JPH0784334B2 - Optical fiber manufacturing method - Google Patents
Optical fiber manufacturing methodInfo
- Publication number
- JPH0784334B2 JPH0784334B2 JP31607287A JP31607287A JPH0784334B2 JP H0784334 B2 JPH0784334 B2 JP H0784334B2 JP 31607287 A JP31607287 A JP 31607287A JP 31607287 A JP31607287 A JP 31607287A JP H0784334 B2 JPH0784334 B2 JP H0784334B2
- Authority
- JP
- Japan
- Prior art keywords
- core
- base material
- optical fiber
- pipe
- diameter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B37/00—Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
- C03B37/01—Manufacture of glass fibres or filaments
- C03B37/02—Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor
- C03B37/025—Manufacture of glass fibres or filaments by drawing or extruding, e.g. direct drawing of molten glass from nozzles; Cooling fins therefor from reheated softened tubes, rods, fibres or filaments, e.g. drawing fibres from preforms
- C03B37/027—Fibres composed of different sorts of glass, e.g. glass optical fibres
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2205/00—Fibre drawing or extruding details
- C03B2205/08—Sub-atmospheric pressure applied, e.g. vacuum
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacture, Treatment Of Glass Fibers (AREA)
Description
【発明の詳細な説明】 〔産業上の利用分野〕 本発明は光フアイバの製造方法に関し、詳しくは線引用
母材から光フアイバを製造する新規な方法に関するもの
である。Description: TECHNICAL FIELD The present invention relates to a method for producing an optical fiber, and more particularly to a novel method for producing an optical fiber from a base material for line drawing.
光フアイバは一般に中心部にあつて主たる光伝送領域と
なるコアと該コアの外周にありコアより低屈折率のクラ
ツドからなり、コア径とクラツド径の径比が最終光フア
イバにおけるそれと同じに作成したコア部ガラスとクラ
ツド部ガラスからなる光フアイバ用母材を作製し、該母
材を線引きして設計値の径比のフアイバを得ている。An optical fiber is generally composed of a core, which is the center of the main optical transmission area at the center, and a cladding with a lower refractive index than the core, which is the same as that of the final optical fiber. An optical fiber preform composed of the core glass and the cladding glass was prepared, and the preform was drawn to obtain a fiber having a designed diameter ratio.
ところで、例えばシングルモードフアイバにおいては、
コア径:クラツド径の比が115程度が要求されている。
このように径比の大きなものを得ようとしても、従来の
VAD法によりスス付けする方法ではせいぜい該比が1:5程
度の母材しか作製できなかつたので、一たん1:5の比の
ガラス体を作製し、これにガラス管をかぶせて(ジヤケ
ツト付ともいう)、1:15の比を得ていた。By the way, for example, in single mode fiber,
A ratio of core diameter to cladding diameter of about 115 is required.
Even if you try to obtain a large diameter ratio like this,
With the method of sooting by the VAD method, at best, only the base material with a ratio of about 1: 5 could be produced, so at the moment, make a glass body with a ratio of 1: 5, cover it with a glass tube (with a jacket) Also called), I got a ratio of 1:15.
また、コア用ロツドをクラツド用パイプ内に挿入し、両
者を加熱融着(コラツプス)するいわゆるロツドインチ
ユーブ法でも、1回のクラプスで1:15のコア:クラツド
径比を達成することは困難である。例えばクラツド用パ
イプの外径が25mmφ程度の場合のコア径としては1.67mm
φ程度の細さとなり、コラツプスの過程で、パイプが十
分に加熱される前に熱容量の小さいコアが軟化するため
のコア用ロツドが変形し易く、これによりコラツプスの
後、コア部の偏心が生じ易い。逆に変形が問題とならな
い5mmφ程度のコア径にすると、クラツド用パイプの外
径には75mmφが必要となるが、このような太いガラスを
加熱融着することは、酸水素淡等の従来の加熱手段では
殆んど不可能である。従つてロツドインチユーブ法でも
径比1:7以上では、一度目のロツドインチユーブにより
得たコアとクラツドからなるプリフオームの外周にさら
にスス付けをして、コア:クラツド径比を1:7以上にす
るか、或は該プリフオームを延伸して細径ロツドとし、
もう一度ガラスパイプとロツドインチユーブ法で加熱融
着して目的を達成していた。Further, even in the so-called rod-inch-Yub method of inserting the core rod into the cladding pipe and heating and fusing the two together (collapse), it is possible to achieve a core: clad diameter ratio of 1:15 with one crap. Have difficulty. For example, when the outer diameter of the cladding pipe is about 25 mmφ, the core diameter is 1.67 mm.
The diameter is about φ, and during the collapsing process, the core rod is easily deformed to soften the core with a small heat capacity before the pipe is sufficiently heated, which causes eccentricity of the core after collapsing. easy. On the contrary, if the core diameter is about 5 mmφ where deformation is not a problem, then 75 mmφ is required for the outer diameter of the cladding pipe. Almost impossible with heating means. Therefore, even in the rod-inch uve method, if the diameter ratio is 1: 7 or more, soot is further attached to the outer periphery of the preform consisting of the core and the cladding obtained by the first rod-inch yuve, and the core-to-clad diameter ratio is 1 :. 7 or more, or by stretching the preform into a rod of small diameter,
Once again, the object was achieved by heating and fusing the glass pipe and the rod-inch-Yube method.
以上のように、コア:クラツト径比が1:15程度に大きい
光フアイバ母材を得ようとすると、従来法ではいずれも
工程が複雑となり、フアイバの低コスト化の防げとなつ
ていた。As described above, when trying to obtain an optical fiber preform having a large core: clat diameter ratio of about 1:15, the conventional method complicates the process and prevents the cost reduction of the fiber.
本発明はこのような現状に鑑みてなされたものであつ
て、簡単な一回工程でコア径:クラツド系の比が充分に
大きい光フアイバ用母材を偏心なく作製できる方法を提
案することを目的とする。The present invention has been made in view of the above circumstances, and proposes a method capable of producing an optical fiber preform having a sufficiently large ratio of core diameter: cladding system without eccentricity in a simple one-step process. To aim.
本発明者らは従来法のコアロツドに対し、設定比を満足
するように外周部を付加形成して線引母材を得るという
方法とは全く発想を転換し、コア及びクラツドからなる
母材のコア部を開孔して、そのコア断面積を削減したパ
イプ状母材をそのまま線引プリフオームとすることを考
えつき、従来法の問題点を解決できた。The present inventors have completely changed the idea from the method of obtaining the wire drawing base material by additionally forming the outer peripheral portion so as to satisfy the set ratio with respect to the core rod of the conventional method. It was possible to solve the problems of the conventional method by opening the core and using the pipe-shaped preform with a reduced core cross-sectional area as it is as a wire drawing preform.
本発明はコア部及びクラツド部を有する光フアイバ用母
材のコア部の一部に長手方向に貫通する孔を開けてパイ
プ状母材とした後、該パイプ状母材の内部を減圧に保ち
つつ線引することを特徴とする光フアイバの製造方法に
関する。該孔の表面は研摩処理を施されることが好まし
く、また開孔後のコア部面積:クラツド部面積の比が線
比後のシングルモードフアイバとして設計されているコ
ア面積:クラツド面積の比に等しくなるように開けるこ
とは、設計値のシングルモードフアイバを簡単に得るこ
とができるので、本発明の特に好ましい実施態様であ
る。The present invention is to form a pipe-shaped base material by forming a hole penetrating in the longitudinal direction in a part of the core portion of an optical fiber base material having a core portion and a cladding portion, and then maintaining the inside of the pipe-shaped base material at a reduced pressure. The present invention relates to a method for manufacturing an optical fiber, which is characterized by drawing while drawing. The surface of the hole is preferably subjected to polishing treatment, and the ratio of the core area after opening to the area of the cladding is the ratio of the core area to the area of the cladding designed as a single mode fiber after the linear ratio. Opening to equality is a particularly preferred embodiment of the present invention, as it is easy to obtain a designed single mode fiber.
線引時のパイプ状母材内部の減圧は真空ポンプ引き又は
該母材を真空封止することにより実現できる。The pressure reduction inside the pipe-shaped base material during drawing can be realized by vacuum pumping or vacuum-sealing the base material.
以下図面を参照して本発明を具体的に説明する。本発明
ではまず第1図(a)に示すようなコア部1及びクラツ
ド部2を有する光フアイバ用ガラス母材を作成してお
く。この母材の作成方法は公知技術のVAD法、MCVD法、
外付け法等ガラススートを堆積させてこれを透明ガラス
化する方法や、ロツドインチユーブ法等のいずれによつ
てもよい。次に第1図(b)に示すように、コア部1の
中心部分に、中心軸方向に母材を貫通する孔3を開け
る。具体的には超音波開孔器等を用いて開孔する。この
とき、フアイバの設計値のコア:クラツド径比から両者
の断面積比を求めておき、開孔及びこれに続く研摩後の
コア部とクラツド部の面積比を上記設計値の比に一致さ
せるように行なう。次に孔3の内面を例えば光学研摩ま
たはフツ素系ガス雰囲気での熱処理によりエツチングし
た後、外周部から加熱して平滑化する等の手段で研摩す
る。The present invention will be specifically described below with reference to the drawings. In the present invention, first, a glass preform for optical fibers having a core portion 1 and a cladding portion 2 as shown in FIG. 1 (a) is prepared. This base material is produced by the known VAD method, MCVD method,
Any of a method of depositing glass soot such as an external method to make it into a transparent vitreous material, or a rod-inch tube method may be used. Next, as shown in FIG. 1B, a hole 3 penetrating the base material in the direction of the central axis is formed in the central portion of the core portion 1. Specifically, the holes are opened using an ultrasonic hole opener or the like. At this time, the cross-sectional area ratio of the two is calculated from the core: clad diameter ratio of the fiber design value, and the area ratio of the core portion and the cladding portion after the opening and subsequent polishing is made to match the above design value ratio. Do so. Next, the inner surface of the hole 3 is etched by, for example, optical polishing or heat treatment in a fluorine-based gas atmosphere, and then polished from the outer peripheral portion by means such as heating and smoothing.
以上の処理を行つた後、得られたパイプ状母材を、第1
図(c)に示すように線引炉6にセツト後、その片端を
接続具4により真空ポンプ5に接続して、パイプ状母材
の内部を0.1〜20torrの減圧にしながら、線引炉6で加
熱して線引きしフアイバ化する。あるいはパイプ状母材
をその内部が減圧を保持した状態で封止し、これを線引
きする。このような母材の真空封止は、第2図(a)に
示すように、母材を旋盤7に保持し一端にロータリージ
ヨイント8を取りつけ、まず母材の内部をパイプ5で減
圧に引きながらその一端部を外部から加熱して融着し、
その後真空ポンプ5にて減圧し、内圧が0.1〜20torr好
ましくは10torr以下となつた時点でもう一端を加熱する
ことにより第2図(b)に示すように融着することによ
り行なう。After performing the above processing, the pipe-shaped base material obtained was
After being set in the drawing furnace 6 as shown in FIG. 6 (c), one end of the drawing furnace 6 is connected to the vacuum pump 5 by the connecting tool 4 to reduce the pressure inside the pipe-shaped base material to 0.1 to 20 torr while the drawing furnace 6 Heat to draw and draw fiber. Alternatively, the pipe-shaped base material is sealed in a state where the inside of the pipe-shaped base material maintains a reduced pressure, and this is drawn. As shown in FIG. 2 (a), such vacuum sealing of the base material is performed by holding the base material on a lathe 7 and attaching a rotary joint 8 at one end, and first depressurizing the inside of the base material with a pipe 5. While pulling, heat one end from the outside to fuse,
After that, the pressure is reduced by the vacuum pump 5, and when the internal pressure becomes 0.1 to 20 torr, preferably 10 torr or less, the other end is heated to cause fusion as shown in FIG. 2 (b).
本発明は従来技術で得られる径比1:5〜1:7程度の母材中
のコア部を穴明けすることで、コア断面積:クラツド断
面積比を所望値に調整できる。したがつて穴明け前の母
材の作製には、例えば簡単なロツドインチユーブ法によ
り、コア変形のおそれのない大径コア材を用いて行なえ
ばよく、これを穴明けするという簡単な工程で、径比1:
15程度のプリフオームを得ることができる。そしてこの
パイプ状プリフオームを線引きすることにより、所望の
径比で偏心のない光フアイバを得ることができる。また
フアイバの長手方向に安定したコア径を得ることができ
るので、フアイバの伝送損失を低減できる。したがつて
本発明の方法はコア径に比してクラツド系の大きい、シ
ングルモードフアイバの製造に用いると有利であるが、
光フアイバ一般の製法としても利用して有利であること
は勿論である。According to the present invention, the core cross-sectional area: clad cross-sectional area ratio can be adjusted to a desired value by drilling the core portion in the base material having a diameter ratio of about 1: 5 to 1: 7 obtained by the prior art. Therefore, the base material before drilling may be prepared, for example, by a simple rod-inch uve method using a large-diameter core material that does not cause core deformation. And the diameter ratio is 1:
You can get about 15 preforms. By drawing this pipe-shaped preform, an optical fiber having a desired diameter ratio and no eccentricity can be obtained. Moreover, since a stable core diameter can be obtained in the longitudinal direction of the fiber, the transmission loss of the fiber can be reduced. Therefore, the method of the present invention is advantageous in the production of a single mode fiber having a large cladding system compared to the core diameter,
Of course, it can be advantageously used as a general manufacturing method for optical fibers.
実施例1 外径35mmφ、内径10mmφのフツ素添加石英ガラスパイプ
(フツ素添加量0.9重量%、比屈折率差0.3%)の中空部
分に、コアとなる直径9mmφの純石英ガラス棒を挿入
し、この状態で該パイプの外側から加熱して両者を融着
一体化し、ガラス母材を得た。該ガラス母材の中心に母
材を貫通する直径8mmφの孔を超音波開孔器を用いて開
孔した。次にこの孔の内面をSF6雰囲気での熱処理によ
り研摩し、孔の直径を8.7mmφにまづ拡大した。得られ
たパイプ状母材の孔内を真空ポンプにてP=500mmHgに
まで減圧しながら、線引炉で2010℃に加熱し、張力10
g、線引速度100m/minで線引きして、外径125mμ、コア
径8.3μm、コア径:クラツド径(比)≒1:15コア・ク
ラツドの比屈折率差0.3%のシングルモードフアイバが
得られた。このフアイバの伝送損失は波長1.55μmで01
9dB/kmと非常に良好な結果を示した。Example 1 A pure silica glass rod having a diameter of 9 mmφ serving as a core was inserted into the hollow portion of a fluorine-added quartz glass pipe having an outer diameter of 35 mmφ and an inner diameter of 10 mmφ (fluorine addition amount: 0.9% by weight, relative refractive index difference: 0.3%). In this state, the pipe was heated from the outside to fuse them together to obtain a glass preform. A hole having a diameter of 8 mm and penetrating the base material was opened at the center of the glass base material using an ultrasonic perforator. Next, the inner surface of this hole was polished by heat treatment in an SF 6 atmosphere, and the diameter of the hole was expanded to 8.7 mmφ. The inside of the hole of the obtained pipe-shaped base material was depressurized to P = 500 mmHg with a vacuum pump, and heated to 2010 ° C in a drawing furnace to obtain a tension of
g, wire drawing speed 100m / min, and outer diameter 125mμ, core diameter 8.3μm, core diameter: cladding diameter (ratio) ≈ 1:15, single-mode fiber with 0.3% relative refractive index difference between core and cladding. Was given. The transmission loss of this fiber is 01 at a wavelength of 1.55 μm.
A very good result of 9 dB / km was shown.
本発明はクラツドの径又はフアイバ外径に対して小さい
コア系のフアイバを、フアイバ長手方向に安定したコア
径でかつコアの偏心もなく低損失であるフアイバを簡単
な工程で実施できるという非常に画期的な製造方法であ
る。通常のフアイバの製造に利用して有利であることは
勿論であるが、特にシングルモードフアイバの製造に用
いて栄品質上、生産コスト上に大きな効果が得られる。The present invention provides a core fiber that is small relative to the diameter of the cladding or the outer diameter of the fiber, and has a stable core diameter in the longitudinal direction of the fiber and a fiber that has a low loss without eccentricity of the core. This is an epoch-making manufacturing method. It is of course advantageous to use it for the production of ordinary fibers, but especially when it is used for the production of single mode fibers, a great effect can be obtained in terms of quality and production cost.
第1図(a),(b)及び(c)は本発明の実施例を各
工程につき説明する概略図、第2図(a)及び(b)は
本発明の別の実施態様を説明する概略断面図である。FIGS. 1 (a), (b) and (c) are schematic diagrams for explaining each embodiment of the present invention, and FIGS. 2 (a) and 2 (b) illustrate another embodiment of the present invention. It is a schematic sectional drawing.
Claims (5)
用母材のコア部の一部に長手方向に貫通する孔を開けて
パイプ状母材とした後、該パイプ状母材の内部を減圧に
保ちつつ線引することを特徴とする光フアイバの製造方
法。1. A pipe-shaped base material having a hole penetrating in a longitudinal direction in a part of a core portion of an optical fiber base material having a core portion and a cladding portion, and the inside of the pipe-shaped base material is decompressed. A method for producing an optical fiber, which is characterized in that drawing is performed while maintaining
る特許請求の範囲第1項に記載の光フアイバの製造方
法。2. The method for producing an optical fiber according to claim 1, wherein the surface of the hole is subjected to polishing treatment.
面積の比が線引後のシングルモードフアイバとして設計
されているコア面積:クラツド面積の比に等しくなるよ
うにあけられる特許請求の範囲第1項又は第2項に記載
の光フアイバの製造方法。3. The hole is formed so that the ratio of the core area after the opening: the area of the cladding is equal to the ratio of the core area designed as a single mode fiber after drawing: the area of the cladding. A method for manufacturing an optical fiber according to claim 1 or 2.
きにより保たれる特許請求の範囲第1項に記載の光フア
イバの製造方法。4. The method for producing an optical fiber according to claim 1, wherein the reduced pressure inside the pipe-shaped base material is maintained by vacuum pumping.
封止により保たれる特許請求の範囲第1項に記載の光フ
アイバの製造方法。5. The method for producing an optical fiber according to claim 1, wherein the reduced pressure inside the pipe-shaped base material is maintained by vacuum sealing the base material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP31607287A JPH0784334B2 (en) | 1987-12-16 | 1987-12-16 | Optical fiber manufacturing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP31607287A JPH0784334B2 (en) | 1987-12-16 | 1987-12-16 | Optical fiber manufacturing method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH01160841A JPH01160841A (en) | 1989-06-23 |
| JPH0784334B2 true JPH0784334B2 (en) | 1995-09-13 |
Family
ID=18072950
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP31607287A Expired - Fee Related JPH0784334B2 (en) | 1987-12-16 | 1987-12-16 | Optical fiber manufacturing method |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0784334B2 (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MXPA01010868A (en) | 1999-04-26 | 2002-05-06 | Corning Inc | An optical fiber and a method for fabricating a low polarization-mode dispersion and low attenuation optical fiber. |
| KR20040024598A (en) | 2001-07-31 | 2004-03-20 | 코닝 인코포레이티드 | The Method for fabricating a low polarization mode dispersion optical fiber |
| US10800865B2 (en) | 2015-09-14 | 2020-10-13 | Exxonmobil Chemical Patents Inc. | Process for making branched EPDM and the EPDM therefrom |
-
1987
- 1987-12-16 JP JP31607287A patent/JPH0784334B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| JPH01160841A (en) | 1989-06-23 |
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