the above-mentioned problems, the inventors of the present invention have found that the original aroma, flavor, and taste of dashi stock can be maintained and it is simple, and furthermore, the aroma and taste can be maintained even when stored at room temperature. Deterioration of flavor is extremely small,
This led to the invention of a method for producing liquid soup stock that can be distributed at room temperature for a long period of time. That is, the present invention relates to a method for producing an acetate-packaged liquid broth, in which the amount of dissolved oxygen in the extracted broth is reduced in advance, and then sterilized, and the amount of oxygen in the container is limited to a low level during filling. First, regarding the extraction of dashi stock, the present inventors have found that dashi stock extracted with purified water has the original flavor and taste of the dashi material, compared to tap water. In other words, dashi extracted with purified water does not have the harsh and astringent taste that occurs in dashi extracted with tap water, and has a rich, rich flavor.
It is thick and can be said to be a high-quality soup stock. Purified water here refers to water that has been subjected to treatments such as distillation and ion exchange to remove impurities as much as possible. Dashi ingredients include bonito flakes,
Usual Japanese-style dashi ingredients such as Muneta-bushi, mackerel-bushi, mackerel-bushi, bonito flakes, other dried fish, dried sardines, kelp, shiitake mushrooms, and other Western-style and Chinese-style dashi ingredients can be used, and their shapes include powdered,
It may be in the form of granules, flakes, or blocks. As for the extraction method, either a batch method or a continuous method can be used, and it is preferable to extract for a short time to obtain the aroma of fresh soup stock, and to extract for a long time to obtain the aroma and flavor of boiled soup stock. Further, 5'-TMP was extracted with purified water.
5’−C,MP、グルタミン酸ナトリウムを添加するこ
とにより、だし本来の呈味質を維持しつつ呈味力価を上
げることも可能である。By adding 5'-C, MP, and monosodium glutamate, it is also possible to increase the taste titer while maintaining the original flavor quality of the soup stock.
抽出しただしを常温流通させるためには、殺菌・充填・
包装を行う必要がある。ここで熱によるだしの品質劣化
を極力避けるためには、連続式高温短時間殺菌機である
プレート式熱交換器、掻き取り式熱交換器等による殺菌
及びアセブチイック充填・包装を組み合わせて行うこと
が好ましい。アセブチイック充填・包装は、だし及び容
器を個々に殺菌後、無菌的に充填・包装をおこなうので
、レトルト殺菌のようにだしに余分な熱負荷がかからず
、殺菌時の品質劣化を招きにくい。また殺菌前のだしの
溶存酸素量は、脱気処理等により、できるだけ低レベル
に抑えることが望ましく、具体的にはi ppm以下、
好ましくは、0.5 ppm以下とする。本処理により
、殺菌による品質劣化がないたしが得られる。さらに本
発明者らは、だし充填時、液量に対する容器内酸素量を
3pplIl、好ましくは0.5ρρm以下に抑えるこ
とにより、従来の液体だし及び関連の液体調味料に比べ
保存時の品質劣化を飛躍的に低減することができること
を見い出した。容器内酸素量とは、だしそのものの溶存
酸素量と容器内ヘッドスペース酸素量の総量である。容
器内酸素量が3 ppmを越えるものについては保存時
に、だしの香り・風味が急速に弱くなり異臭が発現し品
質劣化を招く。容器内酸素量を低レベルに抑えるために
は、まずだしの殺菌前にデアレータ−等により脱気し、
だしの溶存酸素量を除去する。本工程は前述のとおり、
殺菌時の品質劣化をも防止できる。さらにアセブチイッ
ク充填・包装時、容器内にヘッドスペース空気が残存す
る場合、不活性ガスである窒素ガス、炭酸ガスまたはそ
の混合ガス等によりヘッドスペース空気との置換を施し
、容器内酸素を除去する必要がある。In order to distribute the extracted stock at room temperature, sterilization, filling, and
It is necessary to do packaging. In order to avoid deterioration of the quality of the stock as much as possible due to heat, it is recommended to combine sterilization using a continuous high-temperature short-time sterilizer such as a plate heat exchanger or a scraping-type heat exchanger, as well as acetic filling and packaging. preferable. In acetic filling and packaging, the stock and containers are individually sterilized and then filled and packaged aseptically, so unlike retort sterilization, unnecessary heat load is not applied to the stock, and quality deterioration during sterilization is less likely to occur. In addition, it is desirable to keep the amount of dissolved oxygen in the stock as low as possible by deaeration treatment, etc. before sterilization, specifically, ippm or less,
Preferably, it is 0.5 ppm or less. Through this treatment, it is possible to obtain sashimi with no quality deterioration due to sterilization. Furthermore, the present inventors have found that by suppressing the amount of oxygen in the container to 3pplIl, preferably 0.5ρρm or less relative to the liquid volume when filling the soup stock, quality deterioration during storage is reduced compared to conventional liquid soup stock and related liquid seasonings. We have found that this can be dramatically reduced. The amount of oxygen in the container is the total amount of dissolved oxygen in the soup stock itself and the amount of headspace oxygen in the container. If the amount of oxygen in the container exceeds 3 ppm, the aroma and flavor of the soup stock will rapidly weaken during storage, and an off-flavor will develop, leading to quality deterioration. In order to keep the amount of oxygen in the container to a low level, first, before sterilizing the stock, degas it using a deaerator, etc.
Removes the amount of dissolved oxygen in the soup stock. As mentioned above, this process
It can also prevent quality deterioration during sterilization. Furthermore, if headspace air remains in the container during acetic filling and packaging, it is necessary to replace the headspace air with an inert gas such as nitrogen gas, carbon dioxide gas, or a mixture thereof to remove oxygen in the container. There is.
以下に実施例を示す。Examples are shown below.
実施例1゜
蒸留水、水道水各100重量部に粗砕鰹節30重量部を
それぞれ加え、ジャケット釜で90°Cで30分間を攪
拌抽出後、濾過した。得られただし100重景部に5’
−TMPを0.5重量部加え、脱気後、プレート式熱
交換器にて127°Cで一60秒間殺菌を行なった。さ
らに0.2 L液中シール型のアセブチイック充填・包
装を行い、得られた試作品の呈味質を評価した。各試作
品の容器内にヘッドスペースはなく、溶存酸素量はいず
れも0.lppmであった。サンプル調製、評価法は以
下のとおりとした。Example 1 30 parts by weight of coarsely crushed bonito flakes were added to 100 parts by weight each of distilled water and tap water, and the mixture was stirred and extracted in a jacket pot at 90°C for 30 minutes, and then filtered. However, 5' in the 100-layered part
-0.5 parts by weight of TMP was added, and after deaeration, sterilization was performed at 127°C for 160 seconds using a plate heat exchanger. Furthermore, acetic filling and packaging of a 0.2 L liquid submerged seal type was performed, and the taste quality of the obtained prototype product was evaluated. There is no head space in the container of each prototype, and the amount of dissolved oxygen is 0. It was lppm. Sample preparation and evaluation methods were as follows.
(1)サンプル
No、1;水道水による抽出だし試作品の、水道水によ
る5倍希釈液
No、2 ;水道水による抽出だし試作品の、蒸留水に
よる5倍希釈液
No、3;蒸留水による抽出だし試作品の、蒸留水によ
る5倍希釈液
(2)評価法
1)訓練されたパネル20名による2点提示選択法
2)評価項目は下表参照
評価結果
11剰Lノし サンプルNo、1のi・実施例2゜
向流抽出機にて、イオン交換水100重量部を粉砕煮干
25重量部に85°Cで20分接触させ、抽出後、濾過
した。得られただしをデアレータ−で脱気後、溶存酸素
量が0.2.4.2ppmのだしとした。その後プレー
ト式熱交換器にて135°Cで10秒間殺菌を行なった
後、さらに0.2L液中シール型のアセブチイック充填
・包装を行ない、得られた試作品を評価した。各試作品
の容器内にヘッドスペースはなく、溶存酸素量はO,i
ppm(9ンブルNo、1) 、4.0ppm(サン
プルNo、2)であった。評価は、各試作品ともイオン
交換水での7倍希釈液とし、対照は、未殺菌品とし、実
施した。評価法は実施例1.と同様とした。(1) Sample No. 1; 5-fold dilution with tap water of a prototype extracted with tap water; No. 2; 5-fold dilution with distilled water of a prototype extracted with tap water; 3; Distilled water (2) Evaluation method 1) Two-point presentation selection method by a trained panel of 20 people 2) For evaluation items, see the table below.Evaluation results 11.Sample No. , 1, Example 2 In a countercurrent extractor, 100 parts by weight of ion-exchanged water was brought into contact with 25 parts by weight of pulverized dried sardines at 85°C for 20 minutes, and after extraction, the mixture was filtered. The obtained stock was degassed using a dealerator, and then stock with a dissolved oxygen amount of 0.2.4.2 ppm was prepared. After that, it was sterilized for 10 seconds at 135°C in a plate heat exchanger, and then acetic filling and packaging of a 0.2L submerged seal type was performed, and the obtained prototype product was evaluated. There is no headspace inside the container of each prototype, and the amount of dissolved oxygen is O,i
ppm (9 sample No. 1) and 4.0 ppm (sample No. 2). The evaluation was carried out using a 7-fold dilution of each prototype with ion-exchanged water, and an unsterilized product as a control. The evaluation method is Example 1. The same is true.
実施例3゜
向流抽出機にて、イオン交換水100重量部を粗砕鰹節
35重量部に90°Cで30分接触させ、抽出後、濾過
した。得られただし100重量部に5’−IMPを0.
2重量部加え、デアレータ−で脱気し、溶存酸素量を0
.1 ppmとした。その後、プレート式熱交換器にて
130’Cで30秒間殺菌を行ない、無菌的に1.8L
減菌アルミ箔バツグに充填後、容器内酸素量を調整する
ため窒素ガスにてヘッドスペース空気を置換し、密封し
た。得られた各試作品の容器内酸素量は、0.2.2.
5.5.2ppmであり、これらの保存安定性を評価し
た。Example 3 In a countercurrent extractor, 100 parts by weight of ion-exchanged water was brought into contact with 35 parts by weight of coarsely crushed bonito flakes at 90°C for 30 minutes, and after extraction, the mixture was filtered. However, 0.5'-IMP was added to 100 parts by weight of the obtained product.
Add 2 parts by weight and degas with a deaerator to reduce the amount of dissolved oxygen to 0.
.. It was set to 1 ppm. After that, sterilize at 130'C for 30 seconds in a plate heat exchanger to aseptically remove 1.8L.
After filling into sterilized aluminum foil bags, the headspace air was replaced with nitrogen gas to adjust the amount of oxygen in the container, and the bag was sealed. The amount of oxygen in the container of each prototype obtained was 0.2.2.
5.5.2 ppm, and their storage stability was evaluated.
保存条件、評価法は以下のとおりとした。Storage conditions and evaluation methods were as follows.
(1)保存条件 1)温度 24°C2)相対湿
度 78%
(2)サンプル;No、1;容器内酸素量0.2ppm
試作品N o 、2 ;容器内酸素量2.5ppm試作
品No、3;容器内酸素量5.2ppm試作品(3)評
価法 ;訓練されたパネル5名により、各サンプルのイ
オン交換水による10
倍希釈液を官能評価した。(1) Storage conditions 1) Temperature 24°C 2) Relative humidity 78% (2) Sample; No. 1; Oxygen content in container 0.2 ppm
Prototype No. 2; Oxygen content in the container 2.5 ppm Prototype No. 3; Oxygen content in the container 5.2 ppm Prototype (3) Evaluation method; Five trained panels evaluated each sample using ion-exchanged water. The 10-fold diluted solution was subjected to sensory evaluation.
対照は、 上記と同一条件下で抽出した直後 のだしとした。The contrast is Immediately after extraction under the same conditions as above It was laid out.
(4)結果(4) Results
Claims (2)
密封するに際し、殺菌前に液体だし中の溶存酸素量を減
少させ、かつ殺菌後の充填・密封工程において最終的に
容器内酸素量を内容液体だしの3ppm以下とすること
を特徴とする液体だしの製造法。(1) Sterilize the liquid stock and fill it into containers under aseptic conditions.
A liquid stock characterized by reducing the amount of dissolved oxygen in the liquid stock before sterilization when sealing it, and finally reducing the amount of oxygen in the container to 3 ppm or less of the liquid stock content in the filling and sealing process after sterilization. manufacturing method.
理水等の精製水を用いることを特徴とする請求項1記載
のだしの製造法。(2) The method for producing dashi according to claim 1, characterized in that purified water such as distilled water or water treated with an ion exchange resin is used as the water for extracting the dashi.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2168442A JP2924105B2 (en) | 1990-06-28 | 1990-06-28 | Manufacturing method of aseptic packaging liquid stock |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2168442A JP2924105B2 (en) | 1990-06-28 | 1990-06-28 | Manufacturing method of aseptic packaging liquid stock |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0458868A true JPH0458868A (en) | 1992-02-25 |
| JP2924105B2 JP2924105B2 (en) | 1999-07-26 |
Family
ID=15868195
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2168442A Expired - Lifetime JP2924105B2 (en) | 1990-06-28 | 1990-06-28 | Manufacturing method of aseptic packaging liquid stock |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP2924105B2 (en) |
-
1990
- 1990-06-28 JP JP2168442A patent/JP2924105B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JP2924105B2 (en) | 1999-07-26 |
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