JPH0477049B2 - - Google Patents
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- JPH0477049B2 JPH0477049B2 JP58185121A JP18512183A JPH0477049B2 JP H0477049 B2 JPH0477049 B2 JP H0477049B2 JP 58185121 A JP58185121 A JP 58185121A JP 18512183 A JP18512183 A JP 18512183A JP H0477049 B2 JPH0477049 B2 JP H0477049B2
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- Prior art keywords
- weight
- rolled
- strength
- cold
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Heat Treatment Of Sheet Steel (AREA)
Description
技術分野
この発明は、強度レベルが50kgf/mm2以上の高
張力冷延鋼板における、曲げ特性ならびに伸びフ
ランジ成形性の改善技術に関するものである。
背景技術
引張り強度が50kgf/mm2以上程度の高張力冷延
鋼板になると、一般に表面硬度が急激に上昇する
ため、プレス成形時に型かじりによつて表面にク
ラツクがはいり易く、曲げ割れや伸びフランジ割
れが発生し易いという問題があつた。またこの種
の鋼板は、強度の確保のためにSi,MnおよびP
などの強化元素を比較的多量に添加するので、非
金属介在物の生成量が多くなり易く、かような介
在物に起因した割れの発生頻度が高いところにも
問題を残していた。
発明の目的
この発明は、上記の諸問題を有利に解決するも
ので、プレス成形時においても曲げ割れや伸びフ
ランジ割れなどの発生がない、50kgf/mm2級以上
の高張力冷延鋼板の有利な製造方法を提案するこ
とを目的とする。
発明の構成
この発明は、プレス割れに関する綿密な研究の
末開発されたもので、所期した目的達成のために
は、鋼板表面に薄い脱炭層を形成させると共に、
不可避不純物中とくにS量を抑制することが、極
めて有効であることの知見に立脚する。
すなわちこの発明は、C:0.05〜0.20重量%
(以下単に%で示す)、Si:0.05〜1.50%、Nn:
1.00〜3.50%、P:0.020〜0.100%およびS:
0.010%以下を含有し、ときにはさらにNb:0.010
〜0.050%、Ti:0.010〜0.150%のうちから選んだ
一種又は二種を含み、残部は鉄および不可避的不
純物の組成になるスラブを、熱間圧延したのちコ
イルに巻取り、ついで冷間圧延を施してから再結
晶温度以上の温度範囲で連続焼鈍を施す一連の工
程よりなる高張力冷延鋼板の製造方法において、
熱間圧延に引続く巻取りを680℃を超え、850℃
以下の温度で行うことにより、鋼板表面に厚み1
〜200μmの脱炭層を形成させることを特徴とす
る、曲げ特性および伸びフランジ成形性に優れ
た、強度レベル50kgf/mm2以上の高張力冷延鋼板
の製造方法である。
以下この発明を具体的に説明する。
まずこの発明において鋼板の成分組成を上記の
範囲に限定した理由について説明する。
C:0.05〜0.20%
C量が、0.05%未満では、連続焼鈍後に引張り
強さ(T.S.)が低くなるため、その補償の意味で
Si,Mn,P,Ti,NbおよびVなどの強度元素
を大量に必要とする不利が生じ、一方0.20%を超
えるとスポツト溶接継手の疲労強度や静的強度が
低下するので、C含有量は0.05〜0.20%の範囲に
限定した。
S:0.010%以下
Si:0.05〜1.50%
Siは、曲げ性及び伸びフランジ性の改善に有効
に寄与するが、その効果が発揮されるのは0.05%
以上添加した場合であり、一方1.50%を超えて添
加された場合はその効果が飽和に達するだけでな
く、かえつて鋼が硬化し、熱間圧延や冷間圧延に
困難となるので、0.05〜1.50%の範囲に限定し
た。
Mn:1.00〜3.50%
Mnは、強度の向上に寄与する有用元素である
が、1.00%未満ではその添加効果に乏しく、一方
3.50%を超えると強度向上が飽和に達し、また熱
延母板が顕著に硬化し、とくに冷間圧延が困難と
なるので、1.00〜3.50%の範囲に限定した。
P:0.020〜0.100%
Pは、微量の添加で鋼の強化に有効に寄与する
有用元素であるが、0.020%未満ではその添加効
果に乏しく、一方0.100%を超えるとその効果が
飽和に達するだけでなく、偏析が顕在化し、加工
性が劣化するおそれが大きいので、0.020〜0.100
%の範囲に限定した。
Sが多量に含有されると、プレス成形時に伸び
割れや曲げ割れが発生するので、Sは極力低減す
ることが好ましいが、0.010%までなら許容でき
る。
さらにこの発明では、鋼の強化元素としてNb
及びTiのうちから選んだ一種又は二種を、下記
の範囲で添加することができる。
Nb:0.010〜0.050%
Nbは、微量の添加で効果的に鋼の強度を向上
させることができる元素であり、そのためには少
なくとも0.010%の添加を必要とするが、0.050%
を超えるとその効果は飽和に達するので、0.010
〜0.050%の範囲で添加するものとした。
Ti:0.010〜0.150%
Tiも、Nbと同様、微量の添加で効果的に鋼の
強度を向上させることができる元素であるが、
0.010%に満たないとその添加効果に乏しく、一
方0.150%を超えるとその効果は飽和に達するの
で、0.010〜0.150%の範囲で添加するものとし
た。
第1図に、C:0.08%、Si:1.10%、Mn:1.90
%、P:0.095%、Al:0.050%およびO:0.0021
%の他、Sを0.001から0.018%までの範囲にわた
つて変化させた、種々の成分組成になる鋼板のS
量と清浄度との関係について調べた結果を示す。
なお清浄度の測定は、JIS G 0555に準拠して行
つた。
同図より明らかなように、S量が0.010%を超
えると清浄度の急激な悪化を招いているが、清浄
度が悪くなるということは、曲げ割れや伸びフラ
ンジ割れが発生し易くなつたことを意味する。
さてこの発明では、鋼板表面に脱炭層を形成さ
せることが最大の特長であり、かような脱炭層の
形成によつて、50kgf/mm2級以上の高張力冷延鋼
板においても、そのプレス成形時に発生が懸念さ
れた曲げ割れや伸びフランジ割れの効果的な防止
が可能になつたのである。しかしながら脱炭層の
厚みが1μmに満たないと、軟質層の厚さが薄す
ぎるため曲げ性および型かじり性の改善効果に乏
しく、一方200μmを超えると目標とする強度が
得難くなるだけでなく、脱炭層を形成させるため
の処理時間が長くなるなど経済性も損うので、脱
炭層は1〜200μmの範囲に限定した。
かかる脱炭層の形成は、熱延後の巻取りを高温
で行い、熱延コイルの状態で表面に脱炭層を形成
させることにより行う。
なおこのとき、巻取り温度が680℃以下では、
鋼中Cの拡散速度が小さくなり、脱炭するのに好
ましいFeOがすぐにFe3O4に変態してしまうため
十分な脱炭層が形成されにくいので、巻取り温度
は680℃超とすることが必要である。また熱間圧
延の仕上げスタンド出側における温度は950〜850
℃程度であるので、その後の巻取温度の上限は工
業的に850℃以下で十分である。
実施例
以下この発明の実施例について説明する。
第1表に示した化学成分になる6種の鋼スラブ
を、熱間圧延したのち一旦コイルに巻取り、つい
で冷間圧延、連続焼鈍を施すことにより高張力冷
延鋼板を作成した。なお6種の鋼A〜Fのうち鋼
Eを除いた6種の鋼については、その製造過程に
おいて第1表に示したとおりの厚みの脱炭層を形
成させたが、かような脱炭層の形成は、
熱延後に720℃の高温で巻取ることによつて行
つた。なお比較例については、露点:10℃の焼鈍
雰囲気で連続焼鈍することにより、脱炭した。
ついで得られた各鋼板の機械的性質については
調査した。その結果を第1表に併記する。
なお降伏応力、引張り強度および伸びについて
は、JIS Z 2201に従う5号試験片を作成し、
JIS Z 2241に基いて試験を行つた。ここに試験
片は、圧延方向に対して0°(L方向)、90°(C方
向)および45°(D方向)の三ヶ所から採取し、試
験結果はL+C+2D/4の平均値で示した。ま
た曲げ特性については、JIS Z 2204により曲げ
試験片を作成し、JIS Z 2248に準拠した金属材
料曲げ試験方法によつて調べた。この曲げ特性
は、C曲げによる内側の曲げ半径が、板厚をtと
した場合それぞれ、8.0t、2.5t、2.0t、1.5t、1.0t、
0.5tおよび0tとなる各場合について曲げ試験を行
い、わん曲部の外側のさけ疵の有無を観察し、さ
け疵の発生しない限界の曲げ半径で評価した。さ
らに伸びフランジ成形性については、穴拡げ試験
によつて評価した。
Technical Field This invention relates to a technology for improving the bending properties and stretch-flange formability of high-strength cold-rolled steel sheets with a strength level of 50 kgf/mm 2 or higher. Background technology When it comes to high-strength cold-rolled steel sheets with a tensile strength of about 50 kgf/mm2 or more , the surface hardness generally increases rapidly, so cracks are likely to form on the surface due to mold galling during press forming, resulting in bending cracks and stretch flanges. There was a problem that cracks were likely to occur. In addition, this type of steel plate uses Si, Mn and P to ensure strength.
Since relatively large amounts of reinforcing elements such as these are added, a large amount of nonmetallic inclusions are likely to be produced, and there remains a problem in that cracks caused by such inclusions occur frequently. Purpose of the Invention The present invention advantageously solves the above-mentioned problems, and has the advantage of using a 50kgf/mm class 2 or higher high-strength cold-rolled steel sheet that does not cause bending cracks or stretch flange cracks even during press forming. The purpose of this research is to propose a new manufacturing method. Structure of the Invention This invention was developed after thorough research on press cracking, and in order to achieve the intended purpose, a thin decarburized layer is formed on the surface of the steel plate, and
This is based on the knowledge that it is extremely effective to suppress the amount of S in unavoidable impurities. That is, in this invention, C: 0.05 to 0.20% by weight
(hereinafter simply shown in %), Si: 0.05-1.50%, Nn:
1.00-3.50%, P: 0.020-0.100% and S:
Contains 0.010% or less, and sometimes additionally Nb: 0.010
~0.050%, Ti: 0.010~0.150%, and the remainder is iron and unavoidable impurities. After hot rolling, the slab is wound into a coil, and then cold rolled. In the manufacturing method of high-strength cold-rolled steel sheets, which consists of a series of steps in which continuous annealing is performed at a temperature range above the recrystallization temperature.
By performing the process at the following temperature, the steel plate surface has a thickness of 1
This is a method for producing a high-strength cold-rolled steel sheet with a strength level of 50 kgf/mm 2 or more, which is characterized by forming a decarburized layer of ~200 μm, and has excellent bending properties and stretch-flange formability. This invention will be specifically explained below. First, the reason why the composition of the steel sheet is limited to the above range in this invention will be explained. C: 0.05-0.20% If the C content is less than 0.05%, the tensile strength (TS) will decrease after continuous annealing, so in order to compensate for this,
The C content has the disadvantage of requiring large amounts of strength elements such as Si, Mn, P, Ti, Nb and V, while if it exceeds 0.20%, the fatigue strength and static strength of the spot welded joint will decrease. It was limited to the range of 0.05-0.20%. S: 0.010% or less Si: 0.05-1.50% Si effectively contributes to improving bendability and stretch flangeability, but its effect is only achieved at 0.05%.
On the other hand, if it is added in excess of 1.50%, the effect not only reaches saturation, but also hardens the steel and makes hot rolling and cold rolling difficult. It was limited to a range of 1.50%. Mn: 1.00-3.50% Mn is a useful element that contributes to improving strength, but if it is less than 1.00%, the effect of addition is poor;
If it exceeds 3.50%, the strength improvement will reach saturation, and the hot-rolled base plate will harden significantly, making cold rolling particularly difficult, so it was limited to a range of 1.00 to 3.50%. P: 0.020 to 0.100% P is a useful element that effectively contributes to strengthening steel when added in small amounts, but if it is less than 0.020%, the effect of addition is poor, while if it exceeds 0.100%, the effect just reaches saturation. 0.020 to 0.100, as there is a large risk that segregation will become apparent and workability will deteriorate.
% range. If a large amount of S is contained, stretch cracks and bending cracks will occur during press forming, so it is preferable to reduce S as much as possible, but up to 0.010% is acceptable. Furthermore, in this invention, Nb is used as a reinforcing element for steel.
One or two selected from among and Ti can be added in the following range. Nb: 0.010-0.050% Nb is an element that can effectively improve the strength of steel with the addition of a small amount.
The effect reaches saturation when it exceeds 0.010
It was supposed to be added in a range of ~0.050%. Ti: 0.010-0.150% Ti is also an element that can effectively improve the strength of steel when added in small amounts, just like Nb.
If the amount is less than 0.010%, the effect of addition is poor, while if it exceeds 0.150%, the effect reaches saturation, so it was added in the range of 0.010 to 0.150%. Figure 1 shows C: 0.08%, Si: 1.10%, Mn: 1.90.
%, P: 0.095%, Al: 0.050% and O: 0.0021
%, S of steel sheets with various compositions with S ranging from 0.001 to 0.018%.
The results of an investigation into the relationship between quantity and cleanliness are shown.
The cleanliness was measured in accordance with JIS G 0555. As is clear from the figure, when the amount of S exceeds 0.010%, the cleanliness deteriorates rapidly, but the deterioration in the cleanliness means that bending cracks and stretch flange cracks are more likely to occur. means. Now, the greatest feature of this invention is that it forms a decarburized layer on the surface of the steel sheet.By forming such a decarburized layer, even high-strength cold-rolled steel sheets of 50 kgf/mm grade 2 or higher can be press-formed. This made it possible to effectively prevent bending cracks and stretch flange cracks, which were sometimes feared to occur. However, if the thickness of the decarburized layer is less than 1 μm, the soft layer will be too thin and will not be effective in improving bending properties and mold-gathering properties.On the other hand, if it exceeds 200 μm, it will not only be difficult to obtain the target strength; The decarburized layer was limited to a range of 1 to 200 μm because the processing time for forming the decarburized layer would be long, which would impair economic efficiency. The decarburized layer is formed by winding the hot-rolled coil at a high temperature to form a decarburized layer on the surface of the hot-rolled coil. At this time, if the winding temperature is below 680℃,
Since the diffusion rate of C in the steel decreases and FeO, which is preferable for decarburization, immediately transforms into Fe 3 O 4 , it is difficult to form a sufficient decarburization layer, so the coiling temperature should be higher than 680°C. is necessary. In addition, the temperature at the exit side of the finishing stand during hot rolling is 950 to 850.
℃, the upper limit of the subsequent winding temperature is industrially sufficient to be 850°C or less. Examples Examples of the present invention will be described below. Six types of steel slabs having the chemical composition shown in Table 1 were hot-rolled, then wound into a coil, and then cold-rolled and continuously annealed to produce high-strength cold-rolled steel plates. Of the six types of steels A to F, excluding steel E, a decarburized layer with the thickness shown in Table 1 was formed during the manufacturing process. Formation was performed by hot rolling and then winding at a high temperature of 720°C. Note that the comparative example was decarburized by continuous annealing in an annealing atmosphere with a dew point of 10°C. Next, the mechanical properties of each of the obtained steel plates were investigated. The results are also listed in Table 1. For yield stress, tensile strength and elongation, No. 5 test pieces were prepared in accordance with JIS Z 2201.
Tests were conducted based on JIS Z 2241. Here, the test pieces were taken from three locations at 0° (L direction), 90° (C direction), and 45° (D direction) with respect to the rolling direction, and the test results are shown as the average value of L + C + 2D / 4. . Regarding bending properties, bending test pieces were prepared according to JIS Z 2204, and examined using a metal material bending test method according to JIS Z 2248. These bending characteristics are as follows: The inner bending radius due to C bending is 8.0t, 2.5t, 2.0t, 1.5t, 1.0t, respectively, where the plate thickness is t.
A bending test was conducted for each case of 0.5t and 0t, and the presence or absence of bulges on the outside of the curved portion was observed, and evaluation was made at the limit bending radius at which no bulges would occur. Furthermore, stretch flange formability was evaluated by a hole expansion test.
【表】【table】
【表】
第1表に示した試験結果から明らかなように、
この発明に従い得られた鋼板(A〜C)はいずれ
も、比較例(D〜F)に比べて、曲げ特性および
伸びフランジ成形性とも格段に優れている。
発明の効果
以上述べたようにこの発明によれば、従来プレ
ス成形時に曲げ割れや伸びフランジ割れの発生が
懸念された強度レベル50kgf/mm2以上の高張力冷
延鋼板において、上記の如き割れの発生を完全に
防止することができ、有利である。[Table] As is clear from the test results shown in Table 1,
All of the steel plates (A to C) obtained according to the present invention have significantly better bending properties and stretch flange formability than the comparative examples (D to F). Effects of the Invention As described above, according to the present invention, the above-mentioned cracks can be avoided in high-strength cold-rolled steel sheets with a strength level of 50 kgf/mm 2 or higher, where conventionally there was a concern that bending cracks and stretch flange cracks would occur during press forming. This is advantageous because the occurrence can be completely prevented.
第1図は、鋼中S量と清浄度との関係を示した
グラフである。
FIG. 1 is a graph showing the relationship between the amount of S in steel and the cleanliness.
Claims (1)
になるスラブを、熱間圧延したのちコイルに巻取
り、ついで冷間圧延を施してから再結晶温度以上
の温度範囲で連続焼鈍を施す一連の工程よりなる
高張力冷延鋼板の製造方法において、 熱間圧延に引続く巻取りを680℃を超え、850℃
以下の温度で行うことにより、鋼板表面に厚み1
〜200μmの脱炭層を形成させることを特徴とす
る、曲げ特性および伸びフランジ成形性に優れ
た、強度レベル50kgf/mm2以上の高張力冷延鋼板
の製造方法。 2 C:0.05〜0.20重量% Si:0.05〜1.50重量% Mn:1.00〜3.50重量% P:0.020〜0.100重量%および S:0.010重量%以下 を含有し、さらに Nb:0.010〜0.050%、 Ti:0.010〜0.150% のうちから選んだ一種又は二種を含み、残部は鉄
および不可避的不純物の組成になるスラブを、熱
間圧延したのちコイルに巻取り、ついで冷間圧延
を施してから再結晶温度以上の温度範囲で連続焼
鈍を施す一連の工程よりなる高張力冷延鋼板の製
造方法において、 熱間圧延に引続く巻取りを680℃を超え、850℃
以下の温度で行うことにより、鋼板表面に厚み1
〜200μmの脱炭層を形成させることを特徴とす
る、曲げ特性および伸びフランジ成形性に優れ
た、強度レベル50kgf/mm2以上の高張力冷延鋼板
の製造方法。[Claims] 1 Contains C: 0.05 to 0.20% by weight, Si: 0.05 to 1.50% by weight, Mn: 1.00 to 3.50% by weight, P: 0.020 to 0.100% by weight, and S: 0.010% by weight or less, with the remainder being iron and A high-strength cold-rolled steel sheet made of a series of processes in which a slab containing unavoidable impurities is hot-rolled, then wound into a coil, then cold-rolled, and then continuously annealed at a temperature above the recrystallization temperature. In the manufacturing method of
By performing the process at the following temperature, the steel plate surface has a thickness of 1
A method for producing a high-strength cold-rolled steel sheet having a strength level of 50 kgf/mm 2 or more and having excellent bending properties and stretch-flange formability, which is characterized by forming a decarburized layer of ~200 μm. 2 Contains C: 0.05 to 0.20% by weight, Si: 0.05 to 1.50% by weight, Mn: 1.00 to 3.50% by weight, P: 0.020 to 0.100% by weight, and S: 0.010% by weight or less, and further Nb: 0.010 to 0.050%, Ti: A slab containing one or two selected from 0.010 to 0.150%, with the remainder consisting of iron and unavoidable impurities, is hot rolled, wound into a coil, then cold rolled and then recrystallized. In the manufacturing method of high-strength cold-rolled steel sheets, which consists of a series of processes in which continuous annealing is performed at a temperature range above 680°C, the coiling following hot rolling is performed at a temperature exceeding 680°C, then 850°C.
By performing the process at the following temperature, the steel plate surface has a thickness of 1
A method for producing a high-strength cold-rolled steel sheet having a strength level of 50 kgf/mm 2 or more and having excellent bending properties and stretch-flange formability, which is characterized by forming a decarburized layer of ~200 μm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18512183A JPS6077956A (en) | 1983-10-05 | 1983-10-05 | High tensile strength cold-rolled steel plate having above 50kgf/mm2 strength with superior bending characteristic and stretch-flange formability and production of said steel plate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP18512183A JPS6077956A (en) | 1983-10-05 | 1983-10-05 | High tensile strength cold-rolled steel plate having above 50kgf/mm2 strength with superior bending characteristic and stretch-flange formability and production of said steel plate |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6077956A JPS6077956A (en) | 1985-05-02 |
| JPH0477049B2 true JPH0477049B2 (en) | 1992-12-07 |
Family
ID=16165231
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP18512183A Granted JPS6077956A (en) | 1983-10-05 | 1983-10-05 | High tensile strength cold-rolled steel plate having above 50kgf/mm2 strength with superior bending characteristic and stretch-flange formability and production of said steel plate |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6077956A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0697366A1 (en) | 1994-05-26 | 1996-02-21 | Kanji Tomidokoro | Jack |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009044861B3 (en) * | 2009-12-10 | 2011-06-22 | ThyssenKrupp Steel Europe AG, 47166 | Process for producing a readily deformable flat steel product, flat steel product and method for producing a component from such a flat steel product |
| WO2017093143A1 (en) * | 2015-11-30 | 2017-06-08 | Tata Steel Nederland Technology B.V. | A method for producing precipitation strengthened steel strip and steel strip produced thereby |
| CN112877632A (en) * | 2021-01-12 | 2021-06-01 | 鞍钢股份有限公司 | Aluminum-silicon plated steel plate for high-plasticity hot stamping forming and hot stamping method thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS4952756A (en) * | 1972-09-22 | 1974-05-22 | ||
| JPS553414A (en) * | 1978-06-21 | 1980-01-11 | Sandoz Ag | Fireeproofing cellulose acetate |
| JPS5655520A (en) * | 1979-10-09 | 1981-05-16 | Kawasaki Steel Corp | Production of surface decarbonized high carbon steel strip |
| JPS5858410B2 (en) * | 1979-11-27 | 1983-12-24 | 新日本製鐵株式会社 | Method for producing cold-rolled steel sheets with good workability by applying continuous casting and continuous annealing |
| JPS56158820A (en) * | 1981-01-07 | 1981-12-07 | Nippon Steel Corp | Manufacture of cold-rolled high-strength steel plate with high yield ratio and much less sliver for press working |
| JPS6047886B2 (en) * | 1981-03-02 | 1985-10-24 | 新日本製鐵株式会社 | Manufacturing method of high-strength thin steel plate for processing by continuous annealing |
-
1983
- 1983-10-05 JP JP18512183A patent/JPS6077956A/en active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0697366A1 (en) | 1994-05-26 | 1996-02-21 | Kanji Tomidokoro | Jack |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6077956A (en) | 1985-05-02 |
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